Liquid chromatography. Volume 2, Applications /
Saved in:
| Other Authors | , , , |
|---|---|
| Format | Electronic eBook |
| Language | English |
| Published |
Amsterdam, Netherlands :
Elsevier,
[2017]
|
| Edition | Second edition. |
| Subjects | |
| Online Access | Full text |
| ISBN | 9780128093443 0128093447 9780128053928 0128053925 |
| Physical Description | 1 online resource. |
Cover
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| 001 | kn-ocn992119225 | ||
| 003 | OCoLC | ||
| 005 | 20240717213016.0 | ||
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| 007 | cr cn||||||||| | ||
| 008 | 170628s2017 ne o 001 0 eng d | ||
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| 020 | |a 9780128093443 |q (electronic bk.) | ||
| 020 | |a 0128093447 |q (electronic bk.) | ||
| 020 | |z 9780128053928 | ||
| 020 | |z 0128053925 | ||
| 035 | |a (OCoLC)992119225 |z (OCoLC)992265754 |z (OCoLC)1105177469 |z (OCoLC)1105569920 | ||
| 245 | 0 | 0 | |a Liquid chromatography. |n Volume 2, |p Applications / |c edited by Salvatore Fanali, Paul R. Haddad, Colin F. Poole, Marja-Liisa Riekkola. |
| 246 | 3 | 0 | |a Applications |
| 250 | |a Second edition. | ||
| 264 | 1 | |a Amsterdam, Netherlands : |b Elsevier, |c [2017] | |
| 300 | |a 1 online resource. | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 500 | |a Includes index. | ||
| 505 | 0 | |a Front Cover -- Liquid Chromatography: Applications -- Copyright -- Contents -- Contributors -- Chapter 1: Sample preparation for liquid chromatography -- 1.1 Introduction -- 1.2 Overview -- 1.2.1 Objectives of Sample Preparation -- 1.2.2 Classification of Sample Preparation -- 1.2.3 Automation of Sample Preparation -- 1.2.3.1 Robotic sample preparation systems -- 1.2.3.2 Column switching sample preparation -- 1.3 Sample Extraction Techniques -- 1.3.1 Liquid-Phase Microextraction -- 1.3.1.1 DLLME -- 1.3.1.2 SDME -- 1.3.1.3 HF-LPME -- 1.3.2 Solid-Phase Extraction -- 1.3.2.1 SPE devices and processing steps -- 1.3.2.2 On-line column switching SPE -- 1.3.2.3 Sorbent selection and coating materials for SPE -- 1.3.3 Solid-Phase Microextraction -- 1.3.4 Fiber SPME -- 1.3.4.1 Fiber SPME processing steps for HPLC -- 1.3.4.2 Optimization of fiber SPME methods -- 1.3.4.3 Fiber coating materials -- 1.3.5 In-tube SPME -- 1.3.5.1 In-tube SPME processing systems -- 1.3.5.2 Optimization of in-tube SPME methods -- 1.3.5.3 Capillary coating materials -- 1.3.6 Other Sorbent Microextraction Techniques for HPLC -- 1.3.6.1 Static in-vessel microextraction -- 1.3.6.2 Dynamic in-flow microextraction -- 1.4 Conclusions -- References -- Chapter 2: Derivatization in liquid chromatography -- 2.1 Introduction -- 2.2 Reagent Selection -- 2.2.1 Reagents for UV-Visible Detection -- 2.2.2 Reagents for Fluorescence and Chemiluminescence Detection -- 2.2.3 Reagents for Electrochemical Detection -- 2.2.4 Reagents for Mass-Spectrometric Detection -- 2.2.4.1 Stable isotope-coded derivatizing reagents -- 2.2.5 Reagents for the Formation of Diastereomers -- 2.2.6 Multifunctional Reagents for the Formation of Cyclic Derivatives -- 2.2.7 Solid-Phase Analytical Derivatization -- 2.3 Postcolumn Reaction Detectors -- 2.3.1 Photoreactors -- 2.4 Conclusions -- References. | |
| 505 | 8 | |a Chapter 3: Liquid chromatographic separation of enantiomers -- 3.1 Introduction -- 3.2 Short History of Chiral LC Separations -- 3.3 Materials for LC Separation of Enantiomers -- 3.4 Modes of LC Separation of Enantiomers -- 3.4.1 Analytical Scale Separation of Enantiomers -- 3.4.2 Preparative Scale Separation of Enantiomers in LC -- 3.5 Separation of Enantiomers in Supercritical Fluid Chromatography (SFC) -- 3.6 Current Trends -- 3.7 Future Needs -- References -- Chapter 4: Amino acid and bioamine separations -- 4.1 Introduction -- 4.2 Direct Separation of Amino Acids -- 4.2.1 Postcolumn Colorimetric and Fluorescence Derivatization of Amino Acids -- 