Advanced practical organic chemistry.
General introductionSafetySafety is your primary responsibilitySafe working practiceSafety risk assessmentsCommon hazardsAccident and emergency proceduresBibliographyKeeping records of laboratory workIntroductionThe laboratory notebookKeeping records of dataSome tips on report and thesis preparation...
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| Main Authors: | , , |
|---|---|
| Format: | eBook |
| Language: | English |
| Published: |
Boca Raton :
CRC Press, Taylor & Francis Group,
[2013]
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| Edition: | Third edition / |
| Subjects: | |
| ISBN: | 9781628706864 1628706864 9781466593541 1466593547 9781466593558 1466593555 9781439860984 143986098X 9781439860977 1439860971 |
| Physical Description: | 1 online resource (xxv, 330 pages) : illustrations |
Cover
Table of contents
| LEADER | 05930cam a2200517 i 4500 | ||
|---|---|---|---|
| 001 | kn-ocn883131986 | ||
| 003 | OCoLC | ||
| 005 | 20240717213016.0 | ||
| 006 | m o d | ||
| 007 | cr cn||||||||| | ||
| 008 | 140708s2013 flua obf 001 0 eng d | ||
| 040 | |a KNOVL |b eng |e rda |e pn |c KNOVL |d EBLCP |d DEBSZ |d SCB |d UMI |d OCL |d YDXCP |d DEBBG |d CRCPR |d OCLCQ |d MERUC |d KIJ |d CEF |d OCLCQ |d AU@ |d OCLCQ |d WYU |d OCL |d UKAHL |d OCLCQ |d OCL |d VT2 |d OCLCO |d OCLCQ |d OCLCO |d OCLCQ | ||
| 020 | |a 9781628706864 |q (electronic bk.) | ||
| 020 | |a 1628706864 |q (electronic bk.) | ||
| 020 | |a 9781466593541 | ||
| 020 | |a 1466593547 | ||
| 020 | |a 9781466593558 | ||
| 020 | |a 1466593555 | ||
| 020 | |a 9781439860984 | ||
| 020 | |a 143986098X | ||
| 020 | |z 9781439860977 | ||
| 020 | |z 1439860971 | ||
| 035 | |a (OCoLC)883131986 |z (OCoLC)915143490 |z (OCoLC)960895203 |z (OCoLC)965394983 |z (OCoLC)1004169988 |z (OCoLC)1066421167 |z (OCoLC)1156398076 |z (OCoLC)1192347139 |z (OCoLC)1262672582 | ||
| 100 | 1 | |a Leonard, J. |q (John), |d 1954- |e author. | |
| 245 | 1 | 0 | |a Advanced practical organic chemistry. |
| 250 | |a Third edition / |b John Leonard, Barry Lygo, Garry Procter. | ||
| 264 | 1 | |a Boca Raton : |b CRC Press, Taylor & Francis Group, |c [2013] | |
| 264 | 4 | |c ©2013 | |
| 300 | |a 1 online resource (xxv, 330 pages) : |b illustrations | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 504 | |a Includes bibliographical references and index. | ||
| 505 | 0 | |a General introduction -- Safety -- Keeping records of laboratory work -- Equipping the laboratory and the bench -- Purification and drying of solvents -- Reagents : preparation, purification, and handling -- Gases -- Vacuum pumps -- Carrying out the reaction -- Working up the reaction -- Purification -- Small-scale reactions -- Large-scale reactions -- Special procedures -- Characterization -- Troubleshooting : what to do when things don't work -- The chemical literature -- Appendix 1. Properties of common solvents -- Appendix 2. Properties of common gases -- Appendix 3. Approximate pKa values for some common reagents versus common bases -- Appendix 4. Common Bronsted acids -- Appendix 5. Common Lewis acids -- Appendix 6. Common reducing reagents -- Appendix 7. Common oxidizing reagents. | |
| 506 | |a Plný text je dostupný pouze z IP adres počítačů Univerzity Tomáše Bati ve Zlíně nebo vzdáleným přístupem pro zaměstnance a studenty | ||
