Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod
One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.elect...
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Published in | Chinese journal of chemical engineering Vol. 20; no. 1; pp. 89 - 94 |
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Format | Journal Article |
Language | English |
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Elsevier B.V
01.02.2012
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ISSN | 1004-9541 2210-321X |
DOI | 10.1016/S1004-9541(12)60367-X |
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Abstract | One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed. |
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AbstractList | One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed. One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (FT-IR), cold field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samples showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed. |
Author | 宁张磊 常志东 李文军 孙长艳 张经华 刘洋 |
AuthorAffiliation | School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China |
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Notes | strontium hydroxyapatite, biomaterial, solvotherrnal synthesis, optical performance NING Zhanglei , CHANG Zhidong , LI Wenjun, SUN Changyan, ZHANG Jinghua LIU Yang School of Chemical and Biological Engineering, University of Science and Technology Beijing, Beijing 100083, China 2 Beijing Centre for Physical & Chemical Analysis, Beijing 100089, China One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via X-ray diffraction (XRD), Fourier transform infrared (.FT-IR), .cold field emission.sc.anning.elec.tron microscopy_.(FESEM), transmission.electron microscopy (TEM),photoluminescence (PL) excitation and emission spectra. The experimental results indicated that oleic acid as a surfactant played a key role in confining the growth of the Sr-HAp powders. A possible formation mechanism of the one-dimensional nanorod was proposed and elaborated. Moreover, the as-obtained Sr-HAp samoles showed an intense and bright emission band centered at 460 nm under long-wavelength UV light excitation and the contents of NaOH used in the synthetic process had an obvious impact on the optical performance of Sr-HAp powders. The possible luminescent mechanism of the Sr-HAp samples was discussed. 11-3270/TQ ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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Snippet | One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via... One-dimensional strontium hydroxyapatite (Sr-HAp) nanorods were successfully synthesized by a simple solvothermal method. The products were characterized via... |
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SubjectTerms | biomaterial Confining Excitation Hydroxyapatite Nanocomposites Nanomaterials Nanostructure optical performance Scanning electron microscopy solvothermal synthesis Strontium strontium hydroxyapatite 一维 光学性能 溶剂热合成 电子显微镜 紫外光激发 纳米棒 羟基磷灰石 锶 |
Title | Solvothermal Synthesis and Optical Performance of One-dimensional Strontium Hydroxyapatite Nanorod |
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