Characterization of Pyrolytic Lignin Extracted from Bio-oil
Bio-oil is a new liquid fuel produced by fast pyrolysis,which is a promising technology to convert bio-mass into liquid. Pyrolytic lignin extracted from bio-oil,a fine powder,contributes to the instability of bio-oil. The paper presents the structural features of three kinds of pyrolytic lignin extr...
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| Published in | Chinese journal of chemical engineering Vol. 18; no. 6; pp. 1018 - 1022 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.12.2010
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1004-9541 2210-321X |
| DOI | 10.1016/S1004-9541(09)60162-2 |
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| Abstract | Bio-oil is a new liquid fuel produced by fast pyrolysis,which is a promising technology to convert bio-mass into liquid. Pyrolytic lignin extracted from bio-oil,a fine powder,contributes to the instability of bio-oil. The paper presents the structural features of three kinds of pyrolytic lignin extracted from bio-oil with different methods（WIF,HMM,and LMM） . The pyrolytic lignin samples are characterized by Fourier transform infrared spectrometer（FTIR） and X-ray photoelectron spectroscopy（XPS） . FTIR data indicate that the three pyrolytic lignin samples have similar functional groups,while the absorption intensity is different,and show characteristic vibra-tions of typical lignocellulosic material groups O H（3340-3380 cm-1） ,C H（2912-2929 cm-1） and C O（1652-1725 cm-1） . Comparison in the region（3340-3380 cm-1） indicates that WIF has more O H stretch groups than HMM and LMM. The carbon spectra are fitted to four peaks：C1,C C or C H,BE 283.5 eV;C2,C OR or C OH,BE 284.5-285.8 eV;C3,C O or HO C OR,BE 286.10-287.10 eV;C4,O C O,BE 287.5-287.7 eV. The absence of C1,C C or C H indicates the dominant polymerization structure of aro-matic carbon in pyrolytic lignin samples. For HMM and WIF,C2a and C2b can not be separated,so there is no free hydroxyl group in the samples. The oxygen peaks are also fitted to four peaks：O1,OH,BE = 530.3 eV;O2,RC O,BE 531.45-531.72 eV;O3,O C O,BE = 532.73-533.74 eV;O4,H2O,BE 535 eV. The absence of O1 and O4 indicates that little hydroxyl groups and adsorbed water are present in the samples. |
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| AbstractList | Bio-oil is a new liquid fuel produced by fast pyrolysis, which is a promising technology to convert biomass into liquid. Pyrolytic lignin extracted from bio-oil, a fine powder, contributes to the instability of bio-oil. The paper presents the structural features of three kinds of pyrolytic lignin extracted from bio-oil with different methods (WIF, HMM, and LMM). The pyrolytic lignin samples are characterized by Fourier transform infrared spectrometer (FTIR) and X-ray photoelectron spectroscopy (XPS). FTIR data indicate that the three pyrolytic lignin samples have similar functional groups, while the absorption intensity is different, and show characteristic vibrations of typical lignocellulosic material groups OH (3340-3380 cm super(-1)), CH (2912-2929 cm super(-1)) and CO (1652-1725 cm super(-1)). Comparison in the region (3340-3380 cm super(-1)) indicates that WIF has more OH stretch groups than HMM and LMM. The carbon spectra are fitted to four peaks: C1, CC or CH, BE = 283.5 eV; C2, COR or COH, BE = 284.5-285.8 eV; C3, CO or HOCOR, BE = 286.10-287.10 eV; C4, OCO, BE = 287.5-287.7 eV. The absence of C1, CC or CH indicates the dominant polymerization structure of aromatic carbon in pyrolytic lignin samples. For HMM and WIF, C2a and C2b can not be separated, so there is no free hydroxyl group in the samples. The oxygen peaks are also fitted to four peaks: O1, OH, BE = 530.3 eV; O2, RCO, BE = 531.45-531.72 eV; O3, OCO, BE = 532.73-533.74 eV; O4, H sub(2)O, BE = 535 eV. The absence of O1 and O4 indicates that little hydroxyl groups and adsorbed water are present in the samples. Bio-oil is a new liquid fuel produced by fast pyrolysis,which is a promising technology to convert bio-mass into liquid. Pyrolytic lignin extracted from bio-oil,a fine