| 520 | |a General introductionSafetySafety is your primary responsibilitySafe working practiceSafety risk assessmentsCommon hazardsAccident and emergency proceduresBibliographyKeeping records of laboratory workIntroductionThe laboratory notebookKeeping records of dataSome tips on report and thesis preparationReferencesEquipping the laboratory and the benchIntroductionSetting up the laboratoryGeneral laboratory equipmentThe individual benchEquipment for parallel experimentsEquipment for controlled experimentationPurification and drying of solventsIntroductionPurification of solventsDrying agentsDrying of solventsReferencesReagents: Preparation, purification, and handlingIntroductionClassification of reagents for handlingTechniques for obtaining pure and dry reagentsTechniques for handling and measuring reagentsPreparation and titration of simple organometallic reagents and lithium amide basesPreparation of diazomethaneReferencesGasesIntroductionUse of gas cylindersHandling gasesMeasurement of gasesInert gasesReagent gasesReferencesVacuum pumpsIntroductionHouse vacuum systems (low vacuum)Medium vacuum pumpsHigh vacuum pumpsPressure measurement and regulationCarrying out the reactionIntroductionReactions with air-sensitive reagentsReaction monitoringReactions at other than room temperatureDriving equilibriaAgitationUse of controlled reactor systemsReferencesWorking up the reactionIntroductionQuenching the reactionIsolation of the crude productData that need to be collected on the crude product prior to purificationPurificationIntroductionCrystallizationDistillationSublimationFlash chromatographyDry-column flash chromatographyPreparative TLCMedium pressure and prepacked chromatography systemsPreparative HPLCReferencesSmall-scale reactionsIntroductionReactions at or below room temperatureReactions above room temperatureReactions in NMR tubesPurification of. | ||
| 520 | 8 | |a MaterialsLarge-scale reactionsIntroductionCarrying out the reactionWorkup and product isolationPurification of the productsSpecial proceduresIntroductionCatalytic hydrogenationPhotolysisOzonolysisFlash vacuum pyrolysis (FVP)Liquid ammonia reactionsMicrowave reactionsReferencesCharacterizationIntroductionNMR spectraIR spectraUV spectroscopyMass spectrometryMelting point (m.p.) and boiling point (b.p.)Optical rotationMicroanalysisKeeping the dataTroubleshooting: What to do when things don't workThe chemical literatureThe structure of the chemical literatureSome important paper-based sources of chemical informationSome important electronic-based sources of chemical informationHow to find chemical informationCurrent awarenessReferencesAppendicesProperties of common solventsProperties of common gasesApproximate pKa values for some common reagents versus common basesCommon Bronsted acidsCommon Lewis acidsCommon reducing reagentsCommon oxidizing reagentsIndex. | |
| 590 | |a Knovel |b Knovel (All titles) | ||
| 650 | 0 | |a Organic compounds |x Synthesis. | |
| 650 | 0 | |a Chemistry, Organic |v Laboratory manuals. | |
| 655 | 7 | |a elektronické knihy |7 fd186907 |2 czenas | |
| 655 | 9 | |a electronic books |2 eczenas | |
| 700 | 1 | |a Lygo, B., |e author. | |
| 700 | 1 | |a Procter, Garry, |e author. | |
| 776 | 0 | 8 | |i Print version: |a Leonard, J. (John), 1954- |t Advanced practical organic chemistry. |b Third edition |z 9781439860977 |w (DLC) 2013443454 |w (OCoLC)816163080 |
| 856 | 4 | 0 | |u https://proxy.k.utb.cz/login?url=https://app.knovel.com/hotlink/toc/id:kpAPOCE00L/advanced-practical-organic?kpromoter=marc |y Full text |
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