Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod

One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.elect...

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Published inChinese journal of chemical engineering Vol. 20; no. 1; pp. 89 - 94
Main Author 宁张磊 常志东 李文军 孙长艳 张经华 刘洋
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.02.2012
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ISSN1004-9541
2210-321X
DOI10.1016/S1004-9541(12)60367-X

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Abstract One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed.
AbstractList One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed.
One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (FT-IR), cold field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samples showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed.
Author 宁张磊 常志东 李文军 孙长艳 张经华 刘洋
AuthorAffiliation School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China
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Keywords strontium hydroxyapatite
optical performance
biomaterial
solvothermal synthesis
Language English
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Notes strontium hydroxyapatite, biomaterial, solvotherrnal synthesis, optical performance
NING Zhanglei , CHANG Zhidong , LI Wenjun, SUN Changyan, ZHANG Jinghua LIU Yang School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China 2 Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China
One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed.
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SSID ssj0020818
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Snippet One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via...
One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via...
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SubjectTerms biomaterial
Confining
Excitation
Hydroxyapatite
Nanocomposites
Nanomaterials
Nanostructure
optical performance
Scanning electron microscopy
solvothermal synthesis
Strontium
strontium hydroxyapatite
一维
光学性能
溶剂热合成
电子显微镜
紫外光激发
纳米棒
羟基磷灰石

Title Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod
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