Identification of the elastic-plastic properties of CrN coating on elastic-plastic substrate by nanoindentation using finite element method-reverse algorithm

•Nanoindentation of CrN coatings deposited at different substrate bias voltages.•A trust-region algorithm is used to predict the tensile properties of the coating.•The uniqueness issue is addressed by narrowing the range of the initial guess.•The stress-strains coating characteristics were accuratel...

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Published inThin solid films Vol. 756; p. 139356
Main Authors Ben Ammar, Y., Aouadi, Khalil, Nouveau, Corinne, Besnard, Aurélien, Montagne, Alex
Format Journal Article
LanguageEnglish
Published Elsevier B.V 31.08.2022
Elsevier
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Online AccessGet full text
ISSN0040-6090
1879-2731
1879-2731
DOI10.1016/j.tsf.2022.139356

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Abstract •Nanoindentation of CrN coatings deposited at different substrate bias voltages.•A trust-region algorithm is used to predict the tensile properties of the coating.•The uniqueness issue is addressed by narrowing the range of the initial guess.•The stress-strains coating characteristics were accurately generated. This paper proposes an identification methodology based on nanoindentation analysis of coating/substrate system to extract the elastic-plastic properties of coating materials on elastic-plastic substrate when the indenter penetration depth is greater than the film thickness. In order to accurately predict the elastic-plastic properties of the coating materials, a trust-region reflective optimization algorithm is integrated with the finite element analysis, in cooperation with the Jönsson and Hogmark model. The proposed reverse analysis algorithm modifies a predicted load-displacement (P-h) curve by changing the elastic-plastic properties of the coating and the substrate until it fits the experimental nanoindentation (P-h) curve. Numerical and instrumental indentations tests were carried out on a CrN film/Martensitic stainless steel substrate system to verify the proposed reverse method, by which Young's modulus (E), yield stress (σy), and work hardening exponent of the film were obtained. A sensitivity analysis is conducted to study the effect of the elastic-plastic properties of the CrN film/substrate on the (P-h) curve. The results showed a high impact to the loading and unloading part of the (P-h) curve due to variations in (E) and (σy) of the steel substrate compared to those of the CrN coating.
AbstractList This paper proposes an identification methodology based on nanoindentation analysis of coating/substrate system to extract the elastic-plastic properties of coating materials on elastic-plastic substrate when the indenter penetration depth is greater than the film thickness. In order to accurately predict the elastic-plastic properties of the coating materials, a trust-region reflective optimization algorithm is integrated with the finite element analysis, in cooperation with the Jönsson and Hogmark model. The proposed reverse analysis algorithm modifies a predicted load-displacement (P-h) curve by changing the elastic-plastic properties of the coating and the substrate until it fits the experimental nanoindentation (P-h) curve. Numerical and instrumental indentations tests were carried out on a CrN film/Martensitic stainless steel substrate system to verify the proposed reverse method, by which Young's modulus (E), yield stress (σy), and work hardening exponent of the film were obtained. A sensitivity analysis is conducted to study the effect of the elastic-plastic properties of the CrN film/substrate on the (P-h) curve. The results showed a high impact to the loading and unloading part of the (P-h) curve due to variations in (E) and (σy) of the steel substrate compared to those of the CrN coating.
•Nanoindentation of CrN coatings deposited at different substrate bias voltages.•A trust-region algorithm is used to predict the tensile properties of the coating.•The uniqueness issue is addressed by narrowing the range of the initial guess.•The stress-strains coating characteristics were accurately generated. This paper proposes an identification methodology based on nanoindentation analysis of coating/substrate system to extract the elastic-plastic properties of coating materials on elastic-plastic substrate when the indenter penetration depth is greater than the film thickness. In order to accurately predict the elastic-plastic properties of the coating materials, a trust-region reflective optimization algorithm is integrated with the finite element analysis, in cooperation with the Jönsson and Hogmark model. The proposed reverse analysis algorithm modifies a predicted load-displacement (P-h) curve by changing the elastic-plastic properties of the coating and the substrate until it fits the experimental nanoindentation (P-h) curve. Numerical and instrumental indentations tests were carried out on a CrN film/Martensitic stainless steel substrate system to verify the proposed reverse method, by which Young's modulus (E), yield stress (σy), and work hardening exponent of the film were obtained. A sensitivity analysis is conducted to study the effect of the elastic-plastic properties of the CrN film/substrate on the (P-h) curve. The results showed a high impact to the loading and unloading part of the (P-h) curve due to variations in (E) and (σy) of the steel substrate compared to those of the CrN coating.
ArticleNumber 139356
Author Montagne, Alex
Aouadi, Khalil
Nouveau, Corinne
Besnard, Aurélien
Ben Ammar, Y.
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Keywords Film/substrate system
Elasto-plastic properties
Inverse finite element material modelling
Substrate effect
Instrumented-indentation testing
Composite hardness modeling
Language English
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Snippet •Nanoindentation of CrN coatings deposited at different substrate bias voltages.•A trust-region algorithm is used to predict the tensile properties of the...
This paper proposes an identification methodology based on nanoindentation analysis of coating/substrate system to extract the elastic-plastic properties of...
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StartPage 139356
SubjectTerms Composite hardness modeling
Elasto-plastic properties
Engineering Sciences
Film/substrate system
Instrumented-indentation testing
Inverse finite element material modelling
Mechanics
Mechanics of materials
Substrate effect
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Title Identification of the elastic-plastic properties of CrN coating on elastic-plastic substrate by nanoindentation using finite element method-reverse algorithm
URI https://dx.doi.org/10.1016/j.tsf.2022.139356
https://hal.science/hal-03770748
http://hdl.handle.net/10985/22516
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