Air-assisted solvent terminated dispersive liquid–liquid microextraction (AA-ST-DLLME) for the determination of lead in water and beverage samples by graphite furnace atomic absorption spectrometry
[Display omitted] •A novel hybrid AA-ST-DLLME was developed for Pb determination.•Home fish-tank pump for AA-ST-DLLME was used as bubble generator.•Centrifugation step was eliminated by termination step.•AA-ST-DLLME was applied to Pb determination in water, fruit juice, and beverage. A preconcentrat...
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| Published in | Microchemical journal Vol. 162; p. 105828 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.03.2021
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0026-265X 1095-9149 |
| DOI | 10.1016/j.microc.2020.105828 |
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| Abstract | [Display omitted]
•A novel hybrid AA-ST-DLLME was developed for Pb determination.•Home fish-tank pump for AA-ST-DLLME was used as bubble generator.•Centrifugation step was eliminated by termination step.•AA-ST-DLLME was applied to Pb determination in water, fruit juice, and beverage.
A preconcentration method based on a novel hybrid air-assisted solvent terminated dispersive liquid–liquid microextraction (AA-ST-DLLME) using a domestic fish-tank pump as a bubble generator was developed for the determination of Pb in water and beverage samples by GFAAS. The important parameters for the microextraction process (pH, concentration of complexing agent, type of extracting solvent, type of disperser, type of demulsifier, air-assisted time, and extraction time) were optimized. Under the optimized conditions, the enrichment factor (EF) of 58.9 was achieved, with the preconcentration factor (PF) of 60.0 and the extraction efficiency of 98.2%. The limit of detection (LOD) and limit of quantitation (LOQ) were 0.025 ng/mL and 0.084 ng/mL, respectively. The relative standard deviation (RSD) was 1.02–3.19%. The proposed method was applied for the determination of trace level of Pb in water, fruit juice, and beverage samples. The spiked recovery at three different spiked concentrations were 82.0–117.3%. Results from the analysis of standard reference materials (SLRS-6) were not significantly different at the 95% of confidence level. |
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| AbstractList | [Display omitted]
•A novel hybrid AA-ST-DLLME was developed for Pb determination.•Home fish-tank pump for AA-ST-DLLME was used as bubble generator.•Centrifugation step was eliminated by termination step.•AA-ST-DLLME was applied to Pb determination in water, fruit juice, and beverage.
A preconcentration method based on a novel hybrid air-assisted solvent terminated dispersive liquid–liquid microextraction (AA-ST-DLLME) using a domestic fish-tank pump as a bubble generator was developed for the determination of Pb in water and beverage samples by GFAAS. The important parameters for the microextraction process (pH, concentration of complexing agent, type of extracting solvent, type of disperser, type of demulsifier, air-assisted time, and extraction time) were optimized. Under the optimized conditions, the enrichment factor (EF) of 58.9 was achieved, with the preconcentration factor (PF) of 60.0 and the extraction efficiency of 98.2%. The limit of detection (LOD) and limit of quantitation (LOQ) were 0.025 ng/mL and 0.084 ng/mL, respectively. The relative standard deviation (RSD) was 1.02–3.19%. The proposed method was applied for the determination of trace level of Pb in water, fruit juice, and beverage samples. The spiked recovery at three different spiked concentrations were 82.0–117.3%. Results from the analysis of standard reference materials (SLRS-6) were not significantly different at the 95% of confidence level. |
| ArticleNumber | 105828 |
| Author | Udnan, Yuthapong Ampiah-Bonney, Richmond J. Chaiyasith, Wipharat Chuachuad Chaikhan, Pilaipan |
| Author_xml | – sequence: 1 givenname: Pilaipan surname: Chaikhan fullname: Chaikhan, Pilaipan organization: Department of Chemistry, Faculty of Science, Naresuan University, Phitsanulok 65000, Thailand – sequence: 2 givenname: Yuthapong surname: Udnan fullname: Udnan, Yuthapong organization: Department of Chemistry, Faculty of Science, Naresuan University, Phitsanulok 65000, Thailand – sequence: 3 givenname: Richmond J. surname: Ampiah-Bonney fullname: Ampiah-Bonney, Richmond J. organization: Department of Chemistry, A205 Science Center, Amherst College, Amherst, MA 01002-5000, USA – sequence: 4 givenname: Wipharat Chuachuad surname: Chaiyasith fullname: Chaiyasith, Wipharat Chuachuad email: wipharatc@nu.ac.th organization: Department of Chemistry, Faculty of Science, Naresuan University, Phitsanulok 65000, Thailand |
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| Title | Air-assisted solvent terminated dispersive liquid–liquid microextraction (AA-ST-DLLME) for the determination of lead in water and beverage samples by graphite furnace atomic absorption spectrometry |
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