Synthesis and Characterization of Patronite Form of Vanadium Sulfide on Graphitic Layer
With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2 2–, such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthes...
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| Published in | Journal of the American Chemical Society Vol. 135; no. 23; pp. 8720 - 8725 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
12.06.2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0002-7863 1520-5126 1520-5126 |
| DOI | 10.1021/ja403232d |
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| Abstract | With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2 2–, such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS4, V4+(S2 2–)2) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS4 using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS4. Furthermore, the VS4/rGO hybrid was proved to be a promising functional material in energy storage devices. |
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| AbstractList | With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2(2-), such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS4, V(4+)(S2(2-))2) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS4 using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS4. Furthermore, the VS4/rGO hybrid was proved to be a promising functional material in energy storage devices.With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2(2-), such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS4, V(4+)(S2(2-))2) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS4 using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS4. Furthermore, the VS4/rGO hybrid was proved to be a promising functional material in energy storage devices. With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2 2–, such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS4, V4+(S2 2–)2) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS4 using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS4. Furthermore, the VS4/rGO hybrid was proved to be a promising functional material in energy storage devices. With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S₂²–, such as pyrite (FeS₂), cattierite (CoS₂), and vaesite (NiS₂), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS₄, V⁴⁺(S₂²–)₂) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS₄ using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS₄. Furthermore, the VS₄/rGO hybrid was proved to be a promising functional material in energy storage devices. With the exploding interest in transition metal chalcogenides, sulfide minerals containing the dianion S2(2-), such as pyrite (FeS2), cattierite (CoS2), and vaesite (NiS2), have recently attracted much attention for potential applications in energy conversion and storage devices. However, the synthesis of the patronite structure (VS4, V(4+)(S2(2-))2) and its applications have not yet been clearly demonstrated because of experimental difficulties and the existence of nonstoichiometric phases. Herein, we report the synthesis of VS4 using a simple, facile hydrothermal method with a graphene oxide (GO) template and the characterization of the resulting material. Tests of various templates such as CNT, pyrene, perylene-3,4,9,10-tetracarboxylic dianhydride (PTCDA), and graphite led us to the conclusion that the graphitic layer plays a role in the nucleation during growth of VS4. Furthermore, the VS4/rGO hybrid was proved to be a promising functional material in energy storage devices. |
| Author | Jeong, Hu Young Rout, Chandra Sekhar Yang, Jieun Kim, Byeong-Hwan Cho, Jaephil Shin, Hyeon Suk Odkhuu, Dorj Xu, Xiaodong Park, Noejung |
| AuthorAffiliation | UNIST (Ulsan National Institute of Science and Technology) |
| AuthorAffiliation_xml | – name: UNIST (Ulsan National Institute of Science and Technology) |
| Author_xml | – sequence: 1 givenname: Chandra Sekhar surname: Rout fullname: Rout, Chandra Sekhar – sequence: 2 givenname: Byeong-Hwan surname: Kim fullname: Kim, Byeong-Hwan – sequence: 3 givenname: Xiaodong surname: Xu fullname: Xu, Xiaodong – sequence: 4 givenname: Jieun surname: Yang fullname: Yang, Jieun – sequence: 5 givenname: Hu Young surname: Jeong fullname: Jeong, Hu Young – sequence: 6 givenname: Dorj surname: Odkhuu fullname: Odkhuu, Dorj – sequence: 7 givenname: Noejung surname: Park fullname: Park, Noejung – sequence: 8 givenname: Jaephil surname: Cho fullname: Cho, Jaephil email: shin@unist.ac.kr, jpcho@unist.ac.kr – sequence: 9 givenname: Hyeon Suk surname: Shin fullname: Shin, Hyeon Suk email: shin@unist.ac.kr, jpcho@unist.ac.kr |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/23679353$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | energy conversion graphene graphene oxide Graphite - chemical synthesis Graphite - chemistry Models, Molecular Oxides - chemical synthesis Oxides - chemistry Particle Size sulfide minerals sulfides Sulfides - chemical synthesis Sulfides - chemistry Surface Properties vanadium Vanadium Compounds - chemical synthesis Vanadium Compounds - chemistry |
| Title | Synthesis and Characterization of Patronite Form of Vanadium Sulfide on Graphitic Layer |
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