Cu-doped TiO2 hollow nanostructures for the enhanced photocatalysis under visible light conditions
[Display omitted] •Cu doped TiO2 hollow nanostructures were synthesized for visible light responsive photocatalysis.•The Cu-doped TiO2 photocatalysts shows superior activities than its anatase counterpart, under visible light conditions.•CT–650–HCl catalyst shows the best performance in phenol photo...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 99; pp. 352 - 363 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.07.2021
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-086X 1876-794X |
| DOI | 10.1016/j.jiec.2021.04.045 |
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| Abstract | [Display omitted]
•Cu doped TiO2 hollow nanostructures were synthesized for visible light responsive photocatalysis.•The Cu-doped TiO2 photocatalysts shows superior activities than its anatase counterpart, under visible light conditions.•CT–650–HCl catalyst shows the best performance in phenol photo-degradation.
We report a synthetic strategy for fabricating Cu-doped TiO2 hollow nanostructure for visible light responsive photocatalysis. Hollow Cu-doped TiO2 photocatalysts were prepared by sol–gel coating of TiO2 on the surface of SiO2, removal of sacrificial core, Cu2+ ion exchange, and calcination followed by acid leaching. The ion exchanged Cu species allows TiO2 shell to be preferentially crystallized rutile phase, even at low calcination temperature. The acid leaching allows the excess bulk CuO to be dissolved out and Cu-doped TiO2 to expose more reactive TiO2 surface. No measurable CuO composites were observed while uniformly distributed Cu species is detected in acid treated CT–X–HCl samples indicating the Cu2+ ions were homogeneously doped into crystalline TiO2 frameworks. In particular, the CT–650–HCl catalyst that was prepared by calcination at 650°C, followed by HCl leaching, showed beneficial physio-chemical properties, such as narrow bandgap, mixed anatase-rutile crystalline phase, and more reactive TiO2 surface with high surface area, resulting in the best photocatalytic performance towards phenol degradation under visible light conditions. |
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| AbstractList | We report a synthetic strategy for fabricating Cu-doped TiO2 hollow nanostructure for visible lightresponsive photocatalysis. Hollow Cu-doped TiO2 photocatalysts were prepared by sol–gel coating ofTiO2 on the surface of SiO2, removal of sacrificial core, Cu2+ ion exchange, and calcination followed by acidleaching. The ion exchanged Cu species allows TiO2 shell to be preferentially crystallized rutile phase,even at low calcination temperature. The acid leaching allows the excess bulk CuO to be dissolved out andCu-doped TiO2 to expose more reactive TiO2 surface. No measurable CuO composites were observedwhile uniformly distributed Cu species is detected in acid treated CT–X–HCl samples indicating the Cu2+ions were homogeneously doped into crystalline TiO2 frameworks. In particular, the CT–650–HCl catalystthat was prepared by calcination at 650 C, followed by HCl leaching, showed beneficial physio-chemicalproperties, such as narrow bandgap, mixed anatase-rutile crystalline phase, and more reactive TiO2surface with high surface area, resulting in the best photocatalytic performance towards phenoldegradation under visible light conditions. KCI Citation Count: 13 [Display omitted] •Cu doped TiO2 hollow nanostructures were synthesized for visible light responsive photocatalysis.•The Cu-doped TiO2 photocatalysts shows superior activities than its anatase counterpart, under visible light conditions.•CT–650–HCl catalyst shows the best performance in phenol photo-degradation. We report a synthetic strategy for fabricating Cu-doped TiO2 hollow nanostructure for visible light responsive photocatalysis. Hollow Cu-doped TiO2 photocatalysts were prepared by sol–gel coating of TiO2 on the surface of SiO2, removal of sacrificial core, Cu2+ ion exchange, and calcination followed by acid leaching. The ion exchanged Cu species allows TiO2 shell to be preferentially crystallized rutile phase, even at low calcination temperature. The acid leaching allows the excess bulk CuO to be dissolved out and Cu-doped TiO2 to expose more reactive TiO2 surface. No measurable CuO composites were observed while uniformly distributed Cu species is detected in acid treated CT–X–HCl samples indicating the Cu2+ ions were homogeneously doped into crystalline TiO2 frameworks. In particular, the CT–650–HCl catalyst that was prepared by calcination at 650°C, followed by HCl leaching, showed beneficial physio-chemical properties, such as narrow bandgap, mixed anatase-rutile crystalline phase, and more reactive TiO2 surface with high surface area, resulting in the best photocatalytic performance towards phenol degradation under visible light conditions. |
| Author | Joo, Ji Bong Jang, Hyun Sung Kim, Na Yeon Lee, Hyeonkyeong |
| Author_xml | – sequence: 1 givenname: Hyeonkyeong orcidid: 0000-0001-6430-7210 surname: Lee fullname: Lee, Hyeonkyeong – sequence: 2 givenname: Hyun Sung surname: Jang fullname: Jang, Hyun Sung – sequence: 3 givenname: Na Yeon surname: Kim fullname: Kim, Na Yeon – sequence: 4 givenname: Ji Bong surname: Joo fullname: Joo, Ji Bong email: jbjoo@konkuk.ac.kr |
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•Cu doped TiO2 hollow nanostructures were synthesized for visible light responsive photocatalysis.•The Cu-doped TiO2 photocatalysts shows... We report a synthetic strategy for fabricating Cu-doped TiO2 hollow nanostructure for visible lightresponsive photocatalysis. Hollow Cu-doped TiO2... |
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| SubjectTerms | Cu-doped TiO2 Hollow nanostructure Photocatalyst Photodegradation Visible light responsive 화학공학 |
| Title | Cu-doped TiO2 hollow nanostructures for the enhanced photocatalysis under visible light conditions |
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