Analytical characterization methods for crude oil and related products
Basic theory, applications, and recent trends in analytical techniques used in crude oil and related products analysis This book covers the application of different spectroscopic methods to characterize crude oil and related products. Its topics are presented in a pedagogical manner so that those ne...
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Format: | eBook |
Language: | English |
Published: |
Newark :
John Wiley & Sons, Incorporated,
2017.
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Subjects: | |
ISBN: | 9781119286363 1119286360 9781523115556 1523115556 111928631X 9781119286318 9781119286332 1119286336 |
Physical Description: | 1 online resource (298 pages) |
LEADER | 10454cam a2200481Mi 4500 | ||
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001 | kn-on1016159344 | ||
003 | OCoLC | ||
005 | 20240717213016.0 | ||
006 | m o d | ||
007 | cr cn||||||||| | ||
008 | 171218s2017 nju o 000 0 eng | ||
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020 | |a 9781119286363 | ||
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020 | |a 1523115556 | ||
020 | |a 111928631X | ||
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020 | |a 9781119286332 |q (ePub ebook) | ||
020 | |a 1119286336 | ||
035 | |a (OCoLC)1016159344 |z (OCoLC)1086997047 |z (OCoLC)1099583117 |z (OCoLC)1100455232 |z (OCoLC)1117874515 | ||
245 | 0 | 0 | |a Analytical characterization methods for crude oil and related products / |c edited by Ashutosh Kumar Shukla, Physics Department, Ewing Christian College, India. |
264 | 1 | |a Newark : |b John Wiley & Sons, Incorporated, |c 2017. | |
264 | 4 | |c ©2018 | |
300 | |a 1 online resource (298 pages) | ||
336 | |a text |b txt |2 rdacontent | ||
337 | |a computer |b c |2 rdamedia | ||
338 | |a online resource |b cr |2 rdacarrier | ||
505 | 0 | |a "Cover" -- "Title Page" -- "Copyright" -- "Dedication" -- "Contents" -- "List of Contributors" -- "Preface" -- "Chapter 1 Rheological Characterization of Crude Oil and Related Products" -- "1.1 Introduction" -- "1.2 Sample Preparation for Rheological Characterization" -- "1.2.1 Ensuring the Chemical Stability" -- "1.2.2 Choosing the Rheometer Geometry" -- "1.2.3 Erasing the Thermal Memory" -- "1.2.4 Performing the Cooling Process" -- "1.3 Rheological Tests" -- "1.4 Potential Sources of Errors" -- "References" -- "Chapter 2 Optical Interrogation of Petroleum Asphaltenes: Myths and Reality" -- "2.1 Introduction" -- "2.1.1 What are Asphaltenes?" -- "2.1.2 The Reasons for Intensive Asphaltene Research" -- "2.1.3 No Controversy about the Elemental Composition of Asphaltenes" -- "2.1.4 Continuing Debates on the Size and the Structure of Asphaltene Molecules and Aggregates" -- "2.1.5 Conflicting Paradigms based on Similar Analytical Techniques: Apparent Significance of "Human Factors"" -- "2.2 Mythical "Characteristic Signatures" of Asphaltenes in Optical Analytical Methods" -- "2.2.1 Nonexistent "Resonance UV Absorption" of Asphaltenes" -- "2.2.2 Mythical "Characteristic Monomer Peaks" in Fluorescence Emission Studies" -- "2.3 Misconceptions about the Properties of UV/Vis Absorption Spectra of Asphaltenes" -- "2.3.1 The Myth about the Absence of Asphaltene Aggregation Effects in Optical Absorption Studies" -- "2.3.2 The Myth about the "Urbach Tail" in Optical Absorption Spectra of Asphaltenes and Crude Oils" -- "2.3.2.1 Tauc Range" -- "2.3.2.2 Urbach Range" -- "2.3.2.3 Low Absorption (Defects) Range" -- "2.3.3 In the UV/Vis Spectral Range Asphaltenes Apparently Act not as Absorbers, but as Scatterers" -- "2.4 Current State of Knowledge about Asphaltene Monomers and Primary Asphaltene Aggregates." | |
