Mechanical alloying characteristic and thermal stability of Al78Fe20Zr2 amorphous powders
The powders of pure Al, Fe, and Zr for preparing Al78Fe20Zr2 were subject to a high-energy planetary ball milling.The microstructure evolution of the mixtures at the different intervals of milling was characterized by X-ray diffraction（XRD）, transmission electron microscopy（TEM） and differential sca...
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| Published in | Rare metals Vol. 29; no. 2; pp. 226 - 229 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Beijing
University of Science and Technology Beijing
01.04.2010
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1001-0521 1867-7185 |
| DOI | 10.1007/s12598-010-0039-x |
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| Abstract | The powders of pure Al, Fe, and Zr for preparing Al78Fe20Zr2 were subject to a high-energy planetary ball milling.The microstructure evolution of the mixtures at the different intervals of milling was characterized by X-ray diffraction（XRD）, transmission electron microscopy（TEM） and differential scanning calorimetry（DSC）.It was found that a nearly complete amorphization could be achieved in the mixtures after ball milling for 23 h.Further ball milling led to the crystallization of the amorphous powders.A long time ball milling, e.g., 160 h, led to a complete crystallization of the amorphous powders and the formation of Al3Zr and Al13Fe4.The crystallization products caused by ball milling are almost the same as that produced by isothermal annealing of the amorphous powders in vacuum at 800 K for 1 h. |
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| AbstractList | The powders of pure Al, Fe, and Zr for preparing Al78Fe20Zr2 were subject to a high-energy planetary ball milling.The microstructure evolution of the mixtures at the different intervals of milling was characterized by X-ray diffraction（XRD）, transmission electron microscopy（TEM） and differential scanning calorimetry（DSC）.It was found that a nearly complete amorphization could be achieved in the mixtures after ball milling for 23 h.Further ball milling led to the crystallization of the amorphous powders.A long time ball milling, e.g., 160 h, led to a complete crystallization of the amorphous powders and the formation of Al3Zr and Al13Fe4.The crystallization products caused by ball milling are almost the same as that produced by isothermal annealing of the amorphous powders in vacuum at 800 K for 1 h. The powders of pure Al, Fe, and Zr for preparing Al 78 Fe 20 Zr 2 were subject to a high-energy planetary ball milling. The microstructure evolution of the mixtures at the different intervals of milling was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and differential scanning calorimetry (DSC). It was found that a nearly complete amorphization could be achieved in the mixtures after ball milling for 23 h. Further ball milling led to the crystallization of the amorphous powders. A long time ball milling, e.g., 160 h, led to a complete crystallization of the amorphous powders and the formation of Al 3 Zr and Al1 3 Fe 4 . The crystallization products caused by ball milling are almost the same as that produced by isothermal annealing of the amorphous powders in vacuum at 800 K for 1 h. |
| Author | ZHOU Shuzhu WANG Wenwu |
| AuthorAffiliation | School of Metallurgical Engineering, Hunan University of Technology, Zhuzhou 412008, China Key Laboratory of Low Dimensional Materials ＆ Application Technology（Ministry of Education）, Xiangtan University, Xiangtan 411105, China |
| Author_xml | – sequence: 1 givenname: Shuzhu surname: Zhou fullname: Zhou, Shuzhu organization: School of Metallurgical Engineering, Hunan University of Technology – sequence: 2 givenname: Wenwu surname: Wang fullname: Wang, Wenwu email: www_577@hotmail.com organization: School of Metallurgical Engineering, Hunan University of Technology, Key Laboratory of Low Dimensional Materials & Application Technology (Ministry of Education), Xiangtan University |
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| Cites_doi | 10.1016/S0079-6425(99)00010-9 10.1023/A:1013577605806 10.1016/S0079-6425(98)00005-X 10.1016/S0965-9773(99)00202-0 10.1007/BF00544486 10.1016/0965-9773(95)00251-9 10.1007/BF00363438 10.2464/jilm.51.28 10.1016/S0025-5408(01)00804-2 10.1007/BF02670624 10.1016/0921-5093(95)10002-4 10.1016/S0025-5408(02)00762-6 10.1016/j.msea.2007.02.016 10.1016/S0921-5093(97)00041-5 10.2320/matertrans1989.37.1061 |
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| Snippet | The powders of pure Al, Fe, and Zr for preparing Al78Fe20Zr2 were subject to a high-energy planetary ball milling.The microstructure evolution of the mixtures... The powders of pure Al, Fe, and Zr for preparing Al 78 Fe 20 Zr 2 were subject to a high-energy planetary ball milling. The microstructure evolution of the... |
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| SubjectTerms | Biomaterials Chemistry and Materials Science Energy Materials Engineering Materials Science Mechanical alloying Metallic Materials Nanoscale Science and Technology Physical Chemistry Thermal stability 差示扫描量热法 无定形粉末 机械合金化 热稳定性 行星球磨 透射电子显微镜 非晶粉末 |
| Title | Mechanical alloying characteristic and thermal stability of Al78Fe20Zr2 amorphous powders |
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