4.2.2 ESI-MS/MS Determination of Underivatized Amino Acids -- 4.3 Indirect Separation of Amino Acids -- 4.3.1 Derivatization With UV-VIS Reagents -- 4.3.2 Derivatization With Fluorescent Reagents -- 4.3.3 Derivatization for Mass Spectrometric Detection -- 4.4 Enantioselective Liquid Chromatographic Analysis of Amino Acids -- 4.4.1 Chiral Derivatization Reagents for Amino Acid Enantiomers -- 4.4.2 Chiral Stationary Phases for Amino Acid Enantiomers -- 4.4.3 Two-Dimensional Liquid Chromatographic Analysis of Amino Acid Enantiomers -- 4.5 Direct Separation of Biogenic Amines -- 4.6 Indirect Separation of Biogenic Amines -- 4.7 Conclusions -- References -- Chapter 5: Protein and peptide separations -- 5.1 Introduction -- 5.2 Methods of Protein Liquid Chromatography -- 5.2.1 Size-Exclusion Chromatography -- 5.2.2 Ion-Exchange Chromatography -- 5.2.3 Methods Based on the Hydrophobic Interaction -- Hydrophobic-interaction chromatography -- Reversed-phase chromatography -- 5.2.4 Affinity Chromatography -- Pseudoaffinity chromatography -- Hydrophobic charge-induction chromatography -- Immobilized metal-affinity chromatography -- 5.2.5 Chromatography on Hydroxyapatite -- 5.2.6 Chromatography on Monolithic Supports. | |
| 505 | 8 | |a 5.2.7 Displacement Chromatography -- 5.3 Conclusions -- Acknowledgments -- Addendum 1: Protein and Peptide Chromatography-References Update -- Ion-exchange chromatography -- Hydrophobic-interaction chromatography: -- Mixed-mode and hydrophobic charge-induction chromatography: -- Reversed-phase chromatography: -- Size-exclusion chromatography -- Displacement chromatography: -- Preparative and process chromatography: -- Monoliths, membranes and other special supports: -- Optimization and protein and peptide characterization: -- LC applications in proteomics and peptidomics: -- Affinity chromatography -- Protein and peptide chromatography, reviews and overviews -- Addendum 2: Sample Displacement Chromatography -- Introduction -- Development and Use of Sample Displacement Chromatography -- Conclusions -- References -- References -- Further Reading -- Chapter 6: Liquid chromatographic separation of oligonucleotides -- 6.1 Introduction -- 6.2 Oligonucleotide and siRNA Structure and Preparation -- 6.3 Chromatographic Separation of Oligonucleotides -- 6.3.1 Separation of Oligonucleotides With Ion-Exchange Liquid Chromatography -- 6.3.2 Separation of Oligonucleotides With IP-RPLC -- 6.3.2.1 Separation of oligonucleotides with IP-RPLC using core-shell particle columns -- 6.3.3 Separation of Oligonucleotides With Mixed-Mode Chromatography -- 6.4 Summary -- References -- Chapter 7: Separation of glycans and monosaccharides -- 7.1 Introduction -- 7.2 Types of Glycans -- 7.3 Analysis and Characterization of Glycans -- 7.3.1 Glycan Release -- 7.3.2 Fluorescent Labeling of Glycans -- 7.3.3 Hydrophilic Interaction Liquid Chromatography -- 7.3.4 Weak Anion-Exchange Liquid Chromatography -- 7.3.5 Exoglycosidase Sequencing -- 7.3.6 Reversed-Phase Liquid Chromatography -- 7.3.7 Porous Graphitic Carbon -- 7.4 Monosaccharide Composition Analysis. | |
| 505 | 8 | |a 7.4.1 Hydrolysis of Monosaccharides -- 7.4.2 Labeling and Analysis of Monosaccharides -- 7.5 Conclusion -- References -- Chapter 8: Separation of lipids -- 8.1 Introduction and Contents -- 8.2 Definitions and Classification -- 8.3 Structures and Occurrence -- 8.3.1 Fatty Acids -- 8.3.2 Glycerolipids -- 8.3.3 Glycerophospholipids -- 8.3.4 Sphingolipids -- 8.3.5 Sterol Lipids -- 8.3.6 Prenol Lipids -- 8.3.7 Saccharolipids -- 8.3.8 Polyketides -- 8.4 Sample Handling and Extraction -- 8.4.1 Sampling and Sample Preparation -- 8.4.2 Soxhlet Extraction -- 8.4.3 Method of Folch, Lees, and Stanley -- 8.4.4 Method of Bligh and Dyer -- 8.4.5 Accelerated Solvent Extraction -- 8.4.6 Supercritical Fluid Extraction -- 8.4.7 Microwave-Assisted Extraction -- 8.4.8 Other Extraction Methods -- 8.5 Lipid Analysis by LC -- 8.5.1 Thin-Layer Chromatography -- 8.5.1.1 High-Performance and Two-Dimensional TLC -- 8.5.1.2 Detection and Quantification in TLC -- 8.5.2 High-Performance Liquid Chromatography -- 8.5.2.1 Normal-Phase Liquid Chromatography -- 8.5.2.2 Silver-Ion Liquid Chromatography -- 8.5.2.3 Non-aqueous Reversed-Phase Liquid Chromatography -- 8.5.2.4 Other HPLC Techniques -- 8.5.3 HPLC-MS Techniques -- 8.5.3.1 Lipidomics and Data Processing -- 8.5.4 Multidimensional Liquid Chromatography (MDLC, 2DLC) -- 8.6 Conclusions and Future Perspectives -- References -- Chapter 9: Metabolic phenotyping (metabonomics/metabolomics) by liquid chromatography-mass spectrometry -- 9.1 Introduction -- 9.2 LC-MS-based approaches to metabolic phenotyping -- 9.2.1 Reversed-Phase HPLC and U(H)PLC/MS for Metabolic Phenotyping -- 9.2.2 Polar Metabolite Analysis via HILIC, Aqueous Normal Phase (ANP), and Ion Chromatography(IC)/Ion Exchange (IE) LC-MS ... -- 9.2.3 Multicolumn and Multidimensional LC Separations -- 9.2.4 Miniaturization -- 9.3 Supercritical fluid chromatography (SFC). | |
| 505 | 8 | |a 9.4 Ion Mobility Spectrometry -- 9.5 Conclusions -- References -- Chapter 10: Foodomics: LC and LC-MS-based omics strategies in food science and nutrition -- 10.1 Introduction -- 10.2 Fundamentals of omics approaches based on LC -- 10.2.1 Proteomics -- 10.2.2 Peptidomics -- 10.2.3 Metabolomics -- 10.2.4 Lipidomics -- 10.2.5 Glycomics -- 10.3 LC-based foodomics applications -- 10.3.1 Food Bioactivity -- 10.3.2 Food Safety -- 10.3.2.1 Chemical contaminants -- 10.3.2.2 Pathogens and toxins -- 10.3.2.3 Food allergens -- 10.3.3 Food Quality, Authenticity, and Traceability -- Acknowledgments -- References -- Chapter 11: Forensic toxicology -- 11.1 General drug screening -- 11.1.1 Extraction Techniques -- 11.1.2 Screening Using Diode Array Detection -- 11.2 Liquid chromatography-mass spectrometry: background and considerations -- 11.2.1 Atmospheric Pressure Ionization Sources: APCI, ESI -- 11.2.2 ESI and Mobile Phase pH -- 11.2.3 Atmospheric-Pressure Chemical Ionization -- 11.2.4 General Practical Considerations for LC-MS -- 11.3 Forensic toxicology LC-MS applications -- 11.3.1 Overview -- 11.3.2 Single Quadrupole Instruments -- 11.3.3 Time-of-Flight Instruments -- 11.3.4 Orbitrap Analysers -- 11.3.5 Low Resolution Ion Traps -- 11.3.6 Data Dependent Acquisition and Data Independent Acquisition for Broad Screening -- 11.4 LCMS identification criteria in forensic toxicology -- 11.4.1 The Continuing Relevance of Chromatography -- 11.4.2 MS Identification Criteria -- 11.5 Validation and matrix effects -- 11.5.1 Validation Requirements -- 11.5.2 Matrix Effects -- 11.6 Testing for driving under the influence of drugs using oral fluids -- 11.6.1 Analytical Methodology -- 11.6.2 Sample Preparation -- 11.6.3 LC-Tandem MS -- 11.6.4 Liquid Chromatography Analysis of Oral Fluid-Conclusions and Future Directions. | |
| 506 | |a Plný text je dostupný pouze z IP adres počítačů Univerzity Tomáše Bati ve Zlíně nebo vzdáleným přístupem pro zaměstnance a studenty | ||
| 590 | |a Knovel |b Knovel (All titles) | ||
| 650 | 0 | |a Liquid chromatography. | |
| 655 | 7 | |a elektronické knihy |7 fd186907 |2 czenas | |
| 655 | 9 | |a electronic books |2 eczenas | |
| 700 | 1 | |a Fanali, Salvatore, |e editor. |1 https://id.oclc.org/worldcat/entity/E39PBJkHhWDYbfwxmcMmGyj9jC | |
| 700 | 1 | |a Haddad, Paul R., |e editor. |1 https://id.oclc.org/worldcat/entity/E39PBJdCqTr6Mggdq6bJp46dwC | |
| 700 | 1 | |a Poole, Colin, |e editor. |1 https://id.oclc.org/worldcat/entity/E39PCjDfgPdyb7RRmGYftgjYMX | |
| 700 | 1 | |a Riekkola, Marja-Liisa, |e editor. | |
| 776 | 0 | 8 | |c Original |z 0128053925 |z 9780128053928 |w (OCoLC)962889245 |
| 856 | 4 | 0 | |u https://proxy.k.utb.cz/login?url=https://app.knovel.com/hotlink/toc/id:kpLCAVE004/liquid-chromatography-applications?kpromoter=marc |y Full text |