Effect of wear debris of Al2O3, ZrO2 and WC balls on Y-α/β-SiAlON ceramics consolidated by spark plasma sintering
Three types of Y-α/β-SiAlON powders were prepared by mixing and milling the raw materials for 20 h using Al 2 O 3 , ZrO 2 , and WC balls, thereafter denoted as SNA, SNZ and SNW, respectively. The three types of specimens were sintered using spark plasma sintering (SPS) at 1510 °C for 5 min under 30...
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| Published in | Metals and materials international Vol. 19; no. 2; pp. 163 - 169 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Springer
The Korean Institute of Metals and Materials
01.03.2013
대한금속·재료학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1598-9623 2005-4149 |
| DOI | 10.1007/s12540-013-2005-2 |
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| Abstract | Three types of Y-α/β-SiAlON powders were prepared by mixing and milling the raw materials for 20 h using Al
2
O
3
, ZrO
2
, and WC balls, thereafter denoted as SNA, SNZ and SNW, respectively. The three types of specimens were sintered using spark plasma sintering (SPS) at 1510 °C for 5 min under 30 MPa in a vacuum. α-phases (SiAlON and Si
3
N
4
) and β-SiAlON phase were observed in the SNA and SNZ specimens, but only the β-SiAlON phase existed in the SNW specimen. The wear debris of the WC balls affected the grain boundary properties and eventually promoted the full phase transformation of α-Si
3
N
4
into α- and β-SiAlON phases. However, SNA and SNZ were partially transformed into α- and β-SiAlON phases. The Vickers hardness of SNA was the highest (18.7 GPa), due to its having the highest content of α-phase, but its fracture toughness was the lowest (4.09 MPam
1/2
) due to its having the lowest content of β-SiAlON phase. The wear debris and secondary phases existed at the grain boundary, mostly at the triple junction, and also affected the color. The color of the sintered specimen was quite different depending on the milling media. |
|---|---|
| AbstractList | Three types of Y-α/β-SiAlON powders were prepared by mixing and milling the raw materials for 20 h using Al2O3, ZrO2, and WC balls, thereafter denoted as SNA, SNZ and SNW, respectively. The three types of specimens were sintered using spark plasma sintering (SPS) at 1510 °C for 5 min under 30 MPa in a vacuum. α-phases (SiAlON and Si3N4) and β-SiAlON phase were observed in the SNA and SNZ specimens,but only the β-SiAlON phase existed in the SNW specimen. The wear debris of the WC balls affected the grain boundary properties and eventually promoted the full phase transformation of α-Si3N4 into α- and β-SiAlON phases. However, SNA and SNZ were partially transformed into α- and β-SiAlON phases. The Vickers hardness of SNA was the highest (18.7 GPa), due to its having the highest content of α-phase, but its fracture toughness was the lowest (4.09 MPam1/2) due to its having the lowest content of β-SiAlON phase.
The wear debris and secondary phases existed at the grain boundary, mostly at the triple junction, and also affected the color. The color of the sintered specimen was quite different depending on the milling media. KCI Citation Count: 3 Three types of Y-α/β-SiAlON powders were prepared by mixing and milling the raw materials for 20 h using Al 2 O 3 , ZrO 2 , and WC balls, thereafter denoted as SNA, SNZ and SNW, respectively. The three types of specimens were sintered using spark plasma sintering (SPS) at 1510 °C for 5 min under 30 MPa in a vacuum. α-phases (SiAlON and Si 3 N 4 ) and β-SiAlON phase were observed in the SNA and SNZ specimens, but only the β-SiAlON phase existed in the SNW specimen. The wear debris of the WC balls affected the grain boundary properties and eventually promoted the full phase transformation of α-Si 3 N 4 into α- and β-SiAlON phases. However, SNA and SNZ were partially transformed into α- and β-SiAlON phases. The Vickers hardness of SNA was the highest (18.7 GPa), due to its having the highest content of α-phase, but its fracture toughness was the lowest (4.09 MPam 1/2 ) due to its having the lowest content of β-SiAlON phase. The wear debris and secondary phases existed at the grain boundary, mostly at the triple junction, and also affected the color. The color of the sintered specimen was quite different depending on the milling media. |
| Author | Kim, Kwang-Ho Kim, Young-Ki Min, Bong-Ki Kim, Sukyoung Han, Young-Hwan Kim, Young-Moon Lee, Kyeongseok Chun, Sungsu Jung, Young Geun |
| Author_xml | – sequence: 1 givenname: Sungsu surname: Chun fullname: Chun, Sungsu organization: School of Materials Science and Engineering, Yeungnam University – sequence: 2 givenname: Bong-Ki surname: Min fullname: Min, Bong-Ki organization: Center for Research Facilities, Yeungnam University – sequence: 3 givenname: Young-Hwan surname: Han fullname: Han, Young-Hwan organization: School of Materials Science and Engineering, Yeungnam University – sequence: 4 givenname: Young-Moon surname: Kim fullname: Kim, Young-Moon organization: NCRC for Hybrid Materials Solution, Pusan National University – sequence: 5 givenname: Kyeongseok surname: Lee fullname: Lee, Kyeongseok organization: NCRC for Hybrid Materials Solution, Pusan National University – sequence: 6 givenname: Young Geun surname: Jung fullname: Jung, Young Geun organization: NCRC for Hybrid Materials Solution, Pusan National University – sequence: 7 givenname: Kwang-Ho surname: Kim fullname: Kim, Kwang-Ho organization: NCRC for Hybrid Materials Solution, Pusan National University – sequence: 8 givenname: Young-Ki surname: Kim fullname: Kim, Young-Ki organization: Central Research Facility, Ulsan National Institute of Science and Technology – sequence: 9 givenname: Sukyoung surname: Kim fullname: Kim, Sukyoung email: sykim@ynu.ac.kr organization: School of Materials Science and Engineering, Yeungnam University |
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| CitedBy_id | crossref_primary_10_1016_j_ceramint_2022_07_125 crossref_primary_10_1016_j_wear_2020_203216 crossref_primary_10_1007_s12540_014_6003_9 crossref_primary_10_1016_j_ceramint_2021_07_205 |
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2
O
3
, ZrO
2
, and WC balls, thereafter denoted as... Three types of Y-α/β-SiAlON powders were prepared by mixing and milling the raw materials for 20 h using Al2O3, ZrO2, and WC balls, thereafter denoted as SNA,... |
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| Title | Effect of wear debris of Al2O3, ZrO2 and WC balls on Y-α/β-SiAlON ceramics consolidated by spark plasma sintering |
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