Biosynthesis of MgAl2O4 nanoparticles and their use as photocatalyst for sunlight-driven degradation of Amido-Black
Magnesium aluminate MgAl2O4, known as spinel, has been the subject of intense research due to its excellent thermal, optical, and dielectric characteristics. In this work, a green synthesis process that is eco-friendly, easy, and of low cost is used to prepare MgAl2O4 nanoparticles. The structural,...
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| Published in | Solid state communications Vol. 404; p. 116044 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2025
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0038-1098 |
| DOI | 10.1016/j.ssc.2025.116044 |
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| Abstract | Magnesium aluminate MgAl2O4, known as spinel, has been the subject of intense research due to its excellent thermal, optical, and dielectric characteristics. In this work, a green synthesis process that is eco-friendly, easy, and of low cost is used to prepare MgAl2O4 nanoparticles. The structural, morphological, and optical properties of the MgAl2O4 spinel were studied by different techniques, such as X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller surface area analyzer (BET), UV–visible spectroscopy, and Fourier transform-infrared spectroscopy (FT-IR). The XRD patterns indicate the formation of the MgAl2O4 cubic phase, and the average size of nanoparticles is around 17 nm. TEM images confirmed the pure phase and the nanosize of the particles. The UV–vis absorption spectrum of the MgAl2O4 spinel showed an absorption peak at around 230 nm, and the optical band gap energy was found to be 3.92 eV. Surface analysis was conducted using BET isotherms, demonstrating a specific surface area of 58 m2 g−1 and a 5–10 nm pore size. The dielectric properties of MgAl2O4 spinel were studied using the complex impedance spectroscopy technique over a frequency range from 1 Hz to 13 MHz and a temperature range from 648 to 873 K. The temperature and frequency dependence of the material properties was demonstrated, and the activation energy was also calculated. The photocatalytic activity of MgAl2O4 was investigated for the degradation of the Amido Black 10B dye under sunlight irradiation. The dye was effectively decomposed by ca. 98 % under solar light irradiation within ca. 5 h, with pseudo-first-order rate constants of 7.99 10−3 min−1.
•Nano-MgAl2O4 was elaborated by the ecologically Bio-synthesizes technique.•Dye-sensitized NPs extend photocatalysis activity towards sunlight.•Excellent photocatalytic activity in degrading the azo dye Amido Black. |
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| AbstractList | Magnesium aluminate MgAl2O4, known as spinel, has been the subject of intense research due to its excellent thermal, optical, and dielectric characteristics. In this work, a green synthesis process that is eco-friendly, easy, and of low cost is used to prepare MgAl2O4 nanoparticles. The structural, morphological, and optical properties of the MgAl2O4 spinel were studied by different techniques, such as X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller surface area analyzer (BET), UV–visible spectroscopy, and Fourier transform-infrared spectroscopy (FT-IR). The XRD patterns indicate the formation of the MgAl2O4 cubic phase, and the average size of nanoparticles is around 17 nm. TEM images confirmed the pure phase and the nanosize of the particles. The UV–vis absorption spectrum of the MgAl2O4 spinel showed an absorption peak ataround 230 nm, and the optical band gap energy was found to be 3.92 eV. Surface analysis was conducted using BET isotherms, demonstrating a specific surface area of 58 m2 g-1 and a 5–10 nm pore size. The dielectric properties of MgAl2O4 spinel were studied using the complex impedance spectroscopy technique over a frequency range from 1 Hz to 13 MHz and a temperature range from 648 to 873 K. The temperature and frequency dependence of the material properties was demonstrated, and the activation energy was also calculated. The photocatalytic activity of MgAl2O4 was investigated for the degradation of the Amido Black 10B dye under sunlight irradiation. The dye was effectively decomposed by ca. 98 % under solar light irradiation within ca. 5 h, with pseudo-first-order rate constants of 7.99 10-3 min-1. Magnesium aluminate MgAl2O4, known as spinel, has been the subject of intense research due to its excellent thermal, optical, and dielectric characteristics. In this work, a green synthesis process that is eco-friendly, easy, and of low cost is used to prepare MgAl2O4 nanoparticles. The structural, morphological, and optical properties of the MgAl2O4 spinel were studied by different techniques, such as X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller surface area analyzer (BET), UV–visible spectroscopy, and Fourier transform-infrared spectroscopy (FT-IR). The XRD patterns indicate the formation of the MgAl2O4 cubic phase, and the average size of nanoparticles is around 17 nm. TEM images confirmed the pure phase and the nanosize of the particles. The UV–vis absorption spectrum of the MgAl2O4 spinel showed an absorption peak at around 230 nm, and the optical band gap energy was found to be 3.92 eV. Surface analysis was conducted using BET isotherms, demonstrating a specific surface area of 58 m2 g−1 and a 5–10 nm pore size. The dielectric properties of MgAl2O4 spinel were studied using the complex impedance spectroscopy technique over a frequency range from 1 Hz to 13 MHz and a temperature range from 648 to 873 K. The temperature and frequency dependence of the material properties was demonstrated, and the activation energy was also calculated. The photocatalytic activity of MgAl2O4 was investigated for the degradation of the Amido Black 10B dye under sunlight irradiation. The dye was effectively decomposed by ca. 98 % under solar light irradiation within ca. 5 h, with pseudo-first-order rate constants of 7.99 10−3 min−1. •Nano-MgAl2O4 was elaborated by the ecologically Bio-synthesizes technique.•Dye-sensitized NPs extend photocatalysis activity towards sunlight.•Excellent photocatalytic activity in degrading the azo dye Amido Black. |
| ArticleNumber | 116044 |
| Author | Schneider, Raphaël Zouaoui, Mouldi Chouchene, Bilel Ben Ameur, Wiem Hajjaji, Anouar |
| Author_xml | – sequence: 1 givenname: Wiem surname: Ben Ameur fullname: Ben Ameur, Wiem organization: Laboratory of Physics of Materials – Structure and Properties LR01ES15, Department of Physics, Faculty of Sciences of Bizerte, University of Carthage, Zarzouna, 7021, Tunisia – sequence: 2 givenname: Bilel surname: Chouchene fullname: Chouchene, Bilel organization: University of Lorraine, CNRS, LRGP, F-54000, Nancy, France – sequence: 3 givenname: Raphaël surname: Schneider fullname: Schneider, Raphaël organization: University of Lorraine, CNRS, LRGP, F-54000, Nancy, France – sequence: 4 givenname: Anouar surname: Hajjaji fullname: Hajjaji, Anouar organization: Photovoltaic Laboratory, Energy Research and Technology Center, Borj-Cédria Technopole, BP 95, Hammam-Lif, 2050, Tunisia – sequence: 5 givenname: Mouldi orcidid: 0000-0003-1059-0596 surname: Zouaoui fullname: Zouaoui, Mouldi email: zouaoui.mouldi@fsb.u-carthage.tn organization: Laboratory of Physics of Materials – Structure and Properties LR01ES15, Department of Physics, Faculty of Sciences of Bizerte, University of Carthage, Zarzouna, 7021, Tunisia |
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| Keywords | MgAl2O4 nanoparticles Biosynthesis Black amido Photocatalysis MgAl2O4 |
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| Title | Biosynthesis of MgAl2O4 nanoparticles and their use as photocatalyst for sunlight-driven degradation of Amido-Black |
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