Crystal Structure, Thermal Decomposition Behavior and the Standard Molar Enthalpy of Formation of a Novel 3D Hydrogen- Bonded Supramolecular [Co（HnicO）2·（H2O）2]
Hydrothermal synthesis and X-ray characterized 3D supramolecular networks were constructed by [Co（HnicO）2·（H2O）2] （HnicOH=2-hydroxynicofinic acid） （1） as building block via abundant dimeric homomeric （N--H…O） and unusually cyclic tetrameric heteromeric （O-H…O） hydrogen-bonds. It is noted that there...
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| Published in | Chinese journal of chemistry Vol. 25; no. 1; pp. 16 - 19 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
2007
WILEY‐VCH Verlag |
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| Online Access | Get full text |
| ISSN | 1001-604X 1614-7065 |
| DOI | 10.1002/cjoc.200790010 |
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| Abstract | Hydrothermal synthesis and X-ray characterized 3D supramolecular networks were constructed by [Co（HnicO）2·（H2O）2] （HnicOH=2-hydroxynicofinic acid） （1） as building block via abundant dimeric homomeric （N--H…O） and unusually cyclic tetrameric heteromeric （O-H…O） hydrogen-bonds. It is noted that there exist unusually linear metal-water chains comprised of tetrameric units linked by vertexes sharing cobalt centers through hydrogen-bonding. TG-DTG curves illustrated that thermal decomposition was completed by two steps, one is the loss of two terminal water molecules in the range of 156--234℃, and the other is the pyrolysis of HnicO ligand in the range of 234--730 ℃. The standard molar enthalpy of formation of the complex was determined to be （-1845.43± 2.77） kJ·mol^-1 by a rotary-bomb combustion calorimeter. |
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| AbstractList | Hydrothermal synthesis and X‐ray characterized 3D supramolecular networks were constructed by [Co(HnicO)2·(H2O)2] (HnicOH=2‐hydroxynicotinic acid) (1) as building block via abundant dimeric homomeric (N–H···O) and unusually cyclic tetrameric heteromeric (O–H···O) hydrogen‐bonds. It is noted that there exist unusually linear metal‐water chains comprised of tetrameric units linked by vertexes sharing cobalt centers through hydrogen‐bonding. TG‐DTG curves illustrated that thermal decomposition was completed by two steps, one is the loss of two terminal water molecules in the range of 156–234 °C, and the other is the pyrolysis of HnicO ligand in the range of 234–730 °C. The standard molar enthalpy of formation of the complex was determined to be (−1845.43±2.77) kJ·mol−1 by a rotary‐bomb combustion calorimeter. Hydrothermal synthesis and X-ray characterized 3D supramolecular networks were constructed by [Co（HnicO）2·（H2O）2] （HnicOH=2-hydroxynicofinic acid） （1） as building block via abundant dimeric homomeric （N--H…O） and unusually cyclic tetrameric heteromeric （O-H…O） hydrogen-bonds. It is noted that there exist unusually linear metal-water chains comprised of tetrameric units linked by vertexes sharing cobalt centers through hydrogen-bonding. TG-DTG curves illustrated that thermal decomposition was completed by two steps, one is the loss of two terminal water molecules in the range of 156--234℃, and the other is the pyrolysis of HnicO ligand in the range of 234--730 ℃. The standard molar enthalpy of formation of the complex was determined to be （-1845.43± 2.77） kJ·mol^-1 by a rotary-bomb combustion calorimeter. Hydrothermal synthesis and X‐ray characterized 3D supramolecular networks were constructed by [Co(HnicO) 2 ·(H 2 O) 2 ] (HnicOH=2‐hydroxynicotinic