INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY FOR THE DETERMINATION OF 237Np IN SPENT NUCLEAR FUEL SAMPLES BY ISOTOPE DILUTION METHOD USING 239Np AS A SPIKE
A determination method for 237Np in spent nuclear fuel samples was developed using an isotope dilution method with 239Np as a spike. In this method, inductively coupled plasma mass spectrometry (ICP-MS) was taken for the 237Np instead of the previously used alpha spectrometry. 237Np and 239Np were m...
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| Published in | Nuclear engineering and technology Vol. 45; no. 3; pp. 415 - 420 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.06.2013
Elsevier 한국원자력학회 |
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| Online Access | Get full text |
| ISSN | 1738-5733 2234-358X |
| DOI | 10.5516/NET.06.2012.056 |
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| Abstract | A determination method for 237Np in spent nuclear fuel samples was developed using an isotope dilution method with 239Np as a spike. In this method, inductively coupled plasma mass spectrometry (ICP-MS) was taken for the 237Np instead of the previously used alpha spectrometry. 237Np and 239Np were measured by ICP-MS and gamma spectrometry, respectively. The recovery yield of 237Np in synthetic samples was 95.9±9.7% (1S, n=4). The 237Np contents in the spent fuel samples were 0.15, 0.25, and 1.06 μg/mgU and these values were compared with those from ORIGEN-2 code. A fairly good agreement between the measurements (m) and calculations (c) was obtained, giving ratios (m/c) of 0.93, 1.12 and 1.25 for the three PWR spent fuel samples with burnups of 16.7, 19.0, and 55.9 GWd/MtU, respectively. |
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| AbstractList | A determination method for 237Np in spent nuclear fuel samples was developed using an isotope dilution method with 239Np as a spike. In this method, inductively coupled plasma mass spectrometry (ICP-MS) was taken for the 237Np instead of the previously used alpha spectrometry. 237Np and 239Np were measured by ICP-MS and gamma spectrometry, respectively. The recovery yield of 237Np in synthetic samples was 95.9±9.7% (1S, n=4). The 237Np contents in the spent fuel samples were 0.15, 0.25, and 1.06 μg/mgU and these values were compared with those from ORIGEN-2 code. A fairly good agreement between the measurements (m) and calculations (c) was obtained, giving ratios (m/c) of 0.93, 1.12 and 1.25 for the three PWR spent fuel samples with burnups of 16.7, 19.0, and 55.9 GWd/MtU, respectively. A determination method for 237Np in spent nuclear fuel samples was developed using an isotope dilution method with 239Np as a spike. In this method, inductively coupled plasma mass spectrometry (ICP-MS) was taken for the 237Np instead of the previously used alpha spectrometry. 237Np and 239Np were measured by ICP-MS and gamma spectrometry, respectively. The recovery yield of 237Np in synthetic samples was 95.9±9.7% (1S, n=4). The 237Np contents in the spent fuel samples were 0.15,0.25, and 1.06 μg/mgU and these values were compared with those from ORIGEN-2 code. A fairly good agreement between the measurements (m) and calculations (c) was obtained, giving ratios (m/c) of 0.93, 1.12 and 1.25 for the three PWR spent fuel samples with burnups of 16.7, 19.0, and 55.9 GWd/MtU, respectively. KCI Citation Count: 6 |
| Author | HAN, SUN-HO JOE, KIHSOO SONG, BYUNG-CHUL LEE, CHANG-HEON SONG, KYUSEOK HA, YEONG-KEONG |
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| Cites_doi | 10.13182/NT99-A2947 10.1016/j.jenvrad.2008.06.001 10.5516/NET.2009.41.1.099 10.1039/ja9951000381 10.1039/A606359D 10.1016/S0265-931X(97)00033-7 10.1007/BF02043029 10.1016/j.apradiso.2003.11.078 10.5516/NET.2007.39.5.673 10.1080/18811248.1998.9733882 10.1039/b205001c |
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| Keywords | Inductively Coupled Plasma Mass Spectrometry Gamma Spectrometry Neptunium-237 Isotope Dilution Method Spent Nuclear Fuel |
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| SubjectTerms | Gamma Spectrometry Inductively Coupled Plasma Mass Spectrometry Isotope Dilution Method Neptunium-237 Spent Nuclear Fuel 원자력공학 |
| Title | INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY FOR THE DETERMINATION OF 237Np IN SPENT NUCLEAR FUEL SAMPLES BY ISOTOPE DILUTION METHOD USING 239Np AS A SPIKE |
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