505 | 8 | |a "2.4.1 Some Requirements for Preparation of Dilute Asphaltene Solutions" -- "2.4.2 Multiple States/Phases of Primary Asphaltene Aggregates Revealed by Optical Absorption Measurements" -- "2.4.3 Multiple States/Phases of Primary Asphaltene Aggregates Revealed by Refractive Index Measurements" -- "2.4.3.1 Mean Refractive Index at Concentrations below CNAC" -- "2.4.3.2 Standard Deviation of Refractive Index at Concentrations below CNAC" -- "2.4.4 Conditions for Observation of Asphaltene Monomers and Evolution of Primary Asphaltene Aggregates Revealed by Fluorescence Measurements" -- "2.4.4.1 Studies of Steady-State Fluorescence Emission" -- "2.4.4.2 Studies of Time-Resolved Fluorescence Emission" -- "2.4.5 Evolution of Primary Asphaltene Aggregates Revealed by Mass Spectrometry" -- "2.4.6 "Optical Interrogation" Reveals that Primary Asphaltene Aggregates are Porous and Entrap/Occlude Molecules of Metalloporphyrins and other Compounds" -- "2.4.7 Apparent Absence of "Consecutive Aggregation" in Asphaltene Experiments: Revised Description of the Observed Non-monotonic Concentration Effects in Dilute Asphaltene Solutions" -- "References" -- "Chapter 3 ESR Characterization of Organic Free Radicals in Crude Oil and By-Products" -- "3.1 Introduction" -- "3.2 Organic-Free Radicals in Crude Oil" -- "3.3 ESR of Crude Oil" -- "3.4 By-Product Oil by ESR" -- "3.5 ESR and Calculations on the Electronic Structure of Free Radicals in Oil By-Products" -- "References" -- "Chapter 4 High-Field, Pulsed, and Double Resonance Studies of Crude Oils and their Derivatives" -- "4.1 Introduction" -- "4.2 EPR: Basic Principles and Magnetic Interactions" -- "4.3 EPR Pulse Sequences" -- "4.4 Application Examples" -- "4.4.1 W-Band, Relaxation Studies of VO2+ and FR in Asphaltenes Fractions" -- "4.4.2 ENDOR of VO2+ in Crude Oil Samples" -- "4.5 Conclusion" -- "Acknowledgments." | |
504 | |a "References"-"Chapter 5 NMR Spectroscopic Analysis in Characterization of Crude Oil and Related Products"-"5.1 Introduction"-"5.2 1H NMR and 13C NMR Spectroscopy Analysis Methods"-"5.3 NMR Techniques"-"5.4 Application of NMR Analysis in Characterization of Crude Oil and Related Products"-"5.5 Asphaltene Characterization using NMR Techniques"-"5.6 Conclusions"-"References"-"Chapter 6 NMR Spectroscopy in Bitumen Characterization"-"6.1 Introduction"-"6.2 1H and 13C NMR Spectroscopy"-"6.3 Phosphorus-31 NMR Spectroscopy"-"6.4 NMR Imaging and Solid-State NMR"-"6.4.1 Solid-State NMR"-"6.4.2 NMR Imaging"-"6.5 Conclusion"-"References"-"Chapter 7 Applications of Low Field Magnetic Resonance in Viscous Crude Oil/Water Property Determination"-"7.1 Introduction"-"7.2 Background for NMR Measurements"-"7.2.1 Interpretation of NMR Relaxation Rates"-"7.2.2 Interpretation of NMR Amplitudes"-"7.3 Fluid Content in Oil/Water Systems"-"7.4 Oil Viscosity from NMR"-"7.4.1 Viscosity Predictions in High Viscosity Bitumen"-"7.4.2 Viscosity Predictions in Oilfield Emulsions"-"7.5 Fluid Saturations and Viscosity in Porous Media"-"7.5.1 Prediction of Saturations and Viscosity from T2 relaxation distributions"-"7.5.2 Prediction of Saturations from T1-T2 Relaxation Distributions"-"7.6 NMR in Oil-Solvent Systems"-"7.6.1 Predictions of Solvent Content in Oil-Liquid Solvent Systems"-"7.6.2 Predictions of Non-Equilibrium Viscosity in Oil-Vapor Solvent Systems"-"7.7 Summary of NMR and Fluid Property Measurements"-"Acknowledgments"-"References"-"Chapter 8 Application of Near-Infrared Spectroscopy to the Characterization of Petroleum"-"8.1 Introduction"-"8.2 Sample Handling and Preparation"-"8.3 Near-Infrared Spectroscopy"-"8.3.1 Near-Infrared in Refineries." | ||
505 | 8 | |a "8.4 Chemometrics" -- "8.4.1 Pretreatment" -- "8.4.1.1 Smoothing" -- "8.4.1.2 Multiplicative Scatter Correction" -- "8.4.1.3 Mean Centering" -- "8.4.1.4 Derivation" -- "8.4.2 Calibration Model" -- "8.4.2.1 Principal Component Analysis (PCA)" -- "8.4.2.2 Partial Least Squares Regression" -- "8.4.2.3 Artificial Neural Networks" -- "8.4.3 Validation" -- "8.4.4 Other Methods" -- "8.5 Commercial NIR Equipment and Industrial Applications" -- "8.5.1 Industrial Applications" -- "8.5.1.1 Pipeline Product Analysis and Identification" -- "8.5.1.2 Crude Distillation Optimization" -- "8.5.1.3 Product Blending" -- "8.5.1.4 Ethanol Fermentation" -- "8.5.1.5 Conjugated Diolefins in Pygas" -- "8.5.1.6 Regulatory Fuel Screening" -- "8.6 Conclusions" -- "References" -- "Chapter 9 Raman and Infrared Spectroscopy of Crude Oil and its Constituents" -- "9.1 Introduction" -- "9.2 Fundamentals of Raman and Infrared Spectroscopy" -- "9.3 Infrared Spectroscopy" -- "9.4 Raman Spectroscopy" -- "9.5 Evaluation of Vibrational Spectra" -- "9.6 Applications" -- "9.7 Conclusion" -- "References" -- "Index." | |
506 | |a Plný text je dostupný pouze z IP adres počítačů Univerzity Tomáše Bati ve Zlíně nebo vzdáleným přístupem pro zaměstnance a studenty | ||
520 | |a Basic theory, applications, and recent trends in analytical techniques used in crude oil and related products analysis This book covers the application of different spectroscopic methods to characterize crude oil and related products. Its topics are presented in a pedagogical manner so that those new to the subject can better understand the content. The book begins by familiarizing the reader with the rheological characterization of crude oil and related products. Subsequent chapters are directed towards the current trends of different spectroscopic methods for the characterization of crude oil. Analytical Characterization Methods for Crude Oil and Related Products features chapters on: optical interrogation of petroleum asphaltenes (myths and reality); ESR characterization of organic free radicals in petroleum products; high-field, pulsed, and double resonance studies of crude oils and their derivatives; NMR spectroscopy in bitumen characterization; applications of Raman spectroscopy in crude oil and bitumen characterization; and more.-Uses a bottom-up approach-starting from the basic theory of the technique followed by its applications and recent trends in crude oil analysis -Includes informative content so as to take a technician to the level of using a particular analytical method -Covers relevany information so as to enable a manager in the industry to make purchasing decisions Analytical Characterization Methods for Crude Oil and Related Products is aimed at researchers in academia as well as technicians and developers of new analytical methods in the oil industry and related areas. It will also be of interest to professionals, scientists, and graduate students in analytical sciences dealing with oil and environmental analysis. | ||
590 | |a Knovel |b Knovel (All titles) | ||
650 | 0 | |a Petroleum |x Analysis. | |
650 | 0 | |a Petroleum productrs |x Analysis. | |
655 | 7 | |a elektronické knihy |7 fd186907 |2 czenas | |
655 | 9 | |a electronic books |2 eczenas | |
700 | 1 | |a Shukla, Ashutosh Kumar, |d 1978- |e editor. |1 https://id.oclc.org/worldcat/entity/E39PCjMrwxDxQKDhYwwBwv7KtX | |
776 | 0 | 8 | |i Print version: |a Shukla, Ashutosh K. |t Analytical Characterization Methods for Crude Oil and Related Products. |d Newark : John Wiley & Sons, Incorporated, ©2017 |z 9781119286318 |
856 | 4 | 0 | |u https://proxy.k.utb.cz/login?url=https://app.knovel.com/hotlink/toc/id:kpACMCORP2/analytical-characterization-methods?kpromoter=marc |y Full text |