Structure-property relationship in fully biobased epoxidized soybean oil thermosets cured by dicarboxyl terminated polyamide 1010 oligomer with different carboxyl/epoxy ratios
Dicarboxyl terminated polyamide 1010 oligomer was used to cure epoxidized soybean oil (ESO) to synthesize fully biobased epoxy thermosets with different chemical structures via changing carboxyl/epoxy equivalent ratio (R-value). The effect of chemical structures of the epoxy thermosets on their cros...
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| Published in | Polymer testing Vol. 79; p. 106057 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2019
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0142-9418 1873-2348 |
| DOI | 10.1016/j.polymertesting.2019.106057 |
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| Abstract | Dicarboxyl terminated polyamide 1010 oligomer was used to cure epoxidized soybean oil (ESO) to synthesize fully biobased epoxy thermosets with different chemical structures via changing carboxyl/epoxy equivalent ratio (R-value). The effect of chemical structures of the epoxy thermosets on their crosslink density, swelling property, crystallization behavior, dynamic and static mechanical properties, as well as thermal stability was studied systematically. The crosslink density of the epoxy thermosets increased obviously, the gel fraction almost kept unchanged, and the swelling ratio decreased gradually with increasing R-value. The crystallization capability and degree of crystallinity were enhanced meanwhile melting temperature shifted to higher temperature range with increasing R-value, due to the increased concentration of polyamide 1010 segments in the thermoset. Consequently, the stiffness and heat resistance of the epoxy thermosets were enhanced. The Young's modulus increased gradually and the break stress as well as the break strain first increased and then decreased with increasing R-value. This investigation provides a new strategy to regulate physical properties of soybean oil-based epoxy thermosets, which would be valuable for other plant oil-based polymers design.
•Fully biobased epoxy thermosets were prepared by curing epoxidized soybean oil with dicarboxyl terminated polyamide 1010 oligomer.•The chemical structure and crosslink density of the epoxy thermosets were regulated by carboxyl/epoxy equivalent ratio.•The crystallization and Young's modulus of the epoxy thermosets were enhanced with increasing carboxyl/epoxy equivalent ratio.•The break strength and elongation at break first increased and then decreased with increasing carboxyl/epoxy equivalent ratio.•The fully biobased epoxy thermosets showed good thermal stability. |
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| AbstractList | Dicarboxyl terminated polyamide 1010 oligomer was used to cure epoxidized soybean oil (ESO) to synthesize fully biobased epoxy thermosets with different chemical structures via changing carboxyl/epoxy equivalent ratio (R-value). The effect of chemical structures of the epoxy thermosets on their crosslink density, swelling property, crystallization behavior, dynamic and static mechanical properties, as well as thermal stability was studied systematically. The crosslink density of the epoxy thermosets increased obviously, the gel fraction almost kept unchanged, and the swelling ratio decreased gradually with increasing R-value. The crystallization capability and degree of crystallinity were enhanced meanwhile melting temperature shifted to higher temperature range with increasing R-value, due to the increased concentration of polyamide 1010 segments in the thermoset. Consequently, the stiffness and heat resistance of the epoxy thermosets were enhanced. The Young's modulus increased gradually and the break stress as well as the break strain first increased and then decreased with increasing R-value. This investigation provides a new strategy to regulate physical properties of soybean oil-based epoxy thermosets, which would be valuable for other plant oil-based polymers design.
•Fully biobased epoxy thermosets were prepared by curing epoxidized soybean oil with dicarboxyl terminated polyamide 1010 oligomer.•The chemical structure and crosslink density of the epoxy thermosets were regulated by carboxyl/epoxy equivalent ratio.•The crystallization and Young's modulus of the epoxy thermosets were enhanced with increasing carboxyl/epoxy equivalent ratio.•The break strength and elongation at break first increased and then decreased with increasing carboxyl/epoxy equivalent ratio.•The fully biobased epoxy thermosets showed good thermal stability. |
| ArticleNumber | 106057 |
| Author | Weng, Yun-Xuan He, Jia Zeng, Jian-Bing Wang, Xiang-Zhao Li, Yi-Dong |
| Author_xml | – sequence: 1 givenname: Xiang-Zhao surname: Wang fullname: Wang, Xiang-Zhao organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University, Chongqing, 400715, China – sequence: 2 givenname: Jia surname: He fullname: He, Jia organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University, Chongqing, 400715, China – sequence: 3 givenname: Yun-Xuan surname: Weng fullname: Weng, Yun-Xuan email: wyxuan@th.btbu.edu.cn organization: Beijing Key Laboratory of Quality Evaluation Technology for Hygiene and Safety of Plastics, Beijing Technology and Business University, Beijing, 100048, China – sequence: 4 givenname: Jian-Bing surname: Zeng fullname: Zeng, Jian-Bing organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University, Chongqing, 400715, China – sequence: 5 givenname: Yi-Dong surname: Li fullname: Li, Yi-Dong email: liyidong@swu.edu.cn organization: Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing, School of Chemistry and Chemical Engineering, Southwest University, Chongqing, 400715, China |
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| Keywords | Biobased polyamide Epoxidized soybean oil Crosslink density Mechanical property Crystallization |
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| Title | Structure-property relationship in fully biobased epoxidized soybean oil thermosets cured by dicarboxyl terminated polyamide 1010 oligomer with different carboxyl/epoxy ratios |
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