Electrocatalytic Activity of Tungsten Carbide and Natural Zeolite Composite in Aqueous Solution
Tungsten carbide and zeolite nanocomposite was prepared by combining a mechanochemical approach with a reduction and carbonization approach,using natural zeolite and ammonia metatungstate as precursors.The sample was characterized by X-ray diffraction and scanning electron microscope.The results sho...
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| Published in | Chinese journal of chemical engineering Vol. 20; no. 2; pp. 254 - 261 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.04.2012
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1004-9541 2210-321X |
| DOI | 10.1016/S1004-9541(12)60386-3 |
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| Abstract | Tungsten carbide and zeolite nanocomposite was prepared by combining a mechanochemical approach with a reduction and carbonization approach,using natural zeolite and ammonia metatungstate as precursors.The sample was characterized by X-ray diffraction and scanning electron microscope.The results showed that the crystal phase of the sample is composed of zeolite,monotungsten carbide and bitungsten carbide.The mass percentage and the crystallite diameter of tungsten carbide change along with the reacted time.Its electrocatalytic activity was measured with a microelectrode system with three electrodes.The results show that its electrocatalytic property is related to its crystal phase and the mass percentage of tungsten carbide,and its electrocatalytic activity is connected with the property of electrolyte,in which it is measured.Synergistic effect between tungsten carbide and zeolite is found during electrocatalysis. |
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| AbstractList | Tungsten carbide and zeolite nanocomposite was prepared by combining a mechanochemical approach with a reduction and carbonization approach, using natural zeolite and ammonia metatungstate as precursors. The sample was characterized by X-ray diffraction and scanning electron microscope. The results showed that the crystal phase of the sample is composed of zeolite, monotungsten carbide and bitungsten carbide. The mass percentage and the crystallite diameter of tungsten carbide change along with the reacted time. Its electrocatalytic activity was measured with a microelectrode system with three electrodes. The results show that its electrocatalytic property is related to its crystal phase and the mass percentage of tungsten carbide, and its electrocatalytic activity is connected with the property of electrolyte, in which it is measured. Synergistic effect between tungsten carbide and zeolite is found during electrocatalysis. |
| Author | 程媛 谢伟淼 姚国新 胡素绢 李国华 |
| AuthorAffiliation | School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032, China State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, Hangzhou 310032, China Research Center of Nanoscience and Technology, Zhejiang University of Technology, Hangzhou 310032, China |
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| Cites_doi | 10.1039/b202518c 10.1126/science.181.4099.547 10.1016/j.jcat.2004.07.015 10.1149/1.1836953 10.1016/j.micromeso.2005.06.033 10.1039/b205294f 10.1016/S0926-860X(01)00756-6 10.1016/0013-4686(77)85025-1 10.1016/0013-4686(77)80050-9 10.1002/anie.197101941 10.1016/S0920-5861(00)00556-3 |
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| Keywords | nanocomposite zeolite electrocatalytic activity tungsten carbide synergistic effect |
| Language | English |
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| Notes | CHENG Yuan , XIE Weimiao , YAO Guoxin , HU Sujuan , LI Guohua （ School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032, China 2 State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, Hangzhou 310032, China 3 Research Center of Nanoscience and Technology, Zhejia-ng University of Technology, Hangzhou 310032, China） tungsten carbide, zeolite, nanocomposite, electrocatalytic activity, synergistic effect 11-3270/TQ Tungsten carbide and zeolite nanocomposite was prepared by combining a mechanochemical approach with a reduction and carbonization approach,using natural zeolite and ammonia metatungstate as precursors.The sample was characterized by X-ray diffraction and scanning electron microscope.The results showed that the crystal phase of the sample is composed of zeolite,monotungsten carbide and bitungsten carbide.The mass percentage and the crystallite diameter of tungsten carbide change along with the reacted time.Its electrocatalytic activity was measured with a microelectrode system with three electrodes.The results show that its electrocatalytic property is related to its crystal phase and the mass percentage of tungsten carbide,and its electrocatalytic activity is connected with the property of electrolyte,in which it is measured.Synergistic effect between tungsten carbide and zeolite is found during electrocatalysis. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| SubjectTerms | Carbides Crystals Electrocatalysis electrocatalytic activity Electrodes nanocomposite Nanostructure Scanning electron microscopy synergistic effect Tungsten carbide zeolite Zeolites 力化学方法 天然沸石 扫描电子显微镜 水溶液 电催化活性 电极系统 碳化钨 纳米复合材料 |
| Title | Electrocatalytic Activity of Tungsten Carbide and Natural Zeolite Composite in Aqueous Solution |
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