Rapid detection of thiabendazole in food using SERS coupled with flower-like AgNPs and PSL-based variable selection algorithms
Thiabendazole (TBZ) exposure through food can have substantial long-term health consequences for humans. Herein, SERS coupled with flower-like AgNPs and python-scikit-learn (PSL) algorithms, was proposed for rapid detection of TBZ. Initially, AgNFs with a strong enhancement factor (EF) of 1.303 × 10...
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| Published in | Journal of food composition and analysis Vol. 115; p. 105016 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.01.2023
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0889-1575 1096-0481 |
| DOI | 10.1016/j.jfca.2022.105016 |
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| Abstract | Thiabendazole (TBZ) exposure through food can have substantial long-term health consequences for humans. Herein, SERS coupled with flower-like AgNPs and python-scikit-learn (PSL) algorithms, was proposed for rapid detection of TBZ. Initially, AgNFs with a strong enhancement factor (EF) of 1.303 × 106 were synthesized to collect TBZ spectra. Subsequently, three PSL-based variable selection algorithms, including SelectKBest (SKB), variance threshold (VT) and recursive feature elimination (RFE), were comparatively applied to select the informative variables for TBZ prediction. The RFE exhibited the optimal selection ability, and RFE-SVM achieved the best performance for TBZ prediction (Rp2 = 0.976, RPD = 6.477), with a computed limit of detection (LOD) of 0.24 μg/mL obtained. Finally, good recoveries of spiked samples (78.5–95.09%) were obtained, demonstrating that the proposed method is practicable and potentially effective for TBZ rapidly detection in food.
•AgNFs-based SERS coupled with PSL algorithms for TBZ has proposed.•AgNFs with a strong enhancement factor of 1.303 × 106 were synthesized.•SKB, VT, RFE variable selection methods were comparatively investigated.•RFE-SVM achieved the most accurate prediction of TBZ with RPD of 6.477.•The proposed robust SERS-RFE-SVM method for TBZ obtained a LOD of 0.24 μg/mL. |
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| AbstractList | Thiabendazole (TBZ) exposure through food can have substantial long-term health consequences for humans. Herein, SERS coupled with flower-like AgNPs and python-scikit-learn (PSL) algorithms, was proposed for rapid detection of TBZ. Initially, AgNFs with a strong enhancement factor (EF) of 1.303 × 10⁶ were synthesized to collect TBZ spectra. Subsequently, three PSL-based variable selection algorithms, including SelectKBest (SKB), variance threshold (VT) and recursive feature elimination (RFE), were comparatively applied to select the informative variables for TBZ prediction. The RFE exhibited the optimal selection ability, and RFE-SVM achieved the best performance for TBZ prediction (Rp² = 0.976, RPD = 6.477), with a computed limit of detection (LOD) of 0.24 μg/mL obtained. Finally, good recoveries of spiked samples (78.5–95.09%) were obtained, demonstrating that the proposed method is practicable and potentially effective for TBZ rapidly detection in food. Thiabendazole (TBZ) exposure through food can have substantial long-term health consequences for humans. Herein, SERS coupled with flower-like AgNPs and python-scikit-learn (PSL) algorithms, was proposed for rapid detection of TBZ. Initially, AgNFs with a strong enhancement factor (EF) of 1.303 × 106 were synthesized to collect TBZ spectra. Subsequently, three PSL-based variable selection algorithms, including SelectKBest (SKB), variance threshold (VT) and recursive feature elimination (RFE), were comparatively applied to select the informative variables for TBZ prediction. The RFE exhibited the optimal selection ability, and RFE-SVM achieved the best performance for TBZ prediction (Rp2 = 0.976, RPD = 6.477), with a computed limit of detection (LOD) of 0.24 μg/mL obtained. Finally, good recoveries of spiked samples (78.5–95.09%) were obtained, demonstrating that the proposed method is practicable and potentially effective for TBZ rapidly detection in food. •AgNFs-based SERS coupled with PSL algorithms for TBZ has proposed.•AgNFs with a strong enhancement factor of 1.303 × 106 were synthesized.•SKB, VT, RFE variable selection methods were comparatively investigated.•RFE-SVM achieved the most accurate prediction of TBZ with RPD of 6.477.•The proposed robust SERS-RFE-SVM method for TBZ obtained a LOD of 0.24 μg/mL. |
| ArticleNumber | 105016 |
| Author | Zhou, Wenjie Luo, Xiaofeng Haruna, Suleiman A. Chen, Quansheng Li, Huanhuan |
| Author_xml | – sequence: 1 givenname: Huanhuan surname: Li fullname: Li, Huanhuan – sequence: 2 givenname: Xiaofeng surname: Luo fullname: Luo, Xiaofeng – sequence: 3 givenname: Suleiman A. surname: Haruna fullname: Haruna, Suleiman A. – sequence: 4 givenname: Wenjie surname: Zhou fullname: Zhou, Wenjie – sequence: 5 givenname: Quansheng surname: Chen fullname: Chen, Quansheng email: qschen@ujs.edu.cn |
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| Title | Rapid detection of thiabendazole in food using SERS coupled with flower-like AgNPs and PSL-based variable selection algorithms |
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