Direct Synthesis of Diphenyl Carbonate with Heterogeneous Catalyst and Optimal Synthesis Conditions of the Support Prepared by Sol-gel Method
The support of catalyst for the direct synthesis of diphenyl carbonate （DPC） by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared with activated charcoal, molecular sieve, porous ceramics, hopcalite, the support prepared by the sol-gel method has higher activity. The char...
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| Published in | Chinese journal of chemical engineering Vol. 16; no. 2; pp. 223 - 227 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.04.2008
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1004-9541 2210-321X |
| DOI | 10.1016/S1004-9541(08)60067-1 |
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| Abstract | The support of catalyst for the direct synthesis of diphenyl carbonate （DPC） by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared with activated charcoal, molecular sieve, porous ceramics, hopcalite, the support prepared by the sol-gel method has higher activity. The characterization of the support by X-ray diffraction （XRD） and transmission electron microscope （TEM） show that the mare crystal phase is Co2MnO4 and the average particle diameter is about 40 nm. The optimum conditions for synthesis of the support were determined by orthogonal experiments, which indicate that the proportion of Cu, Mn, and Co is the first important factor influencing the yield and selectivity of DPC. Temperature of calcination is the second one. The optimum conditions are： molar proportion of Cu, Mn, and Co being 1 ： 1 ： 1, temperature of calcination 700℃, drying at 100~C, temperature of water bath 85~C. The yield and selectivity of DPC in the process can reach 38% and 99% in the batch operation, respectively. The copper cobalt manganese mixed oxides chosen as the support contribute more to the high catalytic activity than the sol-gel method. |
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| AbstractList | The support of catalyst for the direct synthesis of diphenyl carbonate (DPC) by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared with activated charcoal, molecular sieve, porous ceramics, hopcalite, the support prepared by the sol-gel method has higher activity. The characterization of the support by X-ray diffraction (XRD) and transmission electron microscope (TEM) show that the main crystal phase is Co
2MnO
4 and the average particle diameter is about 40 nm. The optimum conditions for synthesis of the support were determined by orthogonal experiments, which indicate that the proportion of Cu, Mn, and Co is the first important factor influencing the yield and selectivity of DPC. Temperature of calcination is the second one. The optimum conditions are: molar proportion of Cu, Mn, and Co being 1:1:1, temperature of calcination 700°C, drying at 100°C, temperature of water bath 85°C. The yield and selectivity of DPC in the process can reach 38% and 99% in the batch operation, respectively. The copper cobalt manganese mixed oxides chosen as the support contribute more to the high catalytic activity than the sol-gel method. The support of catalyst for the direct synthesis of diphenyl carbonate (DPC) by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared with activated charcoal, molecular sieve, porous ceramics, hopcalite, the support prepared by the sol-gel method has higher activity. The characterization of the support by X-ray diffraction (XRD) and transmission electron microscope (TEM) show that the main crystal phase is Co2MnO4 and the average particle diameter is about 40 nm. The optimum conditions for synthesis of the support were determined by orthogonal experiments, which indicate that the proportion of Cu, Mn, and Co is the first important factor influencing the yield and selectivity of DPC. Temperature of calcination is the second one. The optimum conditions are: molar proportion of Cu, Mn, and Co being 1:1:1, temperature of calcination 700 deg C, drying at 100 deg C, temperature of water bath 85 deg C. The yield and selectivity of DPC in the process can reach 38% and 99% in the batch operation, respectively. The copper cobalt manganese mixed oxides chosen as the support contribute more to the high catalytic activity than the sol-gel method. The support of catalyst for the direct synthesis of diphenyl carbonate （DPC） by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared with activated charcoal, molecular sieve, porous ceramics, hopcalite, the support prepared by the sol-gel method has higher activity. The characterization of the support by X-ray diffraction （XRD） and transmission electron microscope （TEM） show that the mare crystal phase is Co2MnO4 and the average particle diameter is about 40 nm. The optimum conditions for synthesis of the support were determined by orthogonal experiments, which indicate that the proportion of Cu, Mn, and Co is the first important factor influencing the yield and selectivity of DPC. Temperature of calcination is the second one. The optimum conditions are： molar proportion of Cu, Mn, and Co being 1 ： 1 ： 1, temperature of calcination 700℃, drying at 100~C, temperature of water bath 85~C. The yield and selectivity of DPC in the process can reach 38% and 99% in the batch operation, respectively. The copper cobalt manganese mixed oxides chosen as the support contribute more to the high catalytic activity than the sol-gel method. |
| Author | 郭红霞 陈红萍 梁英华 芮玉兰 吕敬德 付占达 |
| AuthorAffiliation | School of Chemical Engineering and Biological Technology, Hebei Polytechnic University, Tangshan 063009, China |
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| Cites_doi | 10.1016/S1381-1169(97)00188-X 10.1016/S1381-1169(99)00005-9 10.1023/A:1019075805134 10.1016/j.cattod.2005.06.023 10.1016/S1381-1169(98)00238-6 10.1016/S1381-1169(03)00281-4 10.1016/S1381-1169(99)00392-1 10.1016/S1381-1169(98)00122-8 10.1016/j.molcata.2005.01.026 |
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A Chem. doi: 10.1016/j.molcata.2005.01.026 – ident: 10.1016/S1004-9541(08)60067-1_bib21 – volume: 137 start-page: 147 year: 1999 ident: 10.1016/S1004-9541(08)60067-1_bib1 article-title: “Direct synthesis of diphenyl carbonate by oxidative carbonylation of phenol using Pd-Cu based redox catalyst” publication-title: J. Mol. Cat. A Chem. doi: 10.1016/S1381-1169(98)00122-8 – volume: 34 start-page: 47 issue: 1 year: 2002 ident: 10.1016/S1004-9541(08)60067-1_bib6 article-title: “Oxidative carbonylation of phenol to diphenyl carbonate over palladium complexes catalysts” publication-title: J. Sichuan Univ. |
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| Snippet | The support of catalyst for the direct synthesis of diphenyl carbonate （DPC） by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared... The support of catalyst for the direct synthesis of diphenyl carbonate (DPC) by heterogeneous catalytic reaction was prepared by the sol-gel method. Compared... |
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| SubjectTerms | diphenyl carbonate heterogeneous catalyst optimum condition sol-gel method 催化剂 溶胶凝胶法 碳酸二苯酯 非均相催化 |
| Title | Direct Synthesis of Diphenyl Carbonate with Heterogeneous Catalyst and Optimal Synthesis Conditions of the Support Prepared by Sol-gel Method |
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