n-Propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 (SBA-DABCO) as basic mesoporous catalyst for the synthesis of 1,4-dihydropyridine hetrocyclic compounds
Regarding the green chemistry's goals, the development of mesoporous silica materials as attractive candidates in the search for supporting of catalysts is currently a subject of increasing interest. Therefore, in the present research n-propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15...
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| Published in | Catalysis communications Vol. 69; pp. 179 - 182 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
05.09.2015
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1566-7367 1873-3905 |
| DOI | 10.1016/j.catcom.2015.06.019 |
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| Abstract | Regarding the green chemistry's goals, the development of mesoporous silica materials as attractive candidates in the search for supporting of catalysts is currently a subject of increasing interest. Therefore, in the present research n-propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 (SBA–DABCO) was used as a basic catalyst for the synthesis of 1,4-dihydropyridine (DHP) derivatives from one pot, three-component condensation of aromatic aldehydes, ammonium acetate and ethylacetoacetate under solvent-free at 80°C. This method offers several advantages, including high yield, short reaction time, simple work-up procedure, ease of separation and recyclability of the catalyst, as well as the ability to tolerate a wide variety of substitutions in the reagents.
•Synthesis of 1,4-dihydropyridine (DHP) derivatives•n-Propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 as a basic catalyst•Inorganic–organic hybrid basic nanocatalyst•Green catalyst in the synthesis of biologically relevant heterocyclic compounds |
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| AbstractList | Regarding the green chemistry's goals, the development of mesoporous silica materials as attractive candidates in the search for supporting of catalysts is currently a subject of increasing interest. Therefore, in the present research n-propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 (SBA–DABCO) was used as a basic catalyst for the synthesis of 1,4-dihydropyridine (DHP) derivatives from one pot, three-component condensation of aromatic aldehydes, ammonium acetate and ethylacetoacetate under solvent-free at 80°C. This method offers several advantages, including high yield, short reaction time, simple work-up procedure, ease of separation and recyclability of the catalyst, as well as the ability to tolerate a wide variety of substitutions in the reagents.
•Synthesis of 1,4-dihydropyridine (DHP) derivatives•n-Propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 as a basic catalyst•Inorganic–organic hybrid basic nanocatalyst•Green catalyst in the synthesis of biologically relevant heterocyclic compounds |
| Author | Davarpanah, Jamal Kiasat, Ali Reza |
| Author_xml | – sequence: 1 givenname: Ali Reza surname: Kiasat fullname: Kiasat, Ali Reza organization: Chemistry Department, College of Science, Shahid Chamran University, Ahvaz, Iran – sequence: 2 givenname: Jamal surname: Davarpanah fullname: Davarpanah, Jamal email: jamaldavarpanah@gmail.com organization: Chemistry Department, Production Technology Research Institute—ACECR, Ahvaz, Iran |
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| SubjectTerms | DABCO Dihydropyridine heterocyclic compounds Mesoporous catalyst Multicomponent reaction Organic–inorganic hybrid silica |
| Title | n-Propyl-4-aza-1-azoniabicyclo[2.2.2]octane chloride-SBA-15 (SBA-DABCO) as basic mesoporous catalyst for the synthesis of 1,4-dihydropyridine hetrocyclic compounds |
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