Solid / Liquid Interfacial Structures, Surface Forces, and Rheology of Colloidal Dispersions Comprised of Silica Particles Suspended in Liquid Epoxy Resins
In the present study, we have investigated the liquid resin composite consisted of an epoxy resin, an epoxy resin curing agent, a filler of silica particles, and a particle surface modifier of silane coupling agent at different temperatures, using atomic force microscopy and rheometry. Particular fo...
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Published in | Funtai Kogakkaishi Vol. 49; no. 8; pp. 599 - 607 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
The Society of Powder Technology, Japan
01.01.2012
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Subjects | |
Online Access | Get full text |
ISSN | 0386-6157 1883-7239 |
DOI | 10.4164/sptj.49.599 |
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Abstract | In the present study, we have investigated the liquid resin composite consisted of an epoxy resin, an epoxy resin curing agent, a filler of silica particles, and a particle surface modifier of silane coupling agent at different temperatures, using atomic force microscopy and rheometry. Particular focus is on the mechanism how interaction forces between the silica surfaces and rheological properties of the liquid resin composite are affected by the silane coupling agent and the temperature. The relationship between the interparticle force and the particulate suspension rheology was discussed at a molecular level. |
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AbstractList | In the present study, we have investigated the liquid resin composite consisted of an epoxy resin, an epoxy resin curing agent, a filler of silica particles, and a particle surface modifier of silane coupling agent at different temperatures, using atomic force microscopy and rheometry. Particular focus is on the mechanism how interaction forces between the silica surfaces and rheological properties of the liquid resin composite are affected by the silane coupling agent and the temperature. The relationship between the interparticle force and the particulate suspension rheology was discussed at a molecular level. |
Author | Fukasawa, Tomonori Shinto, Hiroyuki Fujisaki, Kazuya Oota, Ken Matsuoka, Yuki |
Author_xml | – sequence: 1 fullname: Oota, Ken organization: Production Engineering Research Laboratory, Sumitomo Bakelite Co., Ltd – sequence: 1 fullname: Shinto, Hiroyuki organization: Department of Chemical Engineering, Kyoto University – sequence: 1 fullname: Fujisaki, Kazuya organization: Production Engineering Research Laboratory, Sumitomo Bakelite Co., Ltd – sequence: 1 fullname: Fukasawa, Tomonori organization: Department of Chemical Engineering, Kyoto University – sequence: 1 fullname: Matsuoka, Yuki organization: Production Engineering Research Laboratory, Sumitomo Bakelite Co., Ltd |
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References | 1) Honma, Y. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 3, p. 161-166, (2003 17) Bergna, H. E. and W. O. Roberts, ed. : “Colloidal Silica : Fundamentals and Applications”, Chapter 3, CRC Press (2005 3) Nagata, K. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 2, p. 13-21, (2003 11) Vakarelski, I. U. and K. Higashitani : “Single-nanoparticle-terminated tips for scanning probe microscopy”, Langmuir, 22, 2931-2934 (2006 7) Kanda, Y., T. Nishimura and K. Higashitani : “Interaction forces between silica surfaces in wet cyclohexane”, J. Soc. Powder Technol., Japan, 38, 316-322 (2001 13) Mewis, J. and N. J. Wagner : “Colloidal Suspension Rheology”, Chapter 8, Cambridge University Press (2011 4) Butt, H.-J., B. Cappella and M. Kappl : “Force measurements with the atomic force microscope : Technique, interpretation and applications”, Surface Sci. Rep., 59, 1-152 (2005 12) Mewis, J. and N. J. Wagner : “Colloidal Suspension Rheology”, Chapter 6, Cambridge University Press (2011 6) Kanda, Y., T. Nakamura and K. Higashitani : “AFM studies of interaction forces between surfaces in alcohol-water solutions”, Colloids Surfaces A, 139, 55-62 (1998 15) Evans, D. F. and H. Wennerström : “The Colloidal Domain : where Physics, Chemistry, and Biology Meet”, 2nd edn., p. 264-269, Wiley-VCH (1999 14) Israelachvili, J. N. : “Intermolecular and Surface Forces”, 3rd edn., p. 456-460, Academic Press (2010 2) Nakamura, Y. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 2, p. 22-27, (2003 5) Vakarelski, I. U., Y. Kanda, H. Shinto and K. Higashitani : “Adhesion of particles to surfaces in aqueous and non-aqueous media”, Encyclopedia of Surface and Colloid Science : 2nd edn., 1:1, 1-17, CRC Press (2007 8) Wang, S., J. Liu, L. Zhang, Z. Xu and J. Masliyah : “Colloidal interactions between asphaltene surfaces in toluene”, Energy Fuels, 23, 862-869 (2008 9) Bower, M. J. D., T. L. Bank, R. F. Giese and C. J. van Oss : “Nanoscale forces of interaction between glass in aqueous and non-aqueous media : A theoretical and empirical study”, Colloids Surfaces A, 362, 90-96 (2010 10) Yakubo, T., T. Nakabeppu, T. Fukasawa and H. Shinto : “Interaction forces between hydrophilic or hydrophobized silica surfaces in non-aqueous media studied by AFM”, J. Soc. Powder Technol., Japan, 48, 296-302 (2011 16) Iler, R. K. : “The Chemistry of Silica : Solubility, Polymerization, Colloid and Surface Properties and Biochemistry of Silica”, p. 624-648, Wiley-Interscience (1979 19) Shinto, H. : In “Discharge, Collision and Drying of Small Droplet in Inkjet Technology”, p. 85-102, Technical Information Institute (2009 18) Woutersen, A. T. J. M. and C. G. de Kruif : “The rheology of adhesive hard-sphere dispersions”, J. Chem. Phys., 94, 5739-5750 (1991 11 12 13 14 15 16 1 2 3 4 5 6 7 8 9 10 |
References_xml | – reference: 8) Wang, S., J. Liu, L. Zhang, Z. Xu and J. Masliyah : “Colloidal interactions between asphaltene surfaces in toluene”, Energy Fuels, 23, 862-869 (2008) – reference: 13) Mewis, J. and N. J. Wagner : “Colloidal Suspension Rheology”, Chapter 8, Cambridge University Press (2011) – reference: 17) Bergna, H. E. and W. O. Roberts, ed. : “Colloidal Silica : Fundamentals and Applications”, Chapter 3, CRC Press (2005) – reference: 5) Vakarelski, I. U., Y. Kanda, H. Shinto and K. Higashitani : “Adhesion of particles to surfaces in aqueous and non-aqueous media”, Encyclopedia of Surface and Colloid Science : 2nd edn., 1:1, 1-17, CRC Press (2007) – reference: 11) Vakarelski, I. U. and K. Higashitani : “Single-nanoparticle-terminated tips for scanning probe microscopy”, Langmuir, 22, 2931-2934 (2006) – reference: 6) Kanda, Y., T. Nakamura and K. Higashitani : “AFM studies of interaction forces between surfaces in alcohol-water solutions”, Colloids Surfaces A, 139, 55-62 (1998) – reference: 7) Kanda, Y., T. Nishimura and K. Higashitani : “Interaction forces between silica surfaces in wet cyclohexane”, J. Soc. Powder Technol., Japan, 38, 316-322 (2001) – reference: 9) Bower, M. J. D., T. L. Bank, R. F. Giese and C. J. van Oss : “Nanoscale forces of interaction between glass in aqueous and non-aqueous media : A theoretical and empirical study”, Colloids Surfaces A, 362, 90-96 (2010) – reference: 16) Iler, R. K. : “The Chemistry of Silica : Solubility, Polymerization, Colloid and Surface Properties and Biochemistry of Silica”, p. 624-648, Wiley-Interscience (1979) – reference: 1) Honma, Y. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 3, p. 161-166, (2003) – reference: 19) Shinto, H. : In “Discharge, Collision and Drying of Small Droplet in Inkjet Technology”, p. 85-102, Technical Information Institute (2009) – reference: 12) Mewis, J. and N. J. Wagner : “Colloidal Suspension Rheology”, Chapter 6, Cambridge University Press (2011) – reference: 10) Yakubo, T., T. Nakabeppu, T. Fukasawa and H. Shinto : “Interaction forces between hydrophilic or hydrophobized silica surfaces in non-aqueous media studied by AFM”, J. Soc. Powder Technol., Japan, 48, 296-302 (2011) – reference: 15) Evans, D. F. and H. Wennerström : “The Colloidal Domain : where Physics, Chemistry, and Biology Meet”, 2nd edn., p. 264-269, Wiley-VCH (1999) – reference: 4) Butt, H.-J., B. Cappella and M. Kappl : “Force measurements with the atomic force microscope : Technique, interpretation and applications”, Surface Sci. Rep., 59, 1-152 (2005) – reference: 18) Woutersen, A. T. J. M. and C. G. de Kruif : “The rheology of adhesive hard-sphere dispersions”, J. Chem. Phys., 94, 5739-5750 (1991) – reference: 2) Nakamura, Y. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 2, p. 22-27, (2003) – reference: 3) Nagata, K. : In “Sosetsu Epokishi Jushi (in Japanese)”, The Japan Society of Epoxy Resin Technology vol. 2, p. 13-21, (2003) – reference: 14) Israelachvili, J. N. : “Intermolecular and Surface Forces”, 3rd edn., p. 456-460, Academic Press (2010) – ident: 2 – ident: 3 – ident: 8 doi: 10.1021/ef800812k – ident: 5 – ident: 7 doi: 10.4164/sptj.38.316 – ident: 1 – ident: 9 doi: 10.1016/j.colsurfa.2010.03.040 – ident: 4 doi: 10.1016/j.surfrep.2005.08.003 – ident: 12 – ident: 6 doi: 10.1016/S0927-7757(98)00273-8 – ident: 13 – ident: 15 doi: 10.1201/9781420028706 – ident: 16 – ident: 14 – ident: 11 doi: 10.1017/CBO9780511977978 – ident: 10 doi: 10.1017/CBO9780511977978 |
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SubjectTerms | Coupling agents Epoxy resins Liquid epoxy resin Liquids Particulate composites Polymers Rheology Silane coupling agent Silanes Silica particle Silicon dioxide Surface force |
Title | Solid / Liquid Interfacial Structures, Surface Forces, and Rheology of Colloidal Dispersions Comprised of Silica Particles Suspended in Liquid Epoxy Resins |
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