Reevaluation of Th and U concentrations in marine sediment reference materials using isotope dilution MC-ICP-MS: towards the analytical improvements in dose rate estimation for luminescence dating
The thorium and uranium concentrations of four marine sediment reference materials (CRMs NIST 1646a, NRCC HISS-1, MESS-3 and PACS-2) were determined using isotope dilution-multiple collector-inductively coupled plasmas-mass spectrometry (ID-MC-ICP-MS), aiming at helping the assessment of reliability...
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| Published in | Geosciences journal (Seoul, Korea) Vol. 17; no. 2; pp. 123 - 127 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
The Geological Society of Korea
01.06.2013
Springer Nature B.V 한국지질과학협의회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-4806 1598-7477 |
| DOI | 10.1007/s12303-013-0023-1 |
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| Abstract | The thorium and uranium concentrations of four marine sediment reference materials (CRMs NIST 1646a, NRCC HISS-1, MESS-3 and PACS-2) were determined using isotope dilution-multiple collector-inductively coupled plasmas-mass spectrometry (ID-MC-ICP-MS), aiming at helping the assessment of reliability in dose rate estimation for luminescence dating. Quintuplicate analyses of the CRMs revealed their intrinsic heterogeneity in the concentration of both elements (up to 23% and 8% for thorium and uranium, respectively, in 2σ standard error level) for individual sub-samples of about 100 mg. The thorium and uranium concentrations of all CRMs determined in this study were significantly lower (up to 45%) than the provided or reported informative values, requiring reevaluation of their reference concentrations. The use of informative thorium and uranium concentrations in these CRMs as standard values for elemental analysis of unknown samples will result in overestimated dose rates, and thus age underestimation when applied to luminescence dating techniques. |
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| AbstractList | The thorium and uranium concentrations of four marine sediment reference materials (CRMs NIST 1646a, NRCC HISS-1, MESS-3 and PACS-2) were determined using isotope dilution-multiple collector-inductively coupled plasmas-mass spectrometry (ID-MC-ICP-MS), aiming at helping the assessment of reliability in dose rate estimation for luminescence dating. Quintuplicate analyses of the CRMs revealed their intrinsic heterogeneity in the concentration of both elements (up to 23% and 8% for thorium and uranium, respectively, in 2[sigma] standard error level) for individual sub-samples of about 100 mg. The thorium and uranium concentrations of all CRMs determined in this study were significantly lower (up to 45%) than the provided or reported informative values, requiring reevaluation of their reference concentrations. The use of informative thorium and uranium concentrations in these CRMs as standard values for elemental analysis of unknown samples will result in overestimated dose rates, and thus age underestimation when applied to luminescence dating techniques.[PUBLICATION ABSTRACT] The thorium and uranium concentrations of four marine sediment reference materials (CRMs NIST 1646a, NRCC HISS-1, MESS-3 and PACS-2) were determined using isotope dilution-multiple collector-inductively coupled plasmas-mass spectrometry (ID-MC-ICP-MS), aiming at helping the assessment of reliability in dose rate estimation for luminescence dating. Quintuplicate analyses of the CRMs revealed their intrinsic heterogeneity in the concentration of both elements (up to 23% and 8% for thorium and uranium, respectively, in 2σ standard error level) for individual sub-samples of about 100 mg. The thorium and uranium concentrations of all CRMs determined in this study were significantly lower (up to 45%) than the provided or reported informative values, requiring reevaluation of their reference concentrations. The use of informative thorium and uranium