acid) ( 1 ) as building block via abundant dimeric homomeric (N–H···O) and unusually cyclic tetrameric heteromeric (O–H···O) hydrogen‐bonds. It is noted that there exist unusually linear metal‐water chains comprised of tetrameric units linked by vertexes sharing cobalt centers through hydrogen‐bonding. TG‐DTG curves illustrated that thermal decomposition was completed by two steps, one is the loss of two terminal water molecules in the range of 156–234 °C, and the other is the pyrolysis of HnicO ligand in the range of 234–730 °C. The standard molar enthalpy of formation of the complex was determined to be (−1845.43±2.77) kJ·mol −1 by a rotary‐bomb combustion calorimeter. |
| Author | 曾明华 吴美春 朱立红 梁宏 杨旭武 |
| AuthorAffiliation | Department of Chemistry and Chemical Engineering, Guangxi Normal University, Guilin, Guangxi 541004, China Department of Chemistry, Huanggang Normal College, Huangzhou, Hubei 438000, China Department of Chemistry, Northwest University, Xi＇an, Shaanxi 710069, China |
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| Cites_doi | 10.1016/S0040-6031(99)00010-6 10.1002/anie.200462463 10.1016/j.tca.2003.12.025 10.1039/a827289z 10.1002/3527607439 10.1021/ic049232f 10.1107/S0108767394005726 10.1016/j.ica.2003.06.018 10.1016/j.molstruc.2004.10.060 10.1016/S0020-1693(03)00500-0 10.1002/1521-3773(20020104)41:1<48::AID-ANIE48>3.0.CO;2-U |
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| Notes | 31-1547/O6 O614.812 O641.4 cobalt complex, hydrogen bond, supramolecular, thermal decomposition behavior, standard molar enthalpy of formation the Teaching and Research Award Program for Outstanding Young Teachers in Higher Education Institutions of Chinese Ministry of Education the Natural Science Foundation of Guangxi Province - No. 0447019 ArticleID:CJOC200790010 ark:/67375/WNG-W8WB1NZ3-2 istex:29FD661C88F46C783EA59E9789E6AE971157F7A5 the National Natural Science Foundation of China - No. 30460153, 20561001 |
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| References_xml | – reference: Chen, X. M.; Tong, M. L., Frontiers in Crystal Engineering, John Wiley & Sons, Ltd, USA, 2006, pp. 223-266. – reference: Jeffrey, G. A., An Introduction to Hydrogen Bonding, Spring, Oxford University Press, Oxford, U. K. , 1997, pp. 160-180. – reference: Zeng, M. H.; Zhang, W. X.; Sun, X. Z.; Chen, X. M.. Angew. Chem., Int. Ed., 2005, 44, 3079. – reference: Lehn, J.-M., Supramolecular Chemistry, VCH, Weinheim, 1995. – reference: Jones, J. C.. Chem., Soc. Rev., 1998, 27, 289. – reference: Marco, V. B. D.; Tapparo, A.; Dolmella, A.; Bombi, G. G.. Inorg. Chim. Acta, 2004, 357, 135. – reference: Popov, M. M., Thermometry and Calorimetry, Moscow University Publishing House, Moscow, 1954, p. 382. – reference: Liu, J. R.; Yang, X. W.; Hou, Y. D.. Thermochim. Acta, 1999, 329, 123. – reference: Dogra, S. K.. J. Mol. Struct., 2005, 737, 189. – reference: Steiner, T.. Angew. Chem., Int. Ed., 2002, 41, 48. – reference: Ye, B. H.; Ding, B. B.; Weng, Y. Q.; Chen, X. M.. Inorg. Chem., 2004, 43, 6866. – reference: Chattopadhyay, S.; Fanwick, P. E.; Walton, R. A.. Inorg. Chim. Acta, 2004, 357, 764. – reference: Yang, X. W.; Yang, X. F.; Zhang, Q. Z.; Zhang, T. C.. J. Northwest Univ. (Nat. Sci. Ed.), 1996, 26, 122 (in Chinese). – reference: Fan, X. Z.; Xie, G.; Chen, S. P.; Gao, S. L.; Shi, Q. Z.. Thermochim. Acta, 2004, 413, 87. – reference: Yang, X. F.; Yang, X. W.; Sun, L. Z.. Chem. J. Chin. Univ., 1986, 7, 363 (in Chinese). – reference: Lehaire, M. L.; Scopelliti, R.; Herdeis, L.; Polborn, K.; Mayer, P.; Severin, K.. Inorg. Chem., 