Fast analysis of nine PAHs in beer by ultrasound-vortex-assisted dispersive liquid-liquid micro-extraction coupled with gas chromatography-ion trap mass spectrometry
An Ultrasound-Vortex-Assisted Dispersive Liquid-Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons (fluorene, phenanthrene, anthracene, fluoranthene, pyrene, ch...
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| Published in | RSC advances Vol. 6; no. 17; pp. 1392 - 13927 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.01.2016
|
| Subjects | |
| Online Access | Get full text |
| ISSN | 2046-2069 2046-2069 |
| DOI | 10.1039/c5ra24873f |
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| Abstract | An Ultrasound-Vortex-Assisted Dispersive Liquid-Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons (fluorene, phenanthrene, anthracene, fluoranthene, pyrene, chrysene, benzo(
b
)fluoranthene, benzo(
a
)pyrene and benzoperylene) in beer (alcohol by volume ≤7%). Among 5 possible extraction solvents tested, dichloromethane, density 1.325 g mL
−1
at 25 °C, was selected for method development. Parameters such as extraction solvent type and volume, extraction time and pH, and NaCl concentration were optimized. Under optimal conditions, the enrichment factors of the nine analytes range between 100 and 200 fold, the recoveries from 83% to 99% and the correlation coefficients from 0.9982 to 0.9999. The limit of detection (LOD) and limit of quantification (LOQ) are ≥3.8 pg μL
−1
and ≥9.8 pg μL
−1
, respectively. The precision expressed as relative standard deviation (RSD), is ≤4.0%. The whole proposed methodology was demonstrated to be simple, reproducible and sensitive for the determination of trace PAHs in beer samples.
An Ultrasound-Vortex-Assisted Dispersive Liquid-Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons in beer. |
|---|---|
| AbstractList | An Ultrasound-Vortex-Assisted Dispersive Liquid–Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons (fluorene, phenanthrene, anthracene, fluoranthene, pyrene, chrysene, benzo(b)fluoranthene, benzo(a)pyrene and benzoperylene) in beer (alcohol by volume ≤7%). Among 5 possible extraction solvents tested, dichloromethane, density 1.325 g mL⁻¹ at 25 °C, was selected for method development. Parameters such as extraction solvent type and volume, extraction time and pH, and NaCl concentration were optimized. Under optimal conditions, the enrichment factors of the nine analytes range between 100 and 200 fold, the recoveries from 83% to 99% and the correlation coefficients from 0.9982 to 0.9999. The limit of detection (LOD) and limit of quantification (LOQ) are ≥3.8 pg μL⁻¹ and ≥9.8 pg μL⁻¹, respectively. The precision expressed as relative standard deviation (RSD), is ≤4.0%. The whole proposed methodology was demonstrated to be simple, reproducible and sensitive for the determination of trace PAHs in beer samples. An Ultrasound-Vortex-Assisted Dispersive Liquid-Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons (fluorene, phenanthrene, anthracene, fluoranthene, pyrene, chrysene, benzo( b )fluoranthene, benzo( a )pyrene and benzoperylene) in beer (alcohol by volume ≤7%). Among 5 possible extraction solvents tested, dichloromethane, density 1.325 g mL −1 at 25 °C, was selected for method development. Parameters such as extraction solvent type and volume, extraction time and pH, and NaCl concentration were optimized. Under optimal conditions, the enrichment factors of the nine analytes range between 100 and 200 fold, the recoveries from 83% to 99% and the correlation coefficients from 0.9982 to 0.9999. The limit of detection (LOD) and limit of quantification (LOQ) are ≥3.8 pg μL −1 and ≥9.8 pg μL −1 , respectively. The precision expressed as relative standard deviation (RSD), is ≤4.0%. The whole proposed methodology was demonstrated to be simple, reproducible and sensitive for the determination of trace PAHs in beer samples. An Ultrasound-Vortex-Assisted Dispersive Liquid-Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons in beer. An Ultrasound-Vortex-Assisted Dispersive Liquid–Liquid Micro-Extraction (USVADLLME) procedure coupled