Preparation of SiO2 coated Ce2S3 red pigment with improved thermal stability
SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction （XRD）, scanning electron microscopy （SEM）, energy dispersive spectroscopy （EDX）, UV-visible spectro-photometer and automatic colorimeter were used to investigat...
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| Published in | Journal of rare earths Vol. 31; no. 9; pp. 891 - 896 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.09.2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60375-5 |
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| Abstract | SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction （XRD）, scanning electron microscopy （SEM）, energy dispersive spectroscopy （EDX）, UV-visible spectro-photometer and automatic colorimeter were used to investigate the properties of the samples. The results showed that the compact SiO2 film formed on the surface of Ce2S3 pigment at a cerium silicon molar ratio of 2. The thermal stability temperature of Ce2S3 pigment was improved to 450 oC after SiO2 coating. In addition, the color of Ce2S3 pigment was not affected significantly through coating colorless and transparent SiO2 and it could be used as safe red pigment in higher temperature fields. |
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| AbstractList | SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction （XRD）, scanning electron microscopy （SEM）, energy dispersive spectroscopy （EDX）, UV-visible spectro-photometer and automatic colorimeter were used to investigate the properties of the samples. The results showed that the compact SiO2 film formed on the surface of Ce2S3 pigment at a cerium silicon molar ratio of 2. The thermal stability temperature of Ce2S3 pigment was improved to 450 oC after SiO2 coating. In addition, the color of Ce2S3 pigment was not affected significantly through coating colorless and transparent SiO2 and it could be used as safe red pigment in higher temperature fields. SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDX), UV-visible spectrophotometer and automatic colorimeter were used to investigate the properties of the samples. The results showed that the compact SiO2 film formed on the surface of Ce2S3 pigment at a cerium silicon molar ratio of 2. The thermal stability temperature of Ce2S3 pigment was improved to 450 °C after SiO2 coating. In addition, the color of Ce2S3 pigment was not affected significantly through coating colorless and transparent SiO2 and it could be used as safe red pigment in higher temperature fields. SEM image and UV-visible absorption spectrum of Ce2S3 and SiO2 coated Ce2S3 pigment SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDX), UV-visible spectrophotometer and automatic colorimeter were used to investigate the properties of the samples. The results showed that the compact SiO2 film formed on the surface of Ce2S3 pigment at a cerium silicon molar ratio of 2. The thermal stability temperature of Ce2S3 pigment was improved to 450 degree C after SiO2 coating. In addition, the color of Ce2S3 pigment was not affected significantly through coating colorless and transparent SiO2 and it could be used as safe red pigment in higher temperature fields. |
| Author | 陈观宏 朱振峰 刘辉 武英峰 朱春奎 |
| AuthorAffiliation | School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi ＇an 710021, China |
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| Cites_doi | 10.1016/S1002-0721(12)60251-8 10.1006/jssc.1996.7185 10.1016/j.corsci.2010.09.012 10.1016/0925-8388(94)07095-4 10.1016/0021-9797(68)90272-5 10.1016/0925-8388(94)01476-0 10.1016/S0925-8388(97)00039-X 10.1107/S0567739476001551 10.1016/S1002-0721(08)60239-2 10.1016/S0925-8388(97)00580-X 10.1016/S0925-8388(98)00006-1 10.1103/PhysRevB.54.2428 10.1021/ja0392521 10.1016/0925-8388(94)05058-9 10.1016/S1002-0721(12)60272-5 |
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| Keywords | cerium silicon molar ratio red pigment thermal stability Ce2S3 SiO2 coating rare earths |
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| Notes | 11-2788/TF CHEN Guanhong , ZHU Zhenfeng, LIU Hui , WU Yingfeng , ZHU Chunkui （School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi ＇an 710021, China） Ce2S3; red pigment; SiO2 coating; cerium silicon molar ratio; thermal stability; rare earths SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction （XRD）, scanning electron microscopy （SEM）, energy dispersive spectroscopy （EDX）, UV-visible spectro-photometer and automatic colorimeter were used to investigate the properties of the samples. The results showed that the compact SiO2 film formed on the surface of Ce2S3 pigment at a cerium silicon molar ratio of 2. The thermal stability temperature of Ce2S3 pigment was improved to 450 oC after SiO2 coating. In addition, the color of Ce2S3 pigment was not affected significantly through coating colorless and transparent SiO2 and it could be used as safe red pigment in higher temperature fields. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| Snippet | SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction （XRD）, scanning... SiO2 coated Ce2S3 red pigment was prepared in ethanol/H2O system via sol-gel method and TEOS were used as silica sources. X-ray diffraction (XRD), scanning... |
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| SubjectTerms | Ce2S3 cerium silicon molar ratio Coating Ethyl alcohol Pigments Rare earth metals rare earths red pigment Red pigments Scanning electron microscopy Silicon dioxide SiO2 coating SiO2涂层 Thermal stability X-射线衍射仪 二氧化硅涂层 制备 可见分光光度计 扫描电子显微镜 热稳定性 红色颜料 |
| Title | Preparation of SiO2 coated Ce2S3 red pigment with improved thermal stability |
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