2004, 431, 609. – reference: Blessing, R.. Acta Crystallogr., Sect. A, 1995, 51, 33. – volume: 357 start-page: 135 year: 2004 publication-title: Inorg. Chim. Acta – volume: 41 start-page: 48 year: 2002 publication-title: Angew. Chem., Int. Ed. – volume: 44 start-page: 3079 year: 2005 publication-title: Angew. Chem., Int. Ed. – volume: 431 start-page: 609 year: 2004 publication-title: Inorg. Chem. – volume: 51 start-page: 33 year: 1995 publication-title: Acta Crystallogr., Sect. A – year: 2001 – volume: 26 start-page: 122 year: 1996 publication-title: J. Northwest Univ. (Nat. Sci. Ed.) – start-page: 160 year: 1997 end-page: 180 – start-page: 223 year: 2006 end-page: 266 – year: 1995 – volume: 329 start-page: 123 year: 1999 publication-title: Thermochim. Acta – volume: 27 start-page: 289 year: 1998 publication-title: Chem., Soc. Rev. – volume: 413 start-page: 87 year: 2004 publication-title: Thermochim. Acta – volume: 737 start-page: 189 year: 2005 publication-title: J. Mol. Struct. – volume: 43 start-page: 6866 year: 2004 publication-title: Inorg. Chem. – start-page: 382 year: 1954 – volume: 357 start-page: 764 year: 2004 publication-title: Inorg. Chim. Acta – year: 1998 – year: 1999 – volume: 7 start-page: 363 year: 1986 publication-title: Chem. J. Chin. Univ. – ident: e_1_2_1_16_2 doi: 10.1016/S0040-6031(99)00010-6 – ident: e_1_2_1_11_2 doi: 10.1002/anie.200462463 – ident: e_1_2_1_20_2 doi: 10.1016/j.tca.2003.12.025 – ident: e_1_2_1_3_2 doi: 10.1039/a827289z – start-page: 160 volume-title: An Introduction to Hydrogen Bonding year: 1997 ident: e_1_2_1_5_2 – volume: 431 start-page: 609 year: 2004 ident: e_1_2_1_9_2 publication-title: Inorg. Chem. – volume: 26 start-page: 122 year: 1996 ident: e_1_2_1_18_2 publication-title: J. Northwest Univ. (Nat. Sci. Ed.) – ident: e_1_2_1_6_2 doi: 10.1002/3527607439 – ident: e_1_2_1_21_2 doi: 10.1021/ic049232f – ident: e_1_2_1_13_2 – ident: e_1_2_1_14_2 doi: 10.1107/S0108767394005726 – ident: e_1_2_1_10_2 doi: 10.1016/j.ica.2003.06.018 – ident: e_1_2_1_15_2 – ident: e_1_2_1_7_2 doi: 10.1016/j.molstruc.2004.10.060 – ident: e_1_2_1_8_2 doi: 10.1016/S0020-1693(03)00500-0 – ident: e_1_2_1_12_2 – start-page: 223 volume-title: Frontiers in Crystal Engineering year: 2006 ident: e_1_2_1_2_2 – volume: 7 start-page: 363 year: 1986 ident: e_1_2_1_17_2 publication-title: Chem. J. Chin. Univ. – ident: e_1_2_1_4_2 doi: 10.1002/1521-3773(20020104)41:1<48::AID-ANIE48>3.0.CO;2-U – start-page: 382 volume-title: Thermometry and Calorimetry year: 1954 ident: e_1_2_1_19_2 |
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| Snippet | Hydrothermal synthesis and X-ray characterized 3D supramolecular networks were constructed by [Co（HnicO）2·（H2O）2] （HnicOH=2-hydroxynicofinic acid） （1）... Hydrothermal synthesis and X‐ray characterized 3D supramolecular networks were constructed by [Co(HnicO)2·(H2O)2] (HnicOH=2‐hydroxynicotinic acid) (1) as... Hydrothermal synthesis and X‐ray characterized 3D supramolecular networks were constructed by [Co(HnicO) 2 ·(H 2 O) 2 ] (HnicOH=2‐hydroxynicotinic acid) ( 1 )... |
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| SubjectTerms | 2-羟基烟酸 cobalt complex hydrogen bond standard molar enthalpy of formation supramolecular thermal decomposition behavior 晶体结构 标准摩尔生成焓 热分解行为 超分子组装 钴配合物 |
| Title | Crystal Structure, Thermal Decomposition Behavior and the Standard Molar Enthalpy of Formation of a Novel 3D Hydrogen- Bonded Supramolecular [Co（HnicO）2·（H2O）2] |
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