Group 13 Metal Halide Based Coordination Polymers of Al, Ga, In and 2,4,6‐Tri(4‐pyridyl)‐1,3,5‐triazine
Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr3, GaCl3, GaBr3, and InI3 and the tridentate ligand 2,4,6‐tri(4‐pyridyl)‐1,3,5‐triazine (tpt) serving as bidentate linker. The neutral one‐dimensional CPs 1∞[AlBr3(tpt)], 1∞[GaCl3(tpt)], 1∞...
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| Published in | Zeitschrift für anorganische und allgemeine Chemie (1950) Vol. 646; no. 18; pp. 1555 - 1562 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley Subscription Services, Inc
30.09.2020
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| ISSN | 0044-2313 1521-3749 1521-3749 |
| DOI | 10.1002/zaac.202000103 |
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| Abstract | Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr3, GaCl3, GaBr3, and InI3 and the tridentate ligand 2,4,6‐tri(4‐pyridyl)‐1,3,5‐triazine (tpt) serving as bidentate linker. The neutral one‐dimensional CPs 1∞[AlBr3(tpt)], 1∞[GaCl3(tpt)], 1∞[GaBr3(tpt)], and 1∞[InI3(tpt)] are constituted by zigzag‐shaped chains in the crystal structure, in which one coordination site of the tpt ligand remains uncoordinated. All CPs were characterized by SCXRD, PXRD, simultaneous DTA/TG, elemental‐analysis and IR spectroscopy. Furthermore, three complexes of the composition [(AlBr3)3(tpt)], [(GaCl3)3(tpt)], and [(GaBr3)3(tpt)] were structurally characterized by SCXRD, being preliminary and side products of the formation of the coordination polymers. |
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| AbstractList | Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr3, GaCl3, GaBr3, and InI3 and the tridentate ligand 2,4,6‐tri(4‐pyridyl)‐1,3,5‐triazine (tpt) serving as bidentate linker. The neutral one‐dimensional CPs 1∞[AlBr3(tpt)], 1∞[GaCl3(tpt)], 1∞[GaBr3(tpt)], and 1∞[InI3(tpt)] are constituted by zigzag‐shaped chains in the crystal structure, in which one coordination site of the tpt ligand remains uncoordinated. All CPs were characterized by SCXRD, PXRD, simultaneous DTA/TG, elemental‐analysis and IR spectroscopy. Furthermore, three complexes of the composition [(AlBr3)3(tpt)], [(GaCl3)3(tpt)], and [(GaBr3)3(tpt)] were structurally characterized by SCXRD, being preliminary and side products of the formation of the coordination polymers.Dedicated to Prof. Bernd Harbrecht on the Occasion of his 70th Birthday Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr3, GaCl3, GaBr3, and InI3 and the tridentate ligand 2,4,6‐tri(4‐pyridyl)‐1,3,5‐triazine (tpt) serving as bidentate linker. The neutral one‐dimensional CPs 1∞[AlBr3(tpt)], 1∞[GaCl3(tpt)], 1∞[GaBr3(tpt)], and 1∞[InI3(tpt)] are constituted by zigzag‐shaped chains in the crystal structure, in which one coordination site of the tpt ligand remains uncoordinated. All CPs were characterized by SCXRD, PXRD, simultaneous DTA/TG, elemental‐analysis and IR spectroscopy. Furthermore, three complexes of the composition [(AlBr3)3(tpt)], [(GaCl3)3(tpt)], and [(GaBr3)3(tpt)] were structurally characterized by SCXRD, being preliminary and side products of the formation of the coordination polymers. Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr 3 , GaCl 3 , GaBr 3 , and InI 3 and the tridentate ligand 2,4,6‐tri(4‐pyridyl)‐1,3,5‐triazine (tpt) serving as bidentate linker. The neutral one‐dimensional CPs 1 ∞ [AlBr 3 (tpt)], 1 ∞ [GaCl 3 (tpt)], 1 ∞ [GaBr 3 (tpt)], and 1 ∞ [InI 3 (tpt)] are constituted by zigzag‐shaped chains in the crystal structure, in which one coordination site of the tpt ligand remains uncoordinated. All CPs were characterized by SCXRD, PXRD, simultaneous DTA/TG, elemental‐analysis and IR spectroscopy. Furthermore, three complexes of the composition [(AlBr 3 ) 3 (tpt)], [(GaCl 3 ) 3 (tpt)], and [(GaBr 3 ) 3 (tpt)] were structurally characterized by SCXRD, being preliminary and side products of the formation of the coordination polymers. |
| Author | Becker, Jonathan Schäfer, Thomas Sedykh, Alexander E. Müller‐Buschbaum, Klaus |
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| Snippet | Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr3, GaCl3, GaBr3, and InI3 and the tridentate... Four isotypic one‐dimensional coordination polymers (CP) were synthesized using the group 13 metal halides AlBr 3 , GaCl 3 , GaBr 3 , and InI 3 and the... |
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| SubjectTerms | 2,4,6‐Tri(4‐pyridyl)‐1,3,5‐triazine Aluminum Coordination polymer Coordination polymers Crystal structure Gallium Gallium chloride Indium Infrared analysis Infrared spectroscopy Ligands Metal halides Polymers |
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| Title | Group 13 Metal Halide Based Coordination Polymers of Al, Ga, In and 2,4,6‐Tri(4‐pyridyl)‐1,3,5‐triazine |
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