powder,contributes to the instability of bio-oil. The paper presents the structural features of three kinds of pyrolytic lignin extracted from bio-oil with different methods（WIF,HMM,and LMM） . The pyrolytic lignin samples are characterized by Fourier transform infrared spectrometer（FTIR） and X-ray photoelectron spectroscopy（XPS） . FTIR data indicate that the three pyrolytic lignin samples have similar functional groups,while the absorption intensity is different,and show characteristic vibra-tions of typical lignocellulosic material groups O H（3340-3380 cm-1） ,C H（2912-2929 cm-1） and C O（1652-1725 cm-1） . Comparison in the region（3340-3380 cm-1） indicates that WIF has more O H stretch groups than HMM and LMM. The carbon spectra are fitted to four peaks：C1,C C or C H,BE 283.5 eV;C2,C OR or C OH,BE 284.5-285.8 eV;C3,C O or HO C OR,BE 286.10-287.10 eV;C4,O C O,BE 287.5-287.7 eV. The absence of C1,C C or C H indicates the dominant polymerization structure of aro-matic carbon in pyrolytic lignin samples. For HMM and WIF,C2a and C2b can not be separated,so there is no free hydroxyl group in the samples. The oxygen peaks are also fitted to four peaks：O1,OH,BE = 530.3 eV;O2,RC O,BE 531.45-531.72 eV;O3,O C O,BE = 532.73-533.74 eV;O4,H2O,BE 535 eV. The absence of O1 and O4 indicates that little hydroxyl groups and adsorbed water are present in the samples. Bio-oil is a new liquid fuel produced by fast pyrolysis, which is a promising technology to convert biomass into liquid. Pyrolytic lignin extracted from bio-oil, a fine powder, contributes to the instability of bio-oil. The paper presents the structural features of three kinds of pyrolytic lignin extracted from bio-oil with different methods (WIF, HMM, and LMM). The pyrolytic lignin samples are characterized by Fourier transform infrared spectrometer (FTIR) and X-ray photoelectron spectroscopy (XPS). FTIR data indicate that the three pyrolytic lignin samples have similar functional groups, while the absorption intensity is different, and show characteristic vibrations of typical lignocellulosic material groups OH (3340–3380 cm −1), CH (2912–2929 cm −1) and CO (1652–1725 cm −1). Comparison in the region (3340–3380 cm −1) indicates that WIF has more OH stretch groups than HMM and LMM. The carbon spectra are fitted to four peaks: C1, CC or CH, BE = 283.5 eV; C2, COR or COH, BE = 284.5–285.8 eV; C3, CO or HOCOR, BE = 286.10–287.10 eV; C4, OCO, BE = 287.5–287.7 eV. The absence of C1, CC or CH indicates the dominant polymerization structure of aromatic carbon in pyrolytic lignin samples. For HMM and WIF, C2a and C2b can not be separated, so there is no free hydroxyl group in the samples. The oxygen peaks are also fitted to four peaks: O1, OH, BE = 530.3 eV; O2, RCO, BE = 531.45–531.72 eV; O3, OCO, BE = 532.73–533.74 eV; O4, H 2O, BE = 535 eV. The absence of O1 and O4 indicates that little hydroxyl groups and adsorbed water are present in the samples. |
| Author | JIANG Xiaoxiang Naoko Ellis ZHONG Zhaoping |
| AuthorAffiliation | Thermoenergy Engineering Research Institute, Southeast University, Nanjing 210096, China Department of Chemical and Biological Engineering, University of British Columbia, Vancouver, Canada |
| Author_xml | – sequence: 1 givenname: Xiaoxiang surname: JIANG fullname: JIANG, Xiaoxiang organization: Thermoenergy Engineering Research Institute, Southeast University, Nanjing 210096, China – sequence: 2 givenname: Naoko surname: Ellis fullname: Ellis, Naoko organization: Department of Chemical and Biological Engineering, University of British Columbia, Vancouver, Canada – sequence: 3 givenname: Zhaoping surname: ZHONG fullname: ZHONG, Zhaoping email: zzhong@seu.edu.cn organization: Thermoenergy Engineering Research Institute, Southeast University, Nanjing 210096, China |
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| Keywords | pyrolytic lignin Fourier transform infrared spectrometer bio-oil X-ray photoelectron spectroscopy |
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| Title | Characterization of Pyrolytic Lignin Extracted from Bio-oil |
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