Facile fabrication of a direct Z-scheme Ag2CrO4/g-C3N4 photocatalyst with enhanced visible light photocatalytic activity
[Display omitted] •A Z-scheme Ag2CrO4/g-C3N4-N photocatalyst was prepared successfully;.•The high surface areas of the g-C3N4-N can prevent the aggregation of Ag2CrO4 nanoparticles;.•The synergistic effect between Ag2CrO4 and g-C3N4-N promoted the separation of charges;.•Enhanced photocatalysis was...
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| Published in | Journal of molecular catalysis. A, Chemical Vol. 421; pp. 209 - 221 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.09.2016
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1381-1169 1873-314X |
| DOI | 10.1016/j.molcata.2016.05.024 |
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| Abstract | [Display omitted]
•A Z-scheme Ag2CrO4/g-C3N4-N photocatalyst was prepared successfully;.•The high surface areas of the g-C3N4-N can prevent the aggregation of Ag2CrO4 nanoparticles;.•The synergistic effect between Ag2CrO4 and g-C3N4-N promoted the separation of charges;.•Enhanced photocatalysis was achieved via Z-scheme Ag2CrO4/g-C3N4-N photocatalysts.
Graphite-like carbon nitride (g-C3N4) and silver-based compounds have attracted considerable attentions due to their excellent optical characteristic and photocatalytic performance. In this work, Z-scheme silver chromate-g-C3N4 nanosheets photocatalysts were prepared by binding growth of Ag2CrO4 nanoparticles on the surface of g-C3N4 nanosheets (g-C3N4-N) via a facile precipitation method. The morphologies, structure, specific surface area and optical property of the prepared photocatalysts were characterized by X-ray diffraction (XRD), field emission-scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution-transmission electron microscopy (HR-TEM), X-ray photoelectron spectroscopy (XPS), UV–vis diffuse reflectance spectra (UV-vis DRS) and photoluminescence (PL) spectra. The photocatalytic performances of the prepared Ag2CrO4/g-C3N4-N were evaluated by photodegradation of methyl orange (MO) and rhodamine B (RhB) under visible light irradiation (λ>400nm). The experiment results indicated that Ag2CrO4/g-C3N4-N composites presented enhanced photocatalytic activity and stability in the degradation of the dye contaminants in aqueous solution. The optimal composites with the mass ratio of Ag2CrO4 to g-C3N4-N as 50% (CNA-50) showed the highest photocatalytic activity for MO degradation, which is 5.9 and 10.8 times than those of pure Ag2CrO4 and pure g-C3N4-N, respectively. The formation of Ag2CrO4/g-C3N4-N Z-scheme heterojunction contributed to the improved photodegradation efficiency, which can not only promote the separation and transportation efficiencies of the photogenerated electron-hole pairs, but also present strong redox ability. And meanwhile the excellent transportation efficiency of the photogenerated electrons from Ag2CrO4 to g-C3N4-N greatly hindered the photocorrosion of Ag2CrO4 nanoparticles. This work provides a new understanding into the mechanism of the g-C3N4-N based composite and gives a new insight into the design and fabrication of Z-scheme photocatalysts. |
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| AbstractList | [Display omitted]
•A Z-scheme Ag2CrO4/g-C3N4-N photocatalyst was prepared successfully;.•The high surface areas of the g-C3N4-N can prevent the aggregation of Ag2CrO4 nanoparticles;.•The synergistic effect between Ag2CrO4 and g-C3N4-N promoted the separation of charges;.•Enhanced photocatalysis was achieved via Z-scheme Ag2CrO4/g-C3N4-N photocatalysts.
Graphite-like carbon nitride (g-C3N4) and silver-based compounds have attracted considerable attentions due to their excellent optical characteristic and photocatalytic performance. In this work, Z-scheme silver chromate-g-C3N4 nanosheets photocatalysts were prepared by binding growth of Ag2CrO4 nanoparticles on the surface of g-C3N4 nanosheets (g-C3N4-N) via a facile precipitation method. The morphologies, structure, specific surface area and optical property of the prepared photocatalysts were characterized by X-ray diffraction (XRD), field emission-scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution-transmission electron microscopy (HR-TEM), X-ray photoelectron spectroscopy (XPS), UV–vis diffuse reflectance spectra (UV-vis DRS) and photoluminescence (PL) spectra. The photocatalytic performances of the prepared Ag2CrO4/g-C3N4-N were evaluated by photodegradation of methyl orange (MO) and rhodamine B (RhB) under visible light irradiation (λ>400nm). The experiment results indicated that Ag2CrO4/g-C3N4-N composites presented enhanced photocatalytic activity and stability in the degradation of the dye contaminants in aqueous solution. The optimal composites with the mass ratio of Ag2CrO4 to g-C3N4-N as 50% (CNA-50) showed the highest photocatalytic activity for MO degradation, which is 5.9 and 10.8 times than those of pure Ag2CrO4 and pure g-C3N4-N, respectively. The formation of Ag2CrO4/g-C3N4-N Z-scheme heterojunction contributed to the improved photodegradation efficiency, which can not only promote the separation and transportation efficiencies of the photogenerated electron-hole pairs, but also present strong redox ability. And meanwhile the excellent transportation efficiency of the photogenerated electrons from Ag2CrO4 to g-C3N4-N greatly hindered the photocorrosion of Ag2CrO4 nanoparticles. This work provides a new understanding into the mechanism of the g-C3N4-N based composite and gives a new insight into the design and fabrication of Z-scheme photocatalysts. |
| Author | Chen, Fei Zeng, Guangming Wang, Jiajia Deng, Yaocheng Tang, Lin Wang, Jingjing Tang, Jing Peng, Bo Zhou, Yaoyu Liu, Yani |
| Author_xml | – sequence: 1 givenname: Yaocheng surname: Deng fullname: Deng, Yaocheng organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 2 givenname: Lin surname: Tang fullname: Tang, Lin email: tanglin@hnu.edu.cn organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 3 givenname: Guangming surname: Zeng fullname: Zeng, Guangming email: zgming@hnu.edu.cn organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 4 givenname: Jiajia surname: Wang fullname: Wang, Jiajia organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 5 givenname: Yaoyu surname: Zhou fullname: Zhou, Yaoyu organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 6 givenname: Jingjing surname: Wang fullname: Wang, Jingjing organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 7 givenname: Jing surname: Tang fullname: Tang, Jing organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 8 givenname: Yani surname: Liu fullname: Liu, Yani organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 9 givenname: Bo surname: Peng fullname: Peng, Bo organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China – sequence: 10 givenname: Fei surname: Chen fullname: Chen, Fei organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, China |
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•A Z-scheme Ag2CrO4/g-C3N4-N photocatalyst was prepared successfully;.•The high surface areas of the g-C3N4-N can prevent the aggregation of... |
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| SubjectTerms | Ag2CrO4 g-C3N4 nanosheets Photocatalyst Visible light Z-scheme |
| Title | Facile fabrication of a direct Z-scheme Ag2CrO4/g-C3N4 photocatalyst with enhanced visible light photocatalytic activity |
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