Room temperature synthesized spherical V-MCM-41: a catalyst for vapour phase oxidation of diphenylmethane
Mesoporous spherical Si-MCM-41 and V-MCM-41 materials with a variable Si/V ratio of 25, 50, 75 and 100 were prepared by an economical route at room temperature and characterized by various techniques for qualitative and quantitative understanding of vanadium species. The morphology and mesoporosity...
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| Published in | Journal of porous materials Vol. 19; no. 6; pp. 1027 - 1036 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Boston
Springer US
01.12.2012
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1380-2224 1573-4854 |
| DOI | 10.1007/s10934-012-9562-5 |
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| Abstract | Mesoporous spherical Si-MCM-41 and V-MCM-41 materials with a variable Si/V ratio of 25, 50, 75 and 100 were prepared by an economical route at room temperature and characterized by various techniques for qualitative and quantitative understanding of vanadium species. The morphology and mesoporosity of the spherical particles were confirmed by SEM and TEM micrographs. The catalytic activity of the synthesized catalysts was tested for vapour phase oxidation of diphenylmethane to benzophenone using CO
2
free air as oxidant at atmospheric pressure. The conversion of diphenylmethane and selectivity for benzophenone were measured in the temperature range of 593–713 K over V-MCM-41 catalysts synthesized by adopting room temperature method as well as by direct hydrothermal method. The catalytic performance was related to vanadium content on the surface of the catalysts. |
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| AbstractList | Mesoporous spherical Si-MCM-41 and V-MCM-41 materials with a variable Si/V ratio of 25, 50, 75 and 100 were prepared by an economical route at room temperature and characterized by various techniques for qualitative and quantitative understanding of vanadium species. The morphology and mesoporosity of the spherical particles were confirmed by SEM and TEM micrographs. The catalytic activity of the synthesized catalysts was tested for vapour phase oxidation of diphenylmethane to benzophenone using CO sub(2) free air as oxidant at atmospheric pressure. The conversion of diphenylmethane and selectivity for benzophenone were measured in the temperature range of 593-713 K over V-MCM-41 catalysts synthesized by adopting room temperature method as well as by direct hydrothermal method. The catalytic performance was related to vanadium content on the surface of the catalysts. Mesoporous spherical Si-MCM-41 and V-MCM-41 materials with a variable Si/V ratio of 25, 50, 75 and 100 were prepared by an economical route at room temperature and characterized by various techniques for qualitative and quantitative understanding of vanadium species. The morphology and mesoporosity of the spherical particles were confirmed by SEM and TEM micrographs. The catalytic activity of the synthesized catalysts was tested for vapour phase oxidation of diphenylmethane to benzophenone using CO2 free air as oxidant at atmospheric pressure. The conversion of diphenylmethane and selectivity for benzophenone were measured in the temperature range of 593-713 K over V-MCM-41 catalysts synthesized by adopting room temperature method as well as by direct hydrothermal method. The catalytic performance was related to vanadium content on the surface of the catalysts.[PUBLICATION ABSTRACT] Mesoporous spherical Si-MCM-41 and V-MCM-41 materials with a variable Si/V ratio of 25, 50, 75 and 100 were prepared by an economical route at room temperature and characterized by various techniques for qualitative and quantitative understanding of vanadium species. The morphology and mesoporosity of the spherical particles were confirmed by SEM and TEM micrographs. The catalytic activity of the synthesized catalysts was tested for vapour phase oxidation of diphenylmethane to benzophenone using CO 2 free air as oxidant at atmospheric pressure. The conversion of diphenylmethane and selectivity for benzophenone were measured in the temperature range of 593–713 K over V-MCM-41 catalysts synthesized by adopting room temperature method as well as by direct hydrothermal method. The catalytic performance was related to vanadium content on the surface of the catalysts. |
| Author | Shanthi, K. Sasirekha, N. R. Suresh, C. Santhanaraj, D. Gurulakshmi, M. |
| Author_xml | – sequence: 1 givenname: D. surname: Santhanaraj fullname: Santhanaraj, D. organization: Department of Chemistry, Anna University – sequence: 2 givenname: C. surname: Suresh fullname: Suresh, C. organization: Department of Chemistry, Anna University – sequence: 3 givenname: M. surname: Gurulakshmi fullname: Gurulakshmi, M. organization: Department of Chemistry, Anna University – sequence: 4 givenname: N. R. surname: Sasirekha fullname: Sasirekha, N. R. organization: Department of Chemistry, Anna University – sequence: 5 givenname: K. surname: Shanthi fullname: Shanthi, K. email: shanthiramesh@annauniv.edu organization: Department of Chemistry, Anna University |
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| CitedBy_id | crossref_primary_10_1016_j_catcom_2017_09_004 crossref_primary_10_1016_j_mcat_2017_07_012 crossref_primary_10_1016_j_micromeso_2019_109581 crossref_primary_10_1002_ejic_201800317 |
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| Keywords | Spherical V-MCM-41 Diphenylmethane Vapour phase oxidation Room temperature Benzophenone |
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| SubjectTerms | Atmospheric pressure Catalysis Catalysts Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Economics Micrographs Oxidants Oxidation Physical Chemistry Vanadium Vapour |
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| Title | Room temperature synthesized spherical V-MCM-41: a catalyst for vapour phase oxidation of diphenylmethane |
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