with Gas Chromatography-Ion Trap Mass Spectrometry (GC-IT/MS) is proposed for the fast analysis of nine polycyclic aromatic hydrocarbons (fluorene, phenanthrene, anthracene, fluoranthene, pyrene, chrysene, benzo( b )fluoranthene, benzo( a )pyrene and benzoperylene) in beer (alcohol by volume ≤7%). Among 5 possible extraction solvents tested, dichloromethane, density 1.325 g mL −1 at 25 °C, was selected for method development. Parameters such as extraction solvent type and volume, extraction time and pH, and NaCl concentration were optimized. Under optimal conditions, the enrichment factors of the nine analytes range between 100 and 200 fold, the recoveries from 83% to 99% and the correlation coefficients from 0.9982 to 0.9999. The limit of detection (LOD) and limit of quantification (LOQ) are ≥3.8 pg μL −1 and ≥9.8 pg μL −1 , respectively. The precision expressed as relative standard deviation (RSD), is ≤4.0%. The whole proposed methodology was demonstrated to be simple, reproducible and sensitive for the determination of trace PAHs in beer samples. |
| Author | Russo, Mario Vincenzo Perugini, Luisa Notardonato, Ivan Avino, Pasquale |
| AuthorAffiliation | INAIL Research Area Dipartimento Agricoltura Ambiente e Alimenti DIT Università del Molise |
| AuthorAffiliation_xml | – sequence: 0 name: DIT – sequence: 0 name: Ambiente e Alimenti – sequence: 0 name: INAIL Research Area – sequence: 0 name: Università del Molise – sequence: 0 name: Dipartimento Agricoltura |
| Author_xml | – sequence: 1 givenname: Mario Vincenzo surname: Russo fullname: Russo, Mario Vincenzo – sequence: 2 givenname: Pasquale surname: Avino fullname: Avino, Pasquale – sequence: 3 givenname: Luisa surname: Perugini fullname: Perugini, Luisa – sequence: 4 givenname: Ivan surname: Notardonato fullname: Notardonato, Ivan |
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| CitedBy_id | crossref_primary_10_3390_foods12030454 crossref_primary_10_1016_j_jfca_2021_103888 crossref_primary_10_1016_j_trac_2017_09_005 crossref_primary_10_1016_j_microc_2017_03_052 crossref_primary_10_1002_sscp_201800089 crossref_primary_10_1007_s10337_017_3403_2 crossref_primary_10_3390_app10165441 crossref_primary_10_3390_app9142945 crossref_primary_10_1007_s12161_019_01602_8 crossref_primary_10_1016_j_chroma_2016_10_058 crossref_primary_10_1007_s12161_016_0783_0 crossref_primary_10_1039_C6RA24682F crossref_primary_10_1016_j_foodcont_2021_108104 crossref_primary_10_1080_05704928_2016_1224240 crossref_primary_10_1007_s44211_023_00274_z crossref_primary_10_1002_jsfa_9279 crossref_primary_10_1002_jssc_202200365 crossref_primary_10_1016_j_chroma_2024_465257 |
| Cites_doi | 10.1021/jf048633a 10.1093/chromsci/23.9.422 10.1016/S0140-6736(00)02172-3 10.1016/j.jfca.2004.06.014 10.1039/C4RA08574D 10.1021/jf404966w 10.1021/jf991205y 10.1016/S0278-6915(00)00158-7 10.1021/jf00118a049 10.1002/em.20095 10.1016/j.foodchem.2013.09.064 10.1002/jhrc.1240080911 10.1016/S0378-4347(01)00438-8 10.1016/S0021-9673(00)94677-6 10.1007/BF02492909 10.1016/S0021-9673(01)95934-5 10.1016/0015-6264(79)90323-7 10.1007/BF02490698 10.1007/s00216-012-6205-2 10.1007/BF01192725 10.1007/s00216-011-5551-9 10.1039/C4AY00926F 10.1039/C5RA01916H 10.1016/j.trac.2006.05.010 10.1016/j.chroma.2010.07.079 10.1039/C3AY41641K 10.1016/S1383-5742(99)00016-2 10.1016/S0021-9673(96)00522-5 10.1016/S0308-8146(03)00257-7 10.1016/0039-9140(81)80043-4 10.1002/jhrc.1240130206 10.1515/REVEH.1997.12.3.133 10.1080/10826079608007196 10.1016/S0021-9673(01)87181-8 10.4324/9780203309124 10.1016/j.aca.2013.01.031 10.5897/AJFS2014.1227 |
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| SubjectTerms | anthracenes beers benzo(a)pyrene chemical species detection limit fluorenes mass spectrometry methylene chloride microextraction phenanthrenes sodium chloride solvents standard deviation |
| Title | Fast analysis of nine PAHs in beer by ultrasound-vortex-assisted dispersive liquid-liquid micro-extraction coupled with gas chromatography-ion trap mass spectrometry |
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| Volume | 6 |
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