concentrations in these CRMs as standard values for elemental analysis of unknown samples will result in overestimated dose rates, and thus age underestimation when applied to luminescence dating techniques. The thorium and uranium concentrations of four marine sediment reference materials (CRMs NIST 1646a, NRCC HISS-1, MESS-3 and PACS-2) were determined using isotope dilution-multiple collector-inductively coupled plasmas-mass spectrometry (ID-MC-ICP-MS), aiming at helping the assessment of reliability in dose rate estimation for luminescence dating. Quintuplicate analyses of the CRMs revealed their intrinsic heterogeneity in the concentration of both elements (up to 23% and 8% for thorium and uranium, respectively, in 2s standard error level) for individual sub-samples of about 100 mg. The thorium and uranium concentrations of all CRMs determined in this study were significantly lower (up to 45%) than the provided or reported informative values, requiring reevaluation of their reference concentrations. The use of informative thorium and uranium concentrations in these CRMs as standard values for elemental analysis of unknown samples will result in overestimated dose rates, and thus age underestimation when applied to luminescence dating techniques. KCI Citation Count: 1 |
| Author | Kim, Jeongmin Ryu, Jong-Sik Cheong, Chang-sik Choi, Jeong-Heon Shin, Hyung Seon |
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| Cites_doi | 10.1111/j.1751-908X.2007.00845.x 10.1111/j.1475-4754.1986.tb00388.x 10.1016/j.radmeas.2005.11.001 10.1016/j.radmeas.2009.02.007 10.1016/S0168-1176(97)00136-5 10.1111/j.1751-908X.2002.tb00623.x 10.1016/1350-4487(94)90102-3 10.1016/0009-2541(92)90042-4 10.1111/j.1751-908X.2008.00880.x 10.1021/ac00185a715 |
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| References | Nambi, Aitken (CR9) 1986; 28 Park, Shin, Oh, Moon, Cho, Cheong (CR10) 2013 Waheed, Rahman, Siddique, Ahmad (CR13) 2007; 31 Meisel, Schöner, Paliulionyte, Kahr (CR8) 2002; 26 Luo, Rehkämper, Lee, Halliday (CR7) 1997; 171 Rendell, Wood (CR11) 1994; 23 Aitken (CR2) 1985 Fassett, Paulsen (CR5) 1989; 61 Buylaert, Murray, Thomsen, Jain (CR4) 2009; 44 Wintle, Murray (CR14) 2006; 41 Heumann, Adams, Gijbels, Van Grieken (CR6) 1988 Adamiec, Aitken (CR1) 1998; 16 Bayon, Barrat, Etoubleau, Benoit, Bollinger, Révillon (CR3) 2008; 33 Totland, Jarvis, Jarvis (CR12) 1992; 95 T Meisel (23_CR8) 2002; 26 JD Fassett (23_CR5) 1989; 61 KG Heumann (23_CR6) 1988 G Bayon (23_CR3) 2008; 33 C-S Park (23_CR10) 2013 AG Wintle (23_CR14) 2006; 41 G Adamiec (23_CR1) 1998; 16 M Totland (23_CR12) 1992; 95 HM Rendell (23_CR11) 1994; 23 X Luo (23_CR7) 1997; 171 MJ Aitken (23_CR2) 1985 S Waheed (23_CR13) 2007; 31 KSV Nambi (23_CR9) 1986; 28 JP Buylaert (23_CR4) 2009; 44 |
| References_xml | – volume: 31 start-page: 133 year: 2007 end-page: 141 ident: CR13 article-title: Rare earth and other trace element content of NRCC HISS-1 sandy marine sediment reference material publication-title: Geostandards and Geoanalytical Research doi: 10.1111/j.1751-908X.2007.00845.x – year: 2013 ident: CR10 article-title: Determination of trace elements in geological reference materials G-3, GSP-2 and SGD-1a by low-dilution glass bead digestion and ICP-MS publication-title: Geostandards and Geoanalytical Research (in press) – volume: 28 start-page: 202 year: 1986 end-page: 205 ident: CR9 article-title: Annual dose conversion factors for TL and ESR dating publication-title: Archaeometry doi: 10.1111/j.1475-4754.1986.tb00388.x – volume: 41 start-page: 369 year: 2006 end-page: 391 ident: CR14 article-title: A review of optically stimulated luminescence characteristics and their relevance in singlealiquot regeneration dating protocols publication-title: Radiation Measurements doi: 10.1016/j.radmeas.2005.11.001 – volume: 44 start-page: 560 year: 2009 end-page: 565 ident: CR4 article-title: Testing the potential of an elevated temperature IRSL signal from Kfeldspar publication-title: Radiation Measurements doi: 