Inverse analysis of oxygen diffusivity in oak wood using the back-face method: application to cooperage
During the aging of wines and spirits in oak barrels, oxygen diffusion through the wood occurs and leads to mild oxygenation of the beverage. In this study, the oxygen diffusivity in oak wood was determined by inverse analysis using the back-face method. In the measurement setup, a defined oxygen co...
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| Published in | Wood science and technology Vol. 56; no. 1; pp. 219 - 239 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Berlin/Heidelberg
Springer Berlin Heidelberg
01.01.2022
Springer Nature B.V Springer Verlag |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0043-7719 1432-5225 |
| DOI | 10.1007/s00226-021-01325-2 |
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| Abstract | During the aging of wines and spirits in oak barrels, oxygen diffusion through the wood occurs and leads to mild oxygenation of the beverage. In this study, the oxygen diffusivity in oak wood was determined by inverse analysis using the back-face method. In the measurement setup, a defined oxygen concentration was applied to the front of a sample and the variation of oxygen concentration due to gas diffusion through the sample was measured on the back. The experiment was carried out simultaneously on several samples. It was then possible to study 36 samples and to assess the effect of several parameters in a reasonable time. A finite volume model using the actual experimental conditions as boundary conditions was implemented for the identification of the diffusion coefficient. The obtained values range between 4.64 × 10
−11
and 2.02 × 10
−9
m
2
s
−1
and highlight the high heterogeneity of oak wood. Such low values, compared to the diffusion of oxygen in air (a factor 10
5
lower), reflect the huge tortuosity of oak wood in its tangential direction. |
|---|---|
| AbstractList | During the aging of wines and spirits in oak barrels, oxygen diffusion through the wood occurs and leads to mild oxygenation of the beverage. In this study, the oxygen diffusivity in oak wood was determined by inverse analysis using the back-face method. In the measurement setup, a defined oxygen concentration was applied to the front of a sample and the variation of oxygen concentration due to gas diffusion through the sample was measured on the back. The experiment was carried out simultaneously on several samples. It was then possible to study 36 samples and to assess the effect of several parameters in a reasonable time. A finite volume model using the actual experimental conditions as boundary conditions was implemented for the identification of the diffusion coefficient. The obtained values range between 4.64 × 10−11 and 2.02 × 10−9 m2 s−1 and highlight the high heterogeneity of oak wood. Such low values, compared to the diffusion of oxygen in air (a factor 105 lower), reflect the huge tortuosity of oak wood in its tangential direction. During the aging of wines and spirits in oak barrels, oxygen diffusion through the wood occurs and leads to mild oxygenation of the beverage. In this study, the oxygen diffusivity in oak wood was determined by inverse analysis using the back-face method. In the measurement setup, a defined oxygen concentration was applied to the front of a sample and the variation of oxygen concentration due to gas diffusion through the sample was measured on the back. The experiment was carried out simultaneously on several samples. It was then possible to study 36 samples and to assess the effect of several parameters in a reasonable time. A finite volume model using the actual experimental conditions as boundary conditions was implemented for the identification of the diffusion coefficient. The obtained values range between 4.64 × 10 −11 and 2.02 × 10 −9 m 2 s −1 and highlight the high heterogeneity of oak wood. Such low values, compared to the diffusion of oxygen in air (a factor 10 5 lower), reflect the huge tortuosity of oak wood in its tangential direction. During the aging of wines and spirits in oak barrels, oxygen diffusion through the wood occurs and leads to mild oxygenation of the beverage. In this study, the oxygen diffusivity in oak wood was determined by inverse analysis using the back-face method. In the measurement setup, a defined oxygen concentration was applied to the front of a sample and the variation of oxygen concentration due to gas diffusion through the sample was measured on the back. The experiment was carried out simultaneously on several samples. It was then possible to study 36 samples and to assess the effect of several parameters in a reasonable time. A finite volume model using the actual experimental conditions as boundary conditions was implemented for the identification of the diffusion coefficient. The obtained values range between 4.64 × 10⁻¹¹ and 2.02 × 10⁻⁹ m² s⁻¹ and highlight the high heterogeneity of oak wood. Such low values, compared to the diffusion of oxygen in air (a factor 10⁵ lower), reflect the huge tortuosity of oak wood in its tangential direction. |
| Author | Casalinho, Joel Colin, Julien Roussey, Claire Perré, Patrick |
| Author_xml | – sequence: 1 givenname: Claire orcidid: 0000-0001-9457-2138 surname: Roussey fullname: Roussey, Claire email: claire.roussey@orange.fr organization: CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, Université Paris Saclay, Département R&D, Chêne & Cie – sequence: 2 givenname: Patrick surname: Perré fullname: Perré, Patrick organization: CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, Université Paris Saclay, CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, SFR Condorcet FR CNRS 3417, Centre Européen de Biotechnologie et de Bioéconomie (CEBB), Université Paris Saclay – sequence: 3 givenname: Joel surname: Casalinho fullname: Casalinho, Joel organization: CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, Université Paris Saclay – sequence: 4 givenname: Julien surname: Colin fullname: Colin, Julien organization: CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, Université Paris Saclay, CentraleSupélec, Laboratoire de Génie des Procédés et Matériaux, SFR Condorcet FR CNRS 3417, Centre Européen de Biotechnologie et de Bioéconomie (CEBB), Université Paris Saclay |
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| SubjectTerms | Aging air Biomedical and Life Sciences Boundary conditions Ceramics Chemical Sciences Composites Diffusion coefficient Diffusivity Gaseous diffusion Glass Heterogeneity Humidity Life Sciences Machines Manufacturing Material chemistry Methods Natural Materials Oak Original Oxygen Oxygenation Processes technology Tortuosity Wood Wood Science & Technology Wood sciences |
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| Title | Inverse analysis of oxygen diffusivity in oak wood using the back-face method: application to cooperage |
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