Synthesis and physico-chemical properties of new green electrolyte 1-butyl-3-methylimidazolium perchlorate
1-butyl-3-methylimidazolium perchlorate（[BMIM]ClO4） was synthesized by two steps with N-methylimidazolium.Some physico-chemical properties,such as density,surface tension,viscosity,electrical conductivity as well as electrochemical window,were investigated and solvent performance was also studied.Th...
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| Published in | Transactions of Nonferrous Metals Society of China Vol. 20; no. 10; pp. 2032 - 2036 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2010
School of Materials and Metallurgy,Northeastern University,Shenyang 110004,China College of Applied Chemistry,Shenyang University of Chemical Technology,Shenyang 110142,China%School of Materials and Metallurgy,Northeastern University,Shenyang 110004,China%School of Materials and Metallurgy,Northeastern University,Shenyang 110004,China Beijing General Research Institute of Mining and Metallurgy,Beijing 100044,China |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1003-6326 |
| DOI | 10.1016/S1003-6326(09)60413-1 |
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| Abstract | 1-butyl-3-methylimidazolium perchlorate（[BMIM]ClO4） was synthesized by two steps with N-methylimidazolium.Some physico-chemical properties,such as density,surface tension,viscosity,electrical conductivity as well as electrochemical window,were investigated and solvent performance was also studied.The results show that this kind of ionic liquid is an excellent electrolyte with low viscosity,high electrical conductivity and wide electrochemical window.In addition,[BMIM]ClO4 is soluble in most conventional solvents and some metal oxides have high solubility in it,which lays the foundation of direct electrolysis of metal oxides in this ionic liquid. |
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| AbstractList | 1-butyl-3-methylimidazolium perchlorate（[BMIM]ClO4） was synthesized by two steps with N-methylimidazolium.Some physico-chemical properties,such as density,surface tension,viscosity,electrical conductivity as well as electrochemical window,were investigated and solvent performance was also studied.The results show that this kind of ionic liquid is an excellent electrolyte with low viscosity,high electrical conductivity and wide electrochemical window.In addition,[BMIM]ClO4 is soluble in most conventional solvents and some metal oxides have high solubility in it,which lays the foundation of direct electrolysis of metal oxides in this ionic liquid. 1-butyl-3-methylimidazolium perchlorate ([BMIM]ClO 4) was synthesized by two steps with N-methylimidazolium. Some physico-chemical properties, such as density, surface tension, viscosity, electrical conductivity as well as electrochemical window, were investigated and solvent performance was also studied. The results show that this kind of ionic liquid is an excellent electrolyte with low viscosity, high electrical conductivity and wide electrochemical window. In addition, [BMIM]ClO 4 is soluble in most conventional solvents and some metal oxides have high solubility in it, which lays the foundation of direct electrolysis of metal oxides in this ionic liquid. TF8; 1-butyl-3-methylimidazolium perchlorate ([BMIM]ClO4) was synthesized by two steps with N-methylimidazolium. Some physico-chemical properties, such as density, surface tension, viscosity, electrical conductivity as well as electrochemical window, were investigated and solvent performance was also studied. The results show that this kind of ionic liquid is an excellent electrolyte with low viscosity, high electrical conductivity and wide electrochemical window. In addition, [BMIM]ClO4 is soluble in most conventional solvents and some metal oxides have high solubility in it, which lays the foundation of direct electrolysis of metal oxides in this ionic liquid. |
| Author | 王晓丹 吴文远 徐赣峰 将开喜 |
| AuthorAffiliation | School of Materials and Metallurgy, Northeastern University, Shenyang 110004, China College of Applied Chemistry, Shenyang University of Chemical Technology, Shenyang 110142, China Beijing General Research Institute of Mining and Metallurgy, Beijing 100044, China |
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| Cites_doi | 10.1021/ic0505450 10.1021/am900020w 10.1016/j.electacta.2006.03.016 10.1149/1.1391827 10.1007/s00396-008-1921-z 10.1016/S0022-1139(99)00111-6 10.1016/S0013-4686(02)00509-1 10.1021/ef700734x 10.1021/ac701788r 10.1021/jp711804j 10.1021/la9012119 |
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| Keywords | solubility 1-butyl-3-methylimidazolium perchlorate electrolyte room temperature ionic liquid |
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| Notes | 1-butyl-3-methylimidazolium perchlorate 43-1239/TG O623.624 O614.33 solubility room temperature ionic liquid; 1-butyl-3-methylimidazolium perchlorate; electrolyte; solubility electrolyte room temperature ionic liquid |
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| Snippet | 1-butyl-3-methylimidazolium perchlorate（[BMIM]ClO4） was synthesized by two steps with N-methylimidazolium.Some physico-chemical properties,such as... 1-butyl-3-methylimidazolium perchlorate ([BMIM]ClO 4) was synthesized by two steps with N-methylimidazolium. Some physico-chemical properties, such as density,... TF8; 1-butyl-3-methylimidazolium perchlorate ([BMIM]ClO4) was synthesized by two steps with N-methylimidazolium. Some physico-chemical properties, such as... |
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| SubjectTerms | 1-butyl-3-methylimidazolium perchlorate electrolyte room temperature ionic liquid solubility 物理化学性质 电化学窗口 电解液 离子液体 绿色合成 金属氧化物 高氯酸盐 |
| Title | Synthesis and physico-chemical properties of new green electrolyte 1-butyl-3-methylimidazolium perchlorate |
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