Determination of Corticoids in Commercial Preparations by Micro High Performance Luiquid Chromatography
Determination of corticoids in commercial preparations by micro high performance liquid chromatography (MHPLC) was studied. The analytical conditions were as follows: column, HP-01 (10μm, 0.5 mm i. d.×14cm, Teflon tube); flow rate, 16 or 8, μl/ min.; injection volume, lμl; volume of mobile phase for...
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| Published in | Byōin yakugaku Vol. 12; no. 1; pp. 14 - 20 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | Japanese |
| Published |
Japanese Society of Pharmaceutical Health Care and Sciences
1986
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0389-9098 2185-9477 2185-9477 |
| DOI | 10.5649/jjphcs1975.12.14 |
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| Abstract | Determination of corticoids in commercial preparations by micro high performance liquid chromatography (MHPLC) was studied. The analytical conditions were as follows: column, HP-01 (10μm, 0.5 mm i. d.×14cm, Teflon tube); flow rate, 16 or 8, μl/ min.; injection volume, lμl; volume of mobile phase for one assay, 50-25μl MHPLC is considered to be a convenient method for the rapid analysis of a small amount of pharmaceutical preparations at hospital pharmacy. |
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| AbstractList | Determination of corticoids in commercial preparations by micro high performance liquid chromatography (MHPLC) was studied. The analytical conditions were as follows: column, HP-01 (10μm, 0.5 mm i. d.×14cm, Teflon tube); flow rate, 16 or 8, μl/ min.; injection volume, lμl; volume of mobile phase for one assay, 50-25μl MHPLC is considered to be a convenient method for the rapid analysis of a small amount of pharmaceutical preparations at hospital pharmacy. |
| Author | MAKI, YOSHITSUGU SHIBATA, KATSURO KUMAKAWA, YUKIE SEKIZUKA, MASAYUKI |
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| References | 4) Patricia A. Williams and Edward R. Biehl: J. Pharm. Sci., 70, 530 (1981). 10) John K. Baker and E. Kim Fifer: J. Pharm. Sci., 69, 590 (1980). 5) Michael C. Olson: J. Pharm. Sci., 12, 2001 (1973). V. Das. Gupta: J. Pharm. Sci., 68, 908 (1979). 7) L. M. Upton, E. R. Townley and F. D. Sancilio: J. Pharm. Sci., 67, 913 (1978). 11) 石井大道: 化学の領域, 増刊121号, 49 (1978). 3) 山岡桂子, 西川元博, 斎藤好広, 佐藤孝俊: 病院薬学, 6, 99 (1980). 9) Milda J.Walters and Walter E.Dunbar: J. Pharm. Sci., 71, 446 (1982). 6) M. C. Shaw and A. J. Vanderwielen: J. Pharm. Sci., 73, 1606 (1984). 8) V. Das. Gupta: J. Pharm. Sci., 68, 926 (1978). 2) H. Tokunaga, T. Kimura, and J. Kawamura: Iyakuhin Kenkyu, 14, 31 (1983 V. Das. Gupta: J. Pharm. Sci., 72, 1453 (1983). 1) H. Tokunaga, T. Kimura, and J. Kawamura: Chem. Pharm. Bull., 32, 4012 (1984). H. Tokunaga, T. Kimura, and J. Kawamura: Iyakuhin Kenkyu, 15, 87 (1984). |
| References_xml | – reference: 11) 石井大道: 化学の領域, 増刊121号, 49 (1978). – reference: 6) M. C. Shaw and A. J. Vanderwielen: J. Pharm. Sci., 73, 1606 (1984). – reference: 10) John K. Baker and E. Kim Fifer: J. Pharm. Sci., 69, 590 (1980). – reference: 2) H. Tokunaga, T. Kimura, and J. Kawamura: Iyakuhin Kenkyu, 14, 31 (1983); – reference: H. Tokunaga, T. Kimura, and J. Kawamura: Iyakuhin Kenkyu, 15, 87 (1984). – reference: 8) V. Das. Gupta: J. Pharm. Sci., 68, 926 (1978). – reference: 7) L. M. Upton, E. R. Townley and F. D. Sancilio: J. Pharm. Sci., 67, 913 (1978). – reference: 4) Patricia A. Williams and Edward R. Biehl: J. Pharm. Sci., 70, 530 (1981). – reference: 5) Michael C. Olson: J. Pharm. Sci., 12, 2001 (1973). – reference: 9) Milda J.Walters and Walter E.Dunbar: J. Pharm. Sci., 71, 446 (1982). – reference: 3) 山岡桂子, 西川元博, 斎藤好広, 佐藤孝俊: 病院薬学, 6, 99 (1980). – reference: V. Das. Gupta: J. Pharm. Sci., 72, 1453 (1983). – reference: V. Das. Gupta: J. Pharm. Sci., 68, 908 (1979). – reference: 1) H. Tokunaga, T. Kimura, and J. Kawamura: Chem. Pharm. Bull., 32, 4012 (1984). |
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| Title | Determination of Corticoids in Commercial Preparations by Micro High Performance Luiquid Chromatography |
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