Coordination behavior of N-benzoylamino acids: Synthesis and structure of mixed-ligand complexes of palladium(Ⅱ) with N-benzoylamino acid dianion and diamine
Four new mixed-ligand complexes of pailadiumt(Ⅱ) with L1(N-benzoyl-α-amino acid dianion) and L2[ethyldiamine (en),2,2’-bipyridine (Bpy) and 1,10-phenanthroline (Phen)] were synthesized.Ail the complexes have been characterized by elemental analyses,molar conductance,infrared and 1H NMR spectra and t...
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| Published in | Science China. Chemistry Vol. 40; no. 6; pp. 600 - 607 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
Springer Nature B.V
01.12.1997
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1674-7291 1006-9291 1869-1870 1862-2771 |
| DOI | 10.1007/BF02875478 |
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| Abstract | Four new mixed-ligand complexes of pailadiumt(Ⅱ) with L1(N-benzoyl-α-amino acid dianion) and L2[ethyldiamine (en),2,2’-bipyridine (Bpy) and 1,10-phenanthroline (Phen)] were synthesized.Ail the complexes have been characterized by elemental analyses,molar conductance,infrared and 1H NMR spectra and therme-gravimetric analyses.Crystal structures of [Pd(Bpy)(Bzval-N,O)] and [Pd(en) (Bzphe-N,O)] H2O have been do termmed by X-ray diffraction analysis.The results indicate that in all the complexes hgand L1 coordinates to palladium (Ⅱ) through deprotonated amide nitrogen and carboxylic oxygen,and there are some intramolecular nonrovalent in teractions in the complexes. |
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| AbstractList | Four new mixed-ligand complexes of palladium (II) with L1 (N-benwyl-α-amino acid dianion) and L2 [ethyldiamine (en), 2. 2′-bipyridine (Bpy) and 1.10-phenanthroline (Phen)] were synthesized. All the complexes have been characterized by elemental analyses, molar conductance, infrared and1H NMR spectra and thermo-gravimetric analyses. Crystal structures of [Pd(Bpy)(Bzval-N, O)] and [Pd(en)(Bzphe-N, O) ·H2O have been determined by X-ray diffraction analysis. The results indicate that in all the complexes’ ligand L1 coordinates to palladium (II) through deprotonated amide nitrogen and carboxylic oxygen, and there are some intramolecular noncovalent interactions in the complexes. Four new mixed-ligand complexes of pailadiumt(Ⅱ) with L1(N-benzoyl-α-amino acid dianion) and L2[ethyldiamine (en),2,2’-bipyridine (Bpy) and 1,10-phenanthroline (Phen)] were synthesized.Ail the complexes have been characterized by elemental analyses,molar conductance,infrared and 1H NMR spectra and therme-gravimetric analyses.Crystal structures of [Pd(Bpy)(Bzval-N,O)] and [Pd(en) (Bzphe-N,O)] H2O have been do termmed by X-ray diffraction analysis.The results indicate that in all the complexes hgand L1 coordinates to palladium (Ⅱ) through deprotonated amide nitrogen and carboxylic oxygen,and there are some intramolecular nonrovalent in teractions in the complexes. |
| Author | 龚钰秋 陈耀峰 顾建明 胡秀荣 |
| AuthorAffiliation | Department of Chemistry Hangzhou University Hangzhou 310028 China Department of Polymer Science and Engineering Zhejiang University Hangzhou 310027 Central Laboratory China |
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| Notes | GONG Yuqiu(Department of Chemistry,Hangzhou University,Hangzhou 310028,China)CHEN Yaofeng(Department of Polymer Science and Engineering,Zhejiang University,Hangzhou 310027,China)GU Jianming and HU Xiurong(Central Laboratory,Hangzhou University,Hangzhou 310028,China) 11-5839/O6 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 |
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| References | L. Antolini (BF02875478_CR3) 1984; 23 L. Menabue (BF02875478_CR4) 1990; 29 H. Sigel (BF02875478_CR1) 1982; 82 E. Dubler (BF02875478_CR13) 1984; 23 T. G. Appleton (BF02875478_CR6) 1989; 28 H. Sigel (BF02875478_CR12) 1977; 99 J. L. Burmeister (BF02875478_CR11) 1964; 3 BF02875478_CR5 R. E. Steiger (BF02875478_CR8) 1944; 9 J. R. Mohring (BF02875478_CR9) 1976; 53 L. Antolini (BF02875478_CR2) 1982; 21 T. G. Appleton (BF02875478_CR7) 1994; 33 BF02875478_CR10 BF02875478_CR14 |
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| SubjectTerms | acid amide Amino acids Anions complexes containing deprotonated Diamines group Infrared analysis Infrared spectra interaction intramolecular Ligands molecular N-benzoyl-a-amino Nitrogen NMR noncovalent Nuclear magnetic resonance Palladium palladium(II) structure |
| Title | Coordination behavior of N-benzoylamino acids: Synthesis and structure of mixed-ligand complexes of palladium(Ⅱ) with N-benzoylamino acid dianion and diamine |
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