Comprehensive Kinetics and Thermodynamics Analysis of Salix psammophila Biomass Pyrolysis Using Multicomponent Modeling

Multicomponent deconvolution enables precise peak separation and accurate determination of kinetic parameters and improves identification of the underlying mechanisms of biomass pyrolysis. In the present study, the multicomponent kinetics and thermodynamics of Salix psammophila pyrolysis were invest...

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Published inACS sustainable chemistry & engineering Vol. 13; no. 33; pp. 13695 - 13708
Main Authors Tang, Maoyi, Yao, Zhitong, Wang, Haoqi, Li, Huanxuan, da Silva, Jean Constantino Gomes, Pejic, Ljiljana Medic, Manić, Nebojša, Sun, Yuhang, Kumar, Akash, Chen, Yang, Liu, Jie, Qi, Wei
Format Journal Article
LanguageEnglish
Published American Chemical Society 25.08.2025
Subjects
bioenergy
deconvolution
pyrolysis conversion
Salix psammophila
multicomponent kinetic
Online AccessGet full text
ISSN2168-0485
2168-0485
DOI10.1021/acssuschemeng.5c07132

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Abstract Multicomponent deconvolution enables precise peak separation and accurate determination of kinetic parameters and improves identification of the underlying mechanisms of biomass pyrolysis. In the present study, the multicomponent kinetics and thermodynamics of Salix psammophila pyrolysis were investigated to evaluate its bioenergy potential. Thermogravimetric analysis coupled with peak deconvolution revealed three stages involving four components (pseudoextractives/PS-EC, pseudohemicellulose/PS-CL, pseudocellulose/PS-CL, and pseudolignin/PS-LG) with the corresponding peak temperatures of 246.83–270.83, 291.59–315.59, 335.26–359.26, and 386.14–410.14 °C, respectively. Pyrolysis gas chromatography/mass spectrometry analysis indicated dominant products of acids, phenolics, and alkanes. Activation energies for each pseudocomponent from four isoconversional methods were comparable, following an order of PS-EC (134.96 kJ mol–1) < PS-HC (151.59 kJ mol–1) < PS-CL (166.93 kJ mol–1) < PS-LG (239.65 kJ mol–1). Master plot analysis suggested an order-based reaction mechanism. Positive enthalpy changes (127.83–227.33 kJ mol–1) and Gibbs free energy changes (144.73–193.03 kJ mol–1) indicated higher energy barriers, especially for PS-LG, and limited spontaneity of conversion. These findings highlighted the potential of S. psammophila as a viable feedstock and offered critical insights into reactor design and process optimization for industrial applications.
AbstractList Multicomponent deconvolution enables precise peak separation and accurate determination of kinetic parameters and improves identification of the underlying mechanisms of biomass pyrolysis. In the present study, the multicomponent kinetics and thermodynamics of Salix psammophila pyrolysis were investigated to evaluate its bioenergy potential. Thermogravimetric analysis coupled with peak deconvolution revealed three stages involving four components (pseudoextractives/PS-EC, pseudohemicellulose/PS-CL, pseudocellulose/PS-CL, and pseudolignin/PS-LG) with the corresponding peak temperatures of 246.83–270.83, 291.59–315.59, 335.26–359.26, and 386.14–410.14 °C, respectively. Pyrolysis gas chromatography/mass spectrometry analysis indicated dominant products of acids, phenolics, and alkanes. Activation energies for each pseudocomponent from four isoconversional methods were comparable, following an order of PS-EC (134.96 kJ mol–1) < PS-HC (151.59 kJ mol–1) < PS-CL (166.93 kJ mol–1) < PS-LG (239.65 kJ mol–1). Master plot analysis suggested an order-based reaction mechanism. Positive enthalpy changes (127.83–227.33 kJ mol–1) and Gibbs free energy changes (144.73–193.03 kJ mol–1) indicated higher energy barriers, especially for PS-LG, and limited spontaneity of conversion. These findings highlighted the potential of S. psammophila as a viable feedstock and offered critical insights into reactor design and process optimization for industrial applications.
Author Liu, Jie
Pejic, Ljiljana Medic
Li, Huanxuan
Sun, Yuhang
Yao, Zhitong
Tang, Maoyi
da Silva, Jean Constantino Gomes
Manić, Nebojša
Wang, Haoqi
Chen, Yang
Kumar, Akash
Qi, Wei
AuthorAffiliation Fuel and Combustion Laboratory, Faculty of Mechanical Engineering
Chinese Academy of Sciences
College of Materials Science and Environmental Engineering
Department of Energy and Fuels, E.T.S. Ingenieros de Minas y Energía
Guangzhou Institute of Energy Conversion
State University of Campinas
Beijing Key Laboratory of Lignocellulosic Chemistry
School of Civil Engineering
Interdisciplinary Research Group on Biotechnology Applied to the Agriculture and the Environment, School of Agricultural Engineering
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Keywords bioenergy
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Salix psammophila
multicomponent kinetic
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