High-temperature liquid chromatography : a user's guide for method development
"High-temperature liquid chromatography has attracted much interest in recent years but has not yet recognized its full potential in the chromatographic community. There is a widespread reluctance in industry to use temperature to speed up the separation process, influence the selectivity of a...
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| Main Author: | |
|---|---|
| Format: | eBook |
| Language: | English |
| Published: |
Cambridge :
RSC Pub.,
©2010.
|
| Series: | RSC chromatography monographs.
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| Subjects: | |
| ISBN: | 9781621981626 1621981622 1849731098 9781849731096 9781849730136 184973013X |
| Physical Description: | 1 online resource (x, 210 pages) : illustrations |
Cover
Table of contents
| LEADER | 04780cam a2200445Ma 4500 | ||
|---|---|---|---|
| 001 | kn-ocn776987438 | ||
| 003 | OCoLC | ||
| 005 | 20240717213016.0 | ||
| 006 | m o d | ||
| 007 | cr cn||||||||| | ||
| 008 | 110919s2010 enka ob 001 0 eng d | ||
| 040 | |a COO |b eng |e pn |c COO |d KNOVL |d E7B |d OCLCQ |d KNOVL |d OCLCF |d KNOVL |d ZCU |d KNOVL |d YDXCP |d OCLCQ |d AZK |d LVT |d AGLDB |d MOR |d CCO |d LIP |d OCLCQ |d U3W |d BUF |d STF |d WRM |d OCLCQ |d CEF |d RRP |d OCLCQ |d INT |d VT2 |d OCLCQ |d WYU |d ICG |d YOU |d OCLCQ |d AU@ |d UKAHL |d OCLCQ |d S9I |d UKCRE |d OCLCO |d OCLCQ |d OCLCO |d OCLCL |d SXB |d TUHNV | ||
| 020 | |a 9781621981626 |q (electronic bk.) | ||
| 020 | |a 1621981622 |q (electronic bk.) | ||
| 020 | |a 1849731098 | ||
| 020 | |a 9781849731096 | ||
| 020 | |z 9781849730136 | ||
| 020 | |z 184973013X | ||
| 020 | |z 9781849731096 | ||
| 035 | |a (OCoLC)776987438 |z (OCoLC)961676171 |z (OCoLC)962602507 |z (OCoLC)972040027 |z (OCoLC)988417250 |z (OCoLC)1037756676 |z (OCoLC)1038669839 |z (OCoLC)1038694521 |z (OCoLC)1055370673 |z (OCoLC)1066048348 |z (OCoLC)1077239651 |z (OCoLC)1153541977 |z (OCoLC)1228614953 |z (OCoLC)1243589969 | ||
| 100 | 1 | |a Teutenberg, Thorsten. | |
| 245 | 1 | 0 | |a High-temperature liquid chromatography : |b a user's guide for method development / |c Thorsten Teutenberg. |
| 260 | |a Cambridge : |b RSC Pub., |c ©2010. | ||
| 300 | |a 1 online resource (x, 210 pages) : |b illustrations | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 490 | 1 | |a RSC chromatography monographs | |
| 504 | |a Includes bibliographical references and index. | ||
| 505 | 0 | |a A brief definition of high-temperature liquid chromatography -- System set-up for high-temperature liquid chromatography -- The heating system -- Mobile phase considerations -- Suitable stationary phases -- Method development using temperature as an active variable -- Analyte stability -- Special hyphenation techniques -- Critical outlook and future prospects. | |
| 506 | |a Plný text je dostupný pouze z IP adres počítačů Univerzity Tomáše Bati ve Zlíně nebo vzdáleným přístupem pro zaměstnance a studenty | ||
| 520 | |a "High-temperature liquid chromatography has attracted much interest in recent years but has not yet recognized its full potential in the chromatographic community. There is a widespread reluctance in industry to use temperature to speed up the separation process, influence the selectivity of a separation or implement novel detection techniques. However, the technology has now matured and could revolutionize chromatography as we see it today. Better equipment, such as heating systems able to generate faster heating rates, is becoming more readily available. Also, columns based on silica gel, which can withstand higher temperatures for an extended period, are now being introduced. Nevertheless, further technological and methodical efforts are needed to establish the method in a regulated environment like the pharmaceutical industry. This is the only text to cover all the practical aspects, as well as the underlying theoretical principles, of setting up an HPLC system for high temperature operation. It is not intended solely for academics but will also benefit the researcher interested in more practical considerations. The author is a recognized expert and has conducted several studies with partners from industry to validate the method. Many real examples from these studies have been included in the book. The aim is to support practitioners in the creation of their own protocols without the need to rely solely on trial and error. The book starts with a brief definition of high temperature liquid chromatography before going on to cover: system set up; the heating system; mobile phase considerations; suitable stationary phases; method development using temperature programming; analyte stability, and special hyphenation techniques using superheated water as a mobile phase. In each chapter, experimental data is used to illustrate the main statements and the advantages over conventional HPLC are evaluated. The book concludes with a critical outlook on further developments and applications underlining the necessary advances needed to make high temperature HPLC more robust."--Page 4 of cover. | ||
| 590 | |a Knovel |b Knovel (All titles) | ||
| 650 | 0 | |a High performance liquid chromatography. | |
| 650 | 0 | |a High temperature chemistry. | |
| 655 | 7 | |a elektronické knihy |7 fd186907 |2 czenas | |
| 655 | 9 | |a electronic books |2 eczenas | |
| 776 | 0 | 8 | |i Print version: |a Teutenberg, Thorsten. |t High-temperature liquid chromatography. |d Cambridge : RSC Pub., ©2010 |w (DLC) 2011499097 |
| 830 | 0 | |a RSC chromatography monographs. | |
| 856 | 4 | 0 | |u https://proxy.k.utb.cz/login?url=https://app.knovel.com/hotlink/toc/id:kpHTLCAUGD/high-temperature-liquid?kpromoter=marc |y Full text |
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