10.1016/j.radmeas.2009.02.007 – volume: 33 start-page: 51 year: 2008 end-page: 62 ident: CR3 article-title: Determination of rare earth elements, Sc, Y, Zr, Ba, Hf and Th in geological samples by ICP-MS after Tm addition and alkaline fusion publication-title: Geostandards and Geoanalytical Research – volume: 171 start-page: 105 year: 1997 end-page: 117 ident: CR7 article-title: High precision Th/ Th and U/ U measurements using energyfiltered magnetic sector multiple collector mass spectrometry publication-title: International Journal of Mass Spectrometry and Ion Processes doi: 10.1016/S0168-1176(97)00136-5 – volume: 26 start-page: 53 year: 2002 end-page: 61 ident: CR8 article-title: Determination of rare earth elements, Y, Th, Zr, Hf, Nb and Ta in geological reference materials G-2, G-3, SCo-1 and WGB-1 by sodium peroxide sintering and inductively coupled plasma-mass spectrometry publication-title: Geostandards Newsletter doi: 10.1111/j.1751-908X.2002.tb00623.x – volume: 16 start-page: 37 year: 1998 end-page: 50 ident: CR1 article-title: Dose-rate conversion factors: update publication-title: Ancient TL – start-page: 301 year: 1988 end-page: 376 ident: CR6 article-title: Isotope dilution mass spectrometry publication-title: Inorganic Mass Spectrometry – year: 1985 ident: CR2 publication-title: Thermoluminescence Dating – volume: 23 start-page: 575 year: 1994 end-page: 580 ident: CR11 article-title: Quartz sample pretreatments for TL/OSL dating: studies of TL emission spectra publication-title: Radiation Measurements doi: 10.1016/1350-4487(94)90102-3 – volume: 61 start-page: 643 year: 1989 end-page: 649 ident: CR5 article-title: Isotope dilution mass spectrometry for accurate elemental analysis publication-title: Analytical Chemistry – volume: 95 start-page: 35 year: 1992 end-page: 62 ident: CR12 article-title: An assessment of dissolution techniques for the analysis of geological samples by plasma spectrometry publication-title: Chemical Geology doi: 10.1016/0009-2541(92)90042-4 – volume: 41 start-page: 369 year: 2006 ident: 23_CR14 publication-title: Radiation Measurements doi: 10.1016/j.radmeas.2005.11.001 – volume: 95 start-page: 35 year: 1992 ident: 23_CR12 publication-title: Chemical Geology doi: 10.1016/0009-2541(92)90042-4 – volume: 44 start-page: 560 year: 2009 ident: 23_CR4 publication-title: Radiation Measurements doi: 10.1016/j.radmeas.2009.02.007 – volume: 16 start-page: 37 year: 1998 ident: 23_CR1 publication-title: Ancient TL – volume-title: Thermoluminescence Dating year: 1985 ident: 23_CR2 – volume: 33 start-page: 51 year: 2008 ident: 23_CR3 publication-title: Geostandards and Geoanalytical Research doi: 10.1111/j.1751-908X.2008.00880.x – volume: 31 start-page: 133 year: 2007 ident: 23_CR13 publication-title: Geostandards and Geoanalytical Research doi: 10.1111/j.1751-908X.2007.00845.x – volume: 171 start-page: 105 year: 1997 ident: 23_CR7 publication-title: International Journal of Mass Spectrometry and Ion Processes doi: 10.1016/S0168-1176(97)00136-5 – volume: 23 start-page: 575 year: 1994 ident: 23_CR11 publication-title: Radiation Measurements doi: 10.1016/1350-4487(94)90102-3 – volume: 26 start-page: 53 year: 2002 ident: 23_CR8 publication-title: Geostandards Newsletter doi: 10.1111/j.1751-908X.2002.tb00623.x – volume: 28 start-page: 202 year: 1986 ident: 23_CR9 publication-title: Archaeometry doi: 10.1111/j.1475-4754.1986.tb00388.x – volume: 61 start-page: 643 year: 1989 ident: 23_CR5 publication-title: Analytical Chemistry doi: 10.1021/ac00185a715 – start-page: 301 volume-title: Inorganic Mass Spectrometry year: 1988 ident: 23_CR6 – volume-title: Geostandards and Geoanalytical Research (in press) year: 2013 ident: 23_CR10 |
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| Title | Reevaluation of Th and U concentrations in marine sediment reference materials using isotope dilution MC-ICP-MS: towards the analytical improvements in dose rate estimation for luminescence dating |
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