Efficient preparation of UCl3 by ZnCl2 mediated chlorination
U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl 2 in LiCl–KCl molten salts. Voltammetric studies indicate the instantaneous formation of UCl 3 by reaction with ZnCl 2 , along with the redox reactions of Zn and U–Zn alloys. Chronoamperometry was found effective f...
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| Published in | Journal of radioanalytical and nuclear chemistry Vol. 322; no. 2; pp. 331 - 336 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cham
Springer International Publishing
01.11.2019
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0236-5731 1588-2780 |
| DOI | 10.1007/s10967-019-06782-5 |
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| Abstract | U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl
2
in LiCl–KCl molten salts. Voltammetric studies indicate the instantaneous formation of UCl
3
by reaction with ZnCl
2
, along with the redox reactions of Zn and U–Zn alloys. Chronoamperometry was found effective for indirect monitoring of U chlorination reaction that occurs chemically in the salt. Inductively coupled plasma-optical emission spectroscopy studies confirm the uniform distribution of UCl
3
product in the salt, and the electrochemically recovered liquid Zn metal settles at the bottom of the reactor. |
|---|---|
| AbstractList | U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl
2
in LiCl–KCl molten salts. Voltammetric studies indicate the instantaneous formation of UCl
3
by reaction with ZnCl
2
, along with the redox reactions of Zn and U–Zn alloys. Chronoamperometry was found effective for indirect monitoring of U chlorination reaction that occurs chemically in the salt. Inductively coupled plasma-optical emission spectroscopy studies confirm the uniform distribution of UCl
3
product in the salt, and the electrochemically recovered liquid Zn metal settles at the bottom of the reactor. U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl2 in LiCl–KCl molten salts. Voltammetric studies indicate the instantaneous formation of UCl3 by reaction with ZnCl2, along with the redox reactions of Zn and U–Zn alloys. Chronoamperometry was found effective for indirect monitoring of U chlorination reaction that occurs chemically in the salt. Inductively coupled plasma-optical emission spectroscopy studies confirm the uniform distribution of UCl3 product in the salt, and the electrochemically recovered liquid Zn metal settles at the bottom of the reactor. |
| Author | Jang, Junhyuk Lee, Chang Hwa Yoon, Dalsung Lee, Sung-Jai Kim, Gha-Young Kim, Tack-Jin |
| Author_xml | – sequence: 1 givenname: Chang Hwa orcidid: 0000-0002-4624-5738 surname: Lee fullname: Lee, Chang Hwa email: chwalee@kaeri.re.kr organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute – sequence: 2 givenname: Tack-Jin surname: Kim fullname: Kim, Tack-Jin organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute – sequence: 3 givenname: Dalsung surname: Yoon fullname: Yoon, Dalsung organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute – sequence: 4 givenname: Junhyuk surname: Jang fullname: Jang, Junhyuk organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute – sequence: 5 givenname: Gha-Young surname: Kim fullname: Kim, Gha-Young organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute – sequence: 6 givenname: Sung-Jai surname: Lee fullname: Lee, Sung-Jai organization: Nuclear Fuel Cycle Process Development Division, Korea Atomic Energy Research Institute |
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| Cites_doi | 10.13182/NT09-A7404 10.1179/174328509X431463 10.1007/s10967-017-5368-x 10.1016/j.egypro.2011.06.051 10.1016/0149-1970(96)00007-8 10.1016/j.jallcom.2007.02.104 10.1149/1.1901083 10.1016/0022-5088(75)90180-0 10.1007/s10967-018-5953-7 10.1039/tf9595501904 10.1007/s10967-017-5359-y 10.1149/1.2069109 |
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| Keywords | Electrorefining Uranium chlorination Chronoamperometry ZnCl UCl |
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| References | Tomczuk, Ackerman, Wolson, Miller (CR3) 1992; 139 CR6 Kim, Kim, Jang, Eun, Lee (CR16) 2017; 314 CR8 Shirai, Nagai, Uehara, Yamana (CR18) 2008; 456 Masset, Bottomley, Konings, Malmbeck, Rodrigues, Serp, Glatz (CR12) 2005; 152 CR9 Hait, Jana, Sanyal (CR1) 2009; 118 Li, Vaden, Westphal, Fredrickson, Benedict, Johnson (CR10) 2009; 166 Eun, Kim, Jang, Kim, Lee, Hur (CR13) 2017; 314 Bindra, White, Mallory, Hajdu (CR14) 1990 Chiotti, Mason (CR15) 1975; 40 Lee, Hur, Kim, Ahn, Cho, Paek (CR4) 2011; 7 Inman, Hills, Young, Bockris (CR7) 1959; 55 Lambert, Kerry, Sharrad (CR11) 2018; 317 Popov, Djokic, Grgur (CR2) 2002 Laidler, Battles, Miller, Ackerman, Carls (CR5) 1997; 31 Plambeck, Bard (CR17) 1976 O Shirai (6782_CR18) 2008; 456 JJ Laidler (6782_CR5) 1997; 31 P Masset (6782_CR12) 2005; 152 D Inman (6782_CR7) 1959; 55 H Lee (6782_CR4) 2011; 7 P Bindra (6782_CR14) 1990 H Lambert (6782_CR11) 2018; 317 6782_CR6 Z Tomczuk (6782_CR3) 1992; 139 6782_CR9 J Hait (6782_CR1) 2009; 118 GY Kim (6782_CR16) 2017; 314 6782_CR8 (6782_CR17) 1976 SX Li (6782_CR10) 2009; 166 KI Popov (6782_CR2) 2002 HC Eun (6782_CR13) 2017; 314 P Chiotti (6782_CR15) 1975; 40 |
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| Snippet | U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl
2
in LiCl–KCl molten salts. Voltammetric studies indicate the... U chlorination is demonstrated using electrochemical and chemical reactions with ZnCl2 in LiCl–KCl molten salts. Voltammetric studies indicate the... |
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| SubjectTerms | Chemical reactions Chemistry Chemistry and Materials Science Chlorination Diagnostic Radiology Emission analysis Hadrons Heavy Ions Inductively coupled plasma Inorganic Chemistry Lithium chloride Molten salts Nuclear Chemistry Nuclear Physics Optical emission spectroscopy Organic chemistry Physical Chemistry Plasma Redox reactions Zinc chloride |
| Title | Efficient preparation of UCl3 by ZnCl2 mediated chlorination |
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