A 4d-4f heterometallic coordination polymer： Synthesis, crystal structure and near-infrared luminescent properties
A 4d-4f heterometallic coordination polymer, [AgNd（pydc）2].2H2O （1） （H2pydc=pyridine-3,4-dicarboxylic acid）, was synthesized under hydrothermal conditions, and fimher characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray dif- fraction. Complex 1 featured a thre...
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| Published in | Journal of rare earths Vol. 30; no. 7; pp. 716 - 720 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.07.2012
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| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60117-3 |
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| Abstract | A 4d-4f heterometallic coordination polymer, [AgNd（pydc）2].2H2O （1） （H2pydc=pyridine-3,4-dicarboxylic acid）, was synthesized under hydrothermal conditions, and fimher characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray dif- fraction. Complex 1 featured a three-dimensional （3D） framework containing one-dimensional （1D） channels occupied by free water molecules, which was constructed from 1D inorganic heterometallic chains and linear pydc linkers. To our knowledge, complex 1 represented a rare example of 3D open-framework 4d-4f heterometallic coordination polymer. After removal of the water molecules fi＇om complex 1, the remaining material had high thermal stability. Moreover, the near-infrared luminescent properties of 1 were also investigated in the solid state. |
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| AbstractList | A 4d-4f heterometallic coordination polymer, [AgNd（pydc）2].2H2O （1） （H2pydc=pyridine-3,4-dicarboxylic acid）, was synthesized under hydrothermal conditions, and fimher characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray dif- fraction. Complex 1 featured a three-dimensional （3D） framework containing one-dimensional （1D） channels occupied by free water molecules, which was constructed from 1D inorganic heterometallic chains and linear pydc linkers. To our knowledge, complex 1 represented a rare example of 3D open-framework 4d-4f heterometallic coordination polymer. After removal of the water molecules fi＇om complex 1, the remaining material had high thermal stability. Moreover, the near-infrared luminescent properties of 1 were also investigated in the solid state. A 4d-4f heterometallic coordination polymer, [AgNd(pydc)2]ADT2H2O (1) (H2pydc=pyridine-3,4-dicarboxylic acid), was synthesized under hydrothermal conditions, and further characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray diffraction. Complex 1 featured a three-dimensional (3D) framework containing one-dimensional (1D) channels occupied by free water molecules, which was constructed from 1D inorganic heterometallic chains and linear pydc linkers. To our knowledge, complex 1 represented a rare example of 3D open-framework 4d-4f heterometallic coordination polymer. After removal of the water molecules from complex 1, the remaining material had high thermal stability. Moreover, the near-infrared luminescent properties of 1 were also investigated in the solid state. A 4d-4f heterometallic coordination polymer, [AgNd(pydc)2]·2H2O (1) (H2pydc=pyridine-3,4-dicarboxylic acid), was synthesized under hydrothermal conditions, and further characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray diffraction. Complex 1 featured a three-dimensional (3D) framework containing one-dimensional (1D) channels occupied by free water molecules, which was constructed from 1D inorganic heterometallic chains and linear pydc linkers. To our knowledge, complex 1 represented a rare example of 3D open-framework 4d-4f heterometallic coordination polymer. After removal of the water molecules from complex 1, the remaining material had high thermal stability. Moreover, the near-infrared luminescent properties of 1 were also investigated in the solid state. |
| Author | 刘光祥 |
| AuthorAffiliation | School of Biochemical and Environmental Engineering, Nanjing Xiaozhuang University; Nanjing 211171, China |
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| Keywords | pyridine-3,4-dicarboxylic acid crystal structure Heterometallic coordination polymer near-infrared luminescence rare earths |
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| Notes | 11-2788/TF Heterometallic coordination polymer; pyridine-3,4-dicarboxylic acid; crystal structure; near-infrared luminescence; rare earths LIU Guangxiang （School of Biochemical and Environmental Engineering, Nanjing Xiaozhuang University, Nanjing 211171, China） A 4d-4f heterometallic coordination polymer, [AgNd（pydc）2].2H2O （1） （H2pydc=pyridine-3,4-dicarboxylic acid）, was synthesized under hydrothermal conditions, and fimher characterized by elemental analysis, IR, thermogravimetric analysis and single-crystal X-ray dif- fraction. Complex 1 featured a three-dimensional （3D） framework containing one-dimensional （1D） channels occupied by free water molecules, which was constructed from 1D inorganic heterometallic chains and linear pydc linkers. To our knowledge, complex 1 represented a rare example of 3D open-framework 4d-4f heterometallic coordination polymer. After removal of the water molecules fi＇om complex 1, the remaining material had high thermal stability. Moreover, the near-infrared luminescent properties of 1 were also investigated in the solid state. ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| Snippet | A 4d-4f heterometallic coordination polymer, [AgNd（pydc）2].2H2O （1） （H2pydc=pyridine-3,4-dicarboxylic acid）, was synthesized under hydrothermal... A 4d-4f heterometallic coordination polymer, [AgNd(pydc)2]·2H2O (1) (H2pydc=pyridine-3,4-dicarboxylic acid), was synthesized under hydrothermal conditions, and... A 4d-4f heterometallic coordination polymer, [AgNd(pydc)2]ADT2H2O (1) (H2pydc=pyridine-3,4-dicarboxylic acid), was synthesized under hydrothermal conditions,... |
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| SubjectTerms | Channels Coordination polymers Crystal structure Diffraction Heterometallic coordination polymer Infrared radiation near-infrared luminescence pyridine-3,4-dicarboxylic acid Rare earth metals rare earths Three dimensional X-rays 元素分析 单晶X-射线衍射 发光性能 合成 异金属配位聚合物 晶体结构 水热条件 近红外 |
| Title | A 4d-4f heterometallic coordination polymer： Synthesis, crystal structure and near-infrared luminescent properties |
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