Raspberry-structured silver-carbon hybrid nanoparticle clusters for high-performance capacitive deionization
An aerosol-based synthetic approach, in combination with a real-time characterization method using differential ion-mobility analyses coupled to temperature-programmed Fourier-transform infrared spectroscopy (DMA/TP-FTIR), was demonstrated for the development of raspberry-structured Ag‑carbon hybrid...
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| Published in | Desalination Vol. 520; p. 115343 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.12.2021
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0011-9164 1873-4464 |
| DOI | 10.1016/j.desal.2021.115343 |
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| Abstract | An aerosol-based synthetic approach, in combination with a real-time characterization method using differential ion-mobility analyses coupled to temperature-programmed Fourier-transform infrared spectroscopy (DMA/TP-FTIR), was demonstrated for the development of raspberry-structured Ag‑carbon hybrid nanoparticle clusters (Ag-C-NPC). Physical size, number concentration, and compositions of the Ag-C-NPC were shown to be successfully characterized directly in the aerosol state on a quantitative basis. Remarkable high salt adsorption capacity (15.6 mg/g), good charging/discharging stability, and low requirement of cell voltage were attainable by using the Ag nanoparticle-decorated carbon nanoparticle clusters as the positive electrode material. This work provides a proof of concept of using the aerosol-based synthesis, with the support of in-situ characterization, for the development of AgC nanocomposite clusters to achieve high CDI performance. The method also shows promise for the tuning of the material properties of Ag-C-NPC for the optimization of the CDI capacity and cyclic stability useful for a variety of the water desalination applications (e.g., brackish water).
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•Ag-carbon nanoparticle clusters as positive electrode via aerosol-based synthesis.•Direct gas-phase coupled characterization supports the aerosol-based synthesis.•Successful quantitative characterization of the Ag-C-NPC in aerosol state.•Remarkable high capacity (15.6 mg/g) and stability with a low cell voltage. |
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| AbstractList | An aerosol-based synthetic approach, in combination with a real-time characterization method using differential ion-mobility analyses coupled to temperature-programmed Fourier-transform infrared spectroscopy (DMA/TP-FTIR), was demonstrated for the development of raspberry-structured Ag‑carbon hybrid nanoparticle clusters (Ag-C-NPC). Physical size, number concentration, and compositions of the Ag-C-NPC were shown to be successfully characterized directly in the aerosol state on a quantitative basis. Remarkable high salt adsorption capacity (15.6 mg/g), good charging/discharging stability, and low requirement of cell voltage were attainable by using the Ag nanoparticle-decorated carbon nanoparticle clusters as the positive electrode material. This work provides a proof of concept of using the aerosol-based synthesis, with the support of in-situ characterization, for the development of AgC nanocomposite clusters to achieve high CDI performance. The method also shows promise for the tuning of the material properties of Ag-C-NPC for the optimization of the CDI capacity and cyclic stability useful for a variety of the water desalination applications (e.g., brackish water).
[Display omitted]
•Ag-carbon nanoparticle clusters as positive electrode via aerosol-based synthesis.•Direct gas-phase coupled characterization supports the aerosol-based synthesis.•Successful quantitative characterization of the Ag-C-NPC in aerosol state.•Remarkable high capacity (15.6 mg/g) and stability with a low cell voltage. |
| ArticleNumber | 115343 |
| Author | Tsai, De-Hao Hu, Chi-Chang Chiang, Meng-Ting Tu, Yi-Heng Chiang, Hsin-Li |
| Author_xml | – sequence: 1 givenname: Meng-Ting surname: Chiang fullname: Chiang, Meng-Ting – sequence: 2 givenname: Yi-Heng surname: Tu fullname: Tu, Yi-Heng – sequence: 3 givenname: Hsin-Li surname: Chiang fullname: Chiang, Hsin-Li – sequence: 4 givenname: Chi-Chang surname: Hu fullname: Hu, Chi-Chang email: cchu@che.nthu.edu.tw – sequence: 5 givenname: De-Hao surname: Tsai fullname: Tsai, De-Hao email: dhtsai@mx.nthu.edu.tw |
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