6π-Electrocyclization in water: microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones

Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E -facto...

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Published inGreen chemistry : an international journal and green chemistry resource : GC Vol. 22; no. 14; pp. 4445 - 4449
Main Authors Li, Xiao-Yun, Liu, Yan, Chen, Xiao-Lan, Lu, Xin-Yuan, Liang, Xing-Xing, Zhu, Shan-Shan, Wei, Chuan-Wan, Qu, Ling-Bo, Yu, Bing
Format Journal Article
LanguageEnglish
Published Cambridge Royal Society of Chemistry 20.07.2020
Subjects
Additives
Aniline
carbon disulfide
Catalysts
Chemical reactions
Crystallography
filtration
Green chemistry
microwave treatment
Quinoline
Synthesis
Online AccessGet full text
ISSN1463-9262
1463-9270
1463-9270
DOI10.1039/c9gc04445k

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Abstract Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E -factor of 0.45 and an EcoScale score of 85.5 were obtained. Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives.
AbstractList Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E -factor of 0.45 and an EcoScale score of 85.5 were obtained.
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho-heteroaryl anilines and CS₂ was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E-factor of 0.45 and an EcoScale score of 85.5 were obtained.
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho-heteroaryl anilines and CS2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E-factor of 0.45 and an EcoScale score of 85.5 were obtained.
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E -factor of 0.45 and an EcoScale score of 85.5 were obtained. Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives.
Author Li, Xiao-Yun
Liu, Yan
Chen, Xiao-Lan
Liang, Xing-Xing
Wei, Chuan-Wan
Qu, Ling-Bo
Lu, Xin-Yuan
Yu, Bing
Zhu, Shan-Shan
AuthorAffiliation College of Chemistry
Green Catalysis Centre
Xinyang Agriculture & Forestry University
University of South China
College of Biological and Pharmaceutical Engineering
School of Chemistry and Chemical Engineering
Zhengzhou University
AuthorAffiliation_xml – name: Xinyang Agriculture & Forestry University
– name: Zhengzhou University
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– name: Green Catalysis Centre
– name: College of Chemistry
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Snippet Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water...
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho-heteroaryl anilines and CS2 was realized in water...
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho-heteroaryl anilines and CS₂ was realized in water...
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SubjectTerms Additives
Aniline
carbon disulfide
Catalysts
Chemical reactions
Crystallography
filtration
Green chemistry
microwave treatment
Quinoline
Synthesis
Title 6π-Electrocyclization in water: microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones
URI https://www.proquest.com/docview/2424990639
https://www.proquest.com/docview/2477620441
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