Low-temperature solution synthesis and characterization of Ce-doped YAG nanoparticles
Monophasic Ce3＋-doped yttrium aluminum garnet （Ce：YAG） nanoparticles with high crystallinity and tunable grain size ranging from -19-30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the syn- thesis, aluminum, yttrium, and cerium nitrates were use...
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| Published in | Journal of rare earths Vol. 33; no. 6; pp. 591 - 598 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.06.2015
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(14)60458-0 |
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| Abstract | Monophasic Ce3＋-doped yttrium aluminum garnet （Ce：YAG） nanoparticles with high crystallinity and tunable grain size ranging from -19-30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the syn- thesis, aluminum, yttrium, and cerium nitrates were used as starting materials, ammonium sulfate as dispersant, and a combination of ammonium bicarbonate and ammonia as precipitating agent. Influence of precipitation temperature, the pH value of precipitant solu- tions, aging period, calcination conditions, and Ce-doping level were investigated for controlling the purity, particle size, and photo- luminescence performance of the Ce：YAG nanoparticles. High-purity YAG nanoparticles were prepared at pH= 10.50-11.00 and cal- cination temperatures of 850-1100 ~C with a calcination time of 3 h. With increasing Ce3＋ concentration, the peak in the emission spectra of the obtained nanopowders shifted from 529 nm for the 0.67 wt.%-Ce：YAG to 544 nm for the 3.4 wt.%-Ce：YAG, while the strongest photoluminescence intensity was observed for the 1.3 wt.%-Ce：YAG nanoparticles. |
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| AbstractList | Monophasic Ce3+-doped yttrium aluminum garnet (Ce:YAG) nanoparticles with high crystallinity and tunable grain size ranging from ∼19–30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the synthesis, aluminum, yttrium, and cerium nitrates were used as starting materials, ammonium sulfate as dispersant, and a combination of ammonium bicarbonate and ammonia as precipitating agent. Influence of precipitation temperature, the pH value of precipitant solutions, aging period, calcination conditions, and Ce-doping level were investigated for controlling the purity, particle size, and photoluminescence performance of the Ce:YAG nanoparticles. High-purity YAG nanoparticles were prepared at pH=10.50–11.00 and calcination temperatures of 850–1100 °C with a calcination time of 3 h. With increasing Ce3+ concentration, the peak in the emission spectra of the obtained nanopowders shifted from 529 nm for the 0.67 wt.%-Ce:YAG to 544 nm for the 3.4 wt.%-Ce:YAG, while the strongest photoluminescence intensity was observed for the 1.3 wt.%-Ce:YAG nanoparticles.
XRD patterns of 0.67% (1), 1.3% (2), 2.0% (3), 2.7% (4), and 3.4% (5) Ce-doped YAG products synthesized by calcination at 1000 °C for 3 h (The inset shows magnified (420) peak positions, clearly indicating the successive shifting to low angles with increasing Ce-doping concentration) and Emission spectra of the YAG with different Ce3+ doping concentrations of 0.67% (1), 1.3% (2), 2.0% (3), 2.7% (4), and 3.4% (5) (All spectra were recorded at room temperature) Monophasic Ce super(3+)-doped yttrium aluminum garnet (Ce:YAG) nanoparticles with high crystallinity and tunable grain size ranging from ~19-30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the synthesis, aluminum, yttrium, and cerium nitrates were used as starting materials, ammonium sulfate as dispersant, and a combination of ammonium bicarbonate and ammonia as precipitating agent. Influence of precipitation temperature, the pH value of precipitant solutions, aging period, calcination conditions, and Ce-doping level were investigated for controlling the purity, particle size, and photoluminescence performance of the Ce:YAG nanoparticles. High-purity YAG nanoparticles were prepared at pH=10.50-11.00 and calcination temperatures of 850-1100 [degrees]C with a calcination time of 3 h. With increasing Ce super(3+) concentration, the peak in the emission spectra of the obtained nanopowders shifted from 529 nm for the 0.67 wt.%-Ce:YAG to 544 nm for the 3.4 wt.%-Ce:YAG, while the strongest photoluminescence intensity was observed for the 1.3 wt.%-Ce:YAG nanoparticles. Monophasic Ce3＋-doped yttrium aluminum garnet （Ce：YAG） nanoparticles with high crystallinity and tunable grain size ranging from -19-30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the syn- thesis, aluminum, yttrium, and cerium nitrates were used as starting materials, ammonium sulfate as dispersant, and a combination of ammonium bicarbonate and ammonia as precipitating agent. Influence of precipitation temperature, the pH value of precipitant solu- tions, aging period, calcination conditions, and Ce-doping level were investigated for controlling the purity, particle size, and photo- luminescence performance of the Ce：YAG nanoparticles. High-purity YAG nanoparticles were prepared at pH= 10.50-11.00 and cal- cination temperatures of 850-1100 ~C with a calcination time of 3 h. With increasing Ce3＋ concentration, the peak in the emission spectra of the obtained nanopowders shifted from 529 nm for the 0.67 wt.%-Ce：YAG to 544 nm for the 3.4 wt.%-Ce：YAG, while the strongest photoluminescence intensity was observed for the 1.3 wt.%-Ce：YAG nanoparticles. |
| Author | 吉成 冀立宇 连刘超 沈丽明 张晓艳 王一峰 Arunava Gupta |
| AuthorAffiliation | State Key Laboratory of Materials-Oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, China Centre for Materials for Information Technology, University of Alabama, Tuscaloosa, AL 35487, United States |
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| Keywords | nanoparticles photoluminescence Ce-doping YAG rare earths |
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| Notes | 11-2788/TF Monophasic Ce3＋-doped yttrium aluminum garnet （Ce：YAG） nanoparticles with high crystallinity and tunable grain size ranging from -19-30 nm were prepared by a modified co-precipitation process with a follow-up calcination treatment. For the syn- thesis, aluminum, yttrium, and cerium nitrates were used as starting materials, ammonium sulfate as dispersant, and a combination of ammonium bicarbonate and ammonia as precipitating agent. Influence of precipitation temperature, the pH value of precipitant solu- tions, aging period, calcination conditions, and Ce-doping level were investigated for controlling the purity, particle size, and photo- luminescence performance of the Ce：YAG nanoparticles. High-purity YAG nanoparticles were prepared at pH= 10.50-11.00 and cal- cination temperatures of 850-1100 ~C with a calcination time of 3 h. With increasing Ce3＋ concentration, the peak in the emission spectra of the obtained nanopowders shifted from 529 nm for the 0.67 wt.%-Ce：YAG to 544 nm for the 3.4 wt.%-Ce：YAG, while the strongest photoluminescence intensity was observed for the 1.3 wt.%-Ce：YAG nanoparticles. JI Cheng , JI Llyu , LIAN Liuchao , SHEN Liming , ZHANG Xiaoyan , WANG Yifeng , Arunava Gupta （1. State Key Laboratory of Materials-Oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, China,2. Centre for Materials for Information Technology, University of Alabama, Tuscaloosa, AL 35487, United States） ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| Snippet | Monophasic Ce3＋-doped yttrium aluminum garnet （Ce：YAG） nanoparticles with high crystallinity and tunable grain size ranging from -19-30 nm were prepared by a... Monophasic Ce3+-doped yttrium aluminum garnet (Ce:YAG) nanoparticles with high crystallinity and tunable grain size ranging from ∼19–30 nm were prepared by a... Monophasic Ce super(3+)-doped yttrium aluminum garnet (Ce:YAG) nanoparticles with high crystallinity and tunable grain size ranging from ~19-30 nm were... |
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| SubjectTerms | AG纳米粒子 Aluminum Calcination Ce-doping Ce掺杂 Ce：YAG Nanoparticles Photoluminescence Rare earth metals rare earths Synthesis YAG Yttrium 光致发光性能 共沉淀工艺 纳米颗粒 表征 钇铝石榴石 |
| Title | Low-temperature solution synthesis and characterization of Ce-doped YAG